Quantitation in the regioselectivity of acylation of glycosyl diglycerides: total synthesis of a Streptococcus pneumoniae α-glucosyl diglycerideElectronic supplementary information (ESI) available. See DOI: 10.1039/c6cc09584d

The fidelity of acylation regioselectivity in the synthesis of mixed glycosyl diacylglycerols can be accurately measured by quantitative 13 C NMR spectroscopy using a 1- 13 C-labelled fatty acid and a paramagnetic relaxation enhancement agent. Exquisite regioselectivity is achieved using a stepwise...

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Hauptverfasser:	Richardson, Mark B, Smith, Dylan G. M, Williams, Spencer J
Format:	Artikel
Sprache:	eng
Online-Zugang:	Volltext
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