Continuous niobium phosphate catalysed Skraup reaction for quinoline synthesis from solketalElectronic supplementary information (ESI) available.CCDC 1517275. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c6gc03140d
Solketal is derived from the reaction of acetone with glycerol, a by-product of the biodiesel industry. We report here the continuous reaction of solketal with anilines over a solid acid niobium phosphate (NbP), for the continuous generation of quinolines in the well-established Skraup reaction. Thi...
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