Reductive cleavage of annulated 5,6-dihydro-2-1,2,4-thiadiazine-1,1-dioxides: medium sized ring azasultams

Reductive cleavage of annulated 5,6-dihydro-2-1,2,4-thiadiazine-1,1-dioxides: medium sized ring azasultams

A novel method for synthesis of medium sized ring azasultams was proposed. It includes reductive cleavage with sodium cyanoborohydride of annulated 5,6-dihydro-2 H -1,2,4-thiadiazine-1,1-dioxides that were prepared in bulk quantities by an improved procedure consisting of reacting cyclic imidates wi...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Chemical communications (Cambridge, England) England), 2023-07, Vol.59 (61), p.9396-9399
Hauptverfasser: Lysenko, Viacheslav, Nazarenko, Kostiantyn, Shishkina, Svitlana, Kostyuk, Aleksandr
Format: Artikel
Sprache:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page 9399
container_issue 61
container_start_page 9396
container_title Chemical communications (Cambridge, England)
container_volume 59
creator Lysenko, Viacheslav
Nazarenko, Kostiantyn
Shishkina, Svitlana
Kostyuk, Aleksandr
description A novel method for synthesis of medium sized ring azasultams was proposed. It includes reductive cleavage with sodium cyanoborohydride of annulated 5,6-dihydro-2 H -1,2,4-thiadiazine-1,1-dioxides that were prepared in bulk quantities by an improved procedure consisting of reacting cyclic imidates with taurine followed by treatment with phosphorus oxychloride in the presence of DIPEA. A novel method for synthesis of medium sized ring azasultams was proposed.
doi_str_mv 10.1039/d3cc02849f
format Article
fullrecord <record><control><sourceid>rsc</sourceid><recordid>TN_cdi_rsc_primary_d3cc02849f</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>d3cc02849f</sourcerecordid><originalsourceid>FETCH-rsc_primary_d3cc02849f3</originalsourceid><addsrcrecordid>eNqFjz9rwzAUxEVIoUnbpXtAH8BKLUtK7K6hoXPJ0M08pGfnBf8Jkm1qf_q4UOiYW-64HzccY68y3spYZW9OWRsnqc6KBVtJtdPC6PR7-ZtNJvZKm0e2DuESz5ImXbHLF7redjQgtxXCACXytuDQNH0FHTpuop1wdB6db0UiZJREWnRnAkcwUYNzI2fe_pDD8M5rdNTXPNA0Tz01JYcJQl91UIdn9lBAFfDlz5_Y5vhxOnwKH2x-9VSDH_P_A-oevwG5JEir</addsrcrecordid><sourcetype>Publisher</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>Reductive cleavage of annulated 5,6-dihydro-2-1,2,4-thiadiazine-1,1-dioxides: medium sized ring azasultams</title><source>Royal Society Of Chemistry Journals 2008-</source><source>Alma/SFX Local Collection</source><creator>Lysenko, Viacheslav ; Nazarenko, Kostiantyn ; Shishkina, Svitlana ; Kostyuk, Aleksandr</creator><creatorcontrib>Lysenko, Viacheslav ; Nazarenko, Kostiantyn ; Shishkina, Svitlana ; Kostyuk, Aleksandr</creatorcontrib><description>A novel method for synthesis of medium sized ring azasultams was proposed. It includes reductive cleavage with sodium cyanoborohydride of annulated 5,6-dihydro-2 H -1,2,4-thiadiazine-1,1-dioxides that were prepared in bulk quantities by an improved procedure consisting of reacting cyclic imidates with taurine followed by treatment with phosphorus oxychloride in the presence of DIPEA. A novel method for synthesis of medium sized ring azasultams was proposed.</description><identifier>ISSN: 1359-7345</identifier><identifier>EISSN: 1364-548X</identifier><identifier>DOI: 10.1039/d3cc02849f</identifier><ispartof>Chemical communications (Cambridge, England), 2023-07, Vol.59 (61), p.9396-9399</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27903,27904</link.rule.ids></links><search><creatorcontrib>Lysenko, Viacheslav</creatorcontrib><creatorcontrib>Nazarenko, Kostiantyn</creatorcontrib><creatorcontrib>Shishkina, Svitlana</creatorcontrib><creatorcontrib>Kostyuk, Aleksandr</creatorcontrib><title>Reductive cleavage of annulated 5,6-dihydro-2-1,2,4-thiadiazine-1,1-dioxides: medium sized ring azasultams</title><title>Chemical communications (Cambridge, England)</title><description>A novel method for synthesis of medium sized ring azasultams was proposed. It includes reductive cleavage with sodium cyanoborohydride of annulated 5,6-dihydro-2 H -1,2,4-thiadiazine-1,1-dioxides that were prepared in bulk quantities by an improved procedure consisting of reacting cyclic imidates with taurine followed by treatment with phosphorus oxychloride in the presence of DIPEA. A novel method for synthesis of medium sized ring azasultams was proposed.</description><issn>1359-7345</issn><issn>1364-548X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid/><recordid>eNqFjz9rwzAUxEVIoUnbpXtAH8BKLUtK7K6hoXPJ0M08pGfnBf8Jkm1qf_q4UOiYW-64HzccY68y3spYZW9OWRsnqc6KBVtJtdPC6PR7-ZtNJvZKm0e2DuESz5ImXbHLF7redjQgtxXCACXytuDQNH0FHTpuop1wdB6db0UiZJREWnRnAkcwUYNzI2fe_pDD8M5rdNTXPNA0Tz01JYcJQl91UIdn9lBAFfDlz5_Y5vhxOnwKH2x-9VSDH_P_A-oevwG5JEir</recordid><startdate>20230727</startdate><enddate>20230727</enddate><creator>Lysenko, Viacheslav</creator><creator>Nazarenko, Kostiantyn</creator><creator>Shishkina, Svitlana</creator><creator>Kostyuk, Aleksandr</creator><scope/></search><sort><creationdate>20230727</creationdate><title>Reductive cleavage of annulated 5,6-dihydro-2-1,2,4-thiadiazine-1,1-dioxides: medium sized ring azasultams</title><author>Lysenko, Viacheslav ; Nazarenko, Kostiantyn ; Shishkina, Svitlana ; Kostyuk, Aleksandr</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-rsc_primary_d3cc02849f3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><creationdate>2023</creationdate><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lysenko, Viacheslav</creatorcontrib><creatorcontrib>Nazarenko, Kostiantyn</creatorcontrib><creatorcontrib>Shishkina, Svitlana</creatorcontrib><creatorcontrib>Kostyuk, Aleksandr</creatorcontrib><jtitle>Chemical communications (Cambridge, England)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lysenko, Viacheslav</au><au>Nazarenko, Kostiantyn</au><au>Shishkina, Svitlana</au><au>Kostyuk, Aleksandr</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Reductive cleavage of annulated 5,6-dihydro-2-1,2,4-thiadiazine-1,1-dioxides: medium sized ring azasultams</atitle><jtitle>Chemical communications (Cambridge, England)</jtitle><date>2023-07-27</date><risdate>2023</risdate><volume>59</volume><issue>61</issue><spage>9396</spage><epage>9399</epage><pages>9396-9399</pages><issn>1359-7345</issn><eissn>1364-548X</eissn><abstract>A novel method for synthesis of medium sized ring azasultams was proposed. It includes reductive cleavage with sodium cyanoborohydride of annulated 5,6-dihydro-2 H -1,2,4-thiadiazine-1,1-dioxides that were prepared in bulk quantities by an improved procedure consisting of reacting cyclic imidates with taurine followed by treatment with phosphorus oxychloride in the presence of DIPEA. A novel method for synthesis of medium sized ring azasultams was proposed.</abstract><doi>10.1039/d3cc02849f</doi><tpages>4</tpages></addata></record>
fulltext fulltext
identifier ISSN: 1359-7345
ispartof Chemical communications (Cambridge, England), 2023-07, Vol.59 (61), p.9396-9399
issn 1359-7345
1364-548X
language
recordid cdi_rsc_primary_d3cc02849f
source Royal Society Of Chemistry Journals 2008-; Alma/SFX Local Collection
title Reductive cleavage of annulated 5,6-dihydro-2-1,2,4-thiadiazine-1,1-dioxides: medium sized ring azasultams
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-23T09%3A44%3A32IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-rsc&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Reductive%20cleavage%20of%20annulated%205,6-dihydro-2-1,2,4-thiadiazine-1,1-dioxides:%20medium%20sized%20ring%20azasultams&rft.jtitle=Chemical%20communications%20(Cambridge,%20England)&rft.au=Lysenko,%20Viacheslav&rft.date=2023-07-27&rft.volume=59&rft.issue=61&rft.spage=9396&rft.epage=9399&rft.pages=9396-9399&rft.issn=1359-7345&rft.eissn=1364-548X&rft_id=info:doi/10.1039/d3cc02849f&rft_dat=%3Crsc%3Ed3cc02849f%3C/rsc%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rfr_iscdi=true