Oxidative coupling of 1-(2-methyl-4-phenylquinolin-3-yl)ethanone with ethanol and unexpected deacetylative synthesis of 3-hydroxy quinolineElectronic supplementary information (ESI) available: Experimental procedures, compound characterization, X-ray crystal structure data and ORTEP drawing for 2a; copies of NMR spectra of all the final compounds. CCDC 1492781. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c6ob02336c

Oxidative coupling of 1-(2-methyl-4-phenylquinolin-3-yl)ethanone with ethanol and unexpected deacetylative synthesis of 3-hydroxy quinolineElectronic supplementary information (ESI) available: Experimental procedures, compound characterization, X-ray crystal structure data and ORTEP drawing for 2a; copies of NMR spectra of all the final compounds. CCDC 1492781. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c6ob02336c

An efficient one pot method for the synthesis of anti -α,β-epoxy ketones from 1-(2-methyl-4-phenylquinolin-3-yl)ethanone and ethanol has been developed by a modified Darzen reaction. The reaction occurs under oxidative conditions via a cascade sequence of bromination, aldol condensation followed by...

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Hauptverfasser: Chauhan, Parul, Ravi, Makthala, Kant, Ruchir, Yadav, Prem. P
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Sprache:eng
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