Accessory for high‐sensitivity spectrometry of strongly absorbing and air‐sensitive liquid samples under vacuum

Accessory for high‐sensitivity spectrometry of strongly absorbing and air‐sensitive liquid samples under vacuum

A simple accessory of a previously reported optical absorption cell allows some operations on the sample, and spectrometric measurements with the cell and sample under vacuum to be performed. It enables one to handle extremely air‐sensitive specimens, and to get easily and reproducibly liquid films...

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Veröffentlicht in:Review of scientific instruments 1990-10, Vol.61 (10), p.2696-2698
1. Verfasser: Lunelli, Bruno
Format: Artikel
Sprache:eng
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Exact sciences and technology
Instruments, apparatus, components and techniques common to several branches of physics and astronomy
Optical instruments, equipment and techniques
Physics
Visible and ultraviolet spectrometers
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container_title Review of scientific instruments
container_volume 61
creator Lunelli, Bruno
description A simple accessory of a previously reported optical absorption cell allows some operations on the sample, and spectrometric measurements with the cell and sample under vacuum to be performed. It enables one to handle extremely air‐sensitive specimens, and to get easily and reproducibly liquid films of thickness down to 6 μm. Consequently it is possible to record the entire IR spectrum of a solute in a single solvent and to use very strongly absorbing solvents, water included.
doi_str_mv 10.1063/1.1141862
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source AIP Digital Archive
subjects Exact sciences and technology
Instruments, apparatus, components and techniques common to several branches of physics and astronomy
Optical instruments, equipment and techniques
Physics
Visible and ultraviolet spectrometers
title Accessory for high‐sensitivity spectrometry of strongly absorbing and air‐sensitive liquid samples under vacuum
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