Mechanochemical carbon-carbon bond formation that proceeds via a cocrystal intermediateElectronic supplementary information (ESI) available: Experimental and computational details, in situ Raman and PXRD data, thermal measurements, NMR data and FTIR data. CCDC 1869002 and 1818969. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c8cc07853j
We report the first cocrystal as an intermediate in a solid-state organic reaction wherein molecules of barbituric acid and vanillin assume a favorable orientation for the subsequent Knoevenagel condensation. In situ Raman monitoring revealed the first cocrystal as an intermediate in a mechanochemic...
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| creator | Lukin, Stipe Tireli, Martina Lon ari, Ivor Bariši, Dajana Šket, Primo Vrsaljko, Domagoj di Michiel, Marco Plavec, Janez U arevi, Krunoslav Halasz, Ivan |
| description | We report the first cocrystal as an intermediate in a solid-state organic reaction wherein molecules of barbituric acid and vanillin assume a favorable orientation for the subsequent Knoevenagel condensation.
In situ
Raman monitoring revealed the first cocrystal as an intermediate in a mechanochemical organic reaction. |
| doi_str_mv | 10.1039/c8cc07853j |
| format | Article |
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In situ
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In situ
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In situ
Raman monitoring revealed the first cocrystal as an intermediate in a mechanochemical organic reaction.</abstract><doi>10.1039/c8cc07853j</doi><tpages>4</tpages></addata></record> |
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| source | Royal Society Of Chemistry Journals 2008-; Alma/SFX Local Collection |
| title | Mechanochemical carbon-carbon bond formation that proceeds via a cocrystal intermediateElectronic supplementary information (ESI) available: Experimental and computational details, in situ Raman and PXRD data, thermal measurements, NMR data and FTIR data. CCDC 1869002 and 1818969. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c8cc07853j |
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