Laboratory-scale near-edge X-ray absorption fine structure spectroscopy with a laser-induced plasma source
The authors present a compact soft X-ray spectrometer based on a long-term stable and nearly debris-free picosecond laser-induced plasma from a pulsed krypton gas jet target, suitable for near-edge X-ray absorption fine structure (NEXAFS) spectroscopy in the energy range between 250 to 1000 eV. Alon...
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| Veröffentlicht in: | Journal of analytical atomic spectrometry 2019-09, Vol.34 (9), p.1779-1785 |
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| container_end_page | 1785 |
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| container_issue | 9 |
| container_start_page | 1779 |
| container_title | Journal of analytical atomic spectrometry |
| container_volume | 34 |
| creator | Mller, Matthias Schellhorn, Meike Mann, Klaus |
| description | The authors present a compact soft X-ray spectrometer based on a long-term stable and nearly debris-free picosecond laser-induced plasma from a pulsed krypton gas jet target, suitable for near-edge X-ray absorption fine structure (NEXAFS) spectroscopy in the energy range between 250 to 1000 eV. Along with a detailed description of the table-top spectrometer reaching a spectral resolution of up to
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/
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500 at an energy of 430 eV, NEXAFS measurements were conducted at the carbon, nitrogen and oxygen K-edge. Additionally, oxidation state and coordination at the L-edge of various manganese and iron compounds were analyzed for the first time with a laboratory-scale NEXAFS system.
A compact spectrometer for laboratory NEXAFS measurements, allowing quantitative chemical analysis in the soft X-ray spectral range (2501000 eV). |
| doi_str_mv | 10.1039/c9ja00140a |
| format | Article |
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E
/
E
500 at an energy of 430 eV, NEXAFS measurements were conducted at the carbon, nitrogen and oxygen K-edge. Additionally, oxidation state and coordination at the L-edge of various manganese and iron compounds were analyzed for the first time with a laboratory-scale NEXAFS system.
A compact spectrometer for laboratory NEXAFS measurements, allowing quantitative chemical analysis in the soft X-ray spectral range (2501000 eV).</description><identifier>ISSN: 0267-9477</identifier><identifier>EISSN: 1364-5544</identifier><identifier>DOI: 10.1039/c9ja00140a</identifier><language>eng</language><publisher>London: Royal Society of Chemistry</publisher><subject>Fine structure ; Gas jets ; Iron compounds ; Krypton ; Laboratories ; Laser plasmas ; Manganese ; Oxidation ; Soft x rays ; Spectral resolution ; Spectroscopy ; Spectrum analysis ; Valence ; X ray absorption ; X ray spectrometers</subject><ispartof>Journal of analytical atomic spectrometry, 2019-09, Vol.34 (9), p.1779-1785</ispartof><rights>Copyright Royal Society of Chemistry 2019</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c358t-eccd140051ebf5d20cb8b9decf36a0097ab86998f460dc95552b12e9f8503d5d3</citedby><cites>FETCH-LOGICAL-c358t-eccd140051ebf5d20cb8b9decf36a0097ab86998f460dc95552b12e9f8503d5d3</cites><orcidid>0000-0002-7252-3412</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27915,27916</link.rule.ids></links><search><creatorcontrib>Mller, Matthias</creatorcontrib><creatorcontrib>Schellhorn, Meike</creatorcontrib><creatorcontrib>Mann, Klaus</creatorcontrib><title>Laboratory-scale near-edge X-ray absorption fine structure spectroscopy with a laser-induced plasma source</title><title>Journal of analytical atomic spectrometry</title><description>The authors present a compact soft X-ray spectrometer based on a long-term stable and nearly debris-free picosecond laser-induced plasma from a pulsed krypton gas jet target, suitable for near-edge X-ray absorption fine structure (NEXAFS) spectroscopy in the energy range between 250 to 1000 eV. Along with a detailed description of the table-top spectrometer reaching a spectral resolution of up to
E
/
E
500 at an energy of 430 eV, NEXAFS measurements were conducted at the carbon, nitrogen and oxygen K-edge. Additionally, oxidation state and coordination at the L-edge of various manganese and iron compounds were analyzed for the first time with a laboratory-scale NEXAFS system.
A compact spectrometer for laboratory NEXAFS measurements, allowing quantitative chemical analysis in the soft X-ray spectral range (2501000 eV).</description><subject>Fine structure</subject><subject>Gas jets</subject><subject>Iron compounds</subject><subject>Krypton</subject><subject>Laboratories</subject><subject>Laser plasmas</subject><subject>Manganese</subject><subject>Oxidation</subject><subject>Soft x rays</subject><subject>Spectral resolution</subject><subject>Spectroscopy</subject><subject>Spectrum analysis</subject><subject>Valence</subject><subject>X ray absorption</subject><subject>X ray spectrometers</subject><issn>0267-9477</issn><issn>1364-5544</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><recordid>eNpFkE1LxDAQhoMouH5cvAsBb0I0SZu2OS6Lnyx4UfBW0slUW3abmqRI_73RFT3NDDzMy_sQcib4leCZvgbdG85Fzs0eWYisyJlSeb5PFlwWJdN5WR6SoxB6znmupFqQfm0a5010fmYBzAbpgMYztG9IX5k3MzVNcH6MnRto2w1IQ_QTxMmnbUSI3gVw40w_u_hODd2YgJ51g50ALR3TuTU0uMkDnpCD1mwCnv7OY_Jye_O8umfrp7uH1XLNIFNVZAhgUwGuBDatspJDUzXaIrRZkbrp0jRVoXXV5gW3oJVSshESdVspnllls2Nysfs7evcxYYh1n_KHFFlLWUleCFUWibrcUZAaBI9tPfpua_xcC15_u6xX-nH543KZ4PMd7AP8cf-usy-3iXJW</recordid><startdate>20190901</startdate><enddate>20190901</enddate><creator>Mller, Matthias</creator><creator>Schellhorn, Meike</creator><creator>Mann, Klaus</creator><general>Royal Society of Chemistry</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><orcidid>https://orcid.org/0000-0002-7252-3412</orcidid></search><sort><creationdate>20190901</creationdate><title>Laboratory-scale near-edge X-ray absorption fine structure spectroscopy with a laser-induced plasma source</title><author>Mller, Matthias ; Schellhorn, Meike ; Mann, Klaus</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c358t-eccd140051ebf5d20cb8b9decf36a0097ab86998f460dc95552b12e9f8503d5d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Fine structure</topic><topic>Gas jets</topic><topic>Iron compounds</topic><topic>Krypton</topic><topic>Laboratories</topic><topic>Laser plasmas</topic><topic>Manganese</topic><topic>Oxidation</topic><topic>Soft x rays</topic><topic>Spectral resolution</topic><topic>Spectroscopy</topic><topic>Spectrum analysis</topic><topic>Valence</topic><topic>X ray absorption</topic><topic>X ray spectrometers</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Mller, Matthias</creatorcontrib><creatorcontrib>Schellhorn, Meike</creatorcontrib><creatorcontrib>Mann, Klaus</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of analytical atomic spectrometry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Mller, Matthias</au><au>Schellhorn, Meike</au><au>Mann, Klaus</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Laboratory-scale near-edge X-ray absorption fine structure spectroscopy with a laser-induced plasma source</atitle><jtitle>Journal of analytical atomic spectrometry</jtitle><date>2019-09-01</date><risdate>2019</risdate><volume>34</volume><issue>9</issue><spage>1779</spage><epage>1785</epage><pages>1779-1785</pages><issn>0267-9477</issn><eissn>1364-5544</eissn><abstract>The authors present a compact soft X-ray spectrometer based on a long-term stable and nearly debris-free picosecond laser-induced plasma from a pulsed krypton gas jet target, suitable for near-edge X-ray absorption fine structure (NEXAFS) spectroscopy in the energy range between 250 to 1000 eV. Along with a detailed description of the table-top spectrometer reaching a spectral resolution of up to
E
/
E
500 at an energy of 430 eV, NEXAFS measurements were conducted at the carbon, nitrogen and oxygen K-edge. Additionally, oxidation state and coordination at the L-edge of various manganese and iron compounds were analyzed for the first time with a laboratory-scale NEXAFS system.
A compact spectrometer for laboratory NEXAFS measurements, allowing quantitative chemical analysis in the soft X-ray spectral range (2501000 eV).</abstract><cop>London</cop><pub>Royal Society of Chemistry</pub><doi>10.1039/c9ja00140a</doi><tpages>7</tpages><orcidid>https://orcid.org/0000-0002-7252-3412</orcidid><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0267-9477 |
| ispartof | Journal of analytical atomic spectrometry, 2019-09, Vol.34 (9), p.1779-1785 |
| issn | 0267-9477 1364-5544 |
| language | eng |
| recordid | cdi_rsc_primary_c9ja00140a |
| source | Royal Society Of Chemistry Journals 2008-; Alma/SFX Local Collection |
| subjects | Fine structure Gas jets Iron compounds Krypton Laboratories Laser plasmas Manganese Oxidation Soft x rays Spectral resolution Spectroscopy Spectrum analysis Valence X ray absorption X ray spectrometers |
| title | Laboratory-scale near-edge X-ray absorption fine structure spectroscopy with a laser-induced plasma source |
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