Homopiperazine sulfamic acid functionalized mesoporous silica nanoparticles (MSNs-HPZ-SOH) as an efficient catalyst for one-pot synthesis of 1-amidoalkyl-2-naphthols

Homopiperazine sulfamic acid functionalized mesoporous silica nanoparticles (MSNs-HPZ-SOH) as an efficient catalyst for one-pot synthesis of 1-amidoalkyl-2-naphthols

Mesoporous silica nanoparticles are efficiently functionalized with homopiperazine sulfamic acid. The resulting MSNs-HPZ-SO 3 H is employed as a nanocatalyst in one-pot synthesis of 1-amidoalkyl-2-naphthols, through three-component condensation reaction of aromatic aldehydes, amides/urea and β-napht...

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Veröffentlicht in:New journal of chemistry 2016-01, Vol.4 (5), p.472-4726
Hauptverfasser: Nasresfahani, Zahra, Kassaee, Mohammad Zaman, Eidi, Esmaiel
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creator Nasresfahani, Zahra
Kassaee, Mohammad Zaman
Eidi, Esmaiel
description Mesoporous silica nanoparticles are efficiently functionalized with homopiperazine sulfamic acid. The resulting MSNs-HPZ-SO 3 H is employed as a nanocatalyst in one-pot synthesis of 1-amidoalkyl-2-naphthols, through three-component condensation reaction of aromatic aldehydes, amides/urea and β-naphthol, under thermal solvent-free conditions. Characterizations of the catalyst are carried out using XRD, SEM, FT-IR, TGA-DTA and nitrogen adsorption-desorption analysis. This protocol is developed as a safe and convenient alternative method for the synthesis of 1-amidoalkyl-2-naphthols utilizing an ecofriendly catalyst. MSNs-HPZ-SO 3 H was synthesized, characterized, and employed as an efficient nanocatalyst in one-pot synthesis of 1-amidoalkyl-2-naphthols.
doi_str_mv 10.1039/c5nj02974k
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title Homopiperazine sulfamic acid functionalized mesoporous silica nanoparticles (MSNs-HPZ-SOH) as an efficient catalyst for one-pot synthesis of 1-amidoalkyl-2-naphthols
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