Rapid Wolff-Kishner reductions in a silicon carbide microreactorElectronic supplementary information (ESI) available: Experimental details and NMR spectra. See DOI: 10.1039/c3gc41942h
Wolff-Kishner reductions are performed in a novel silicon carbide microreactor. Greatly reduced reaction times and safer operation are achieved, giving high yields without requiring a large excess of hydrazine. The corrosion resistance of silicon carbide avoids the problematic reactor compatibility...
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