Synthesis and crystal structure of Fe6Ca2(SeO3)9Cl4 a porous oxohalideElectronic supplementary information (ESI) available: Experimental details, crystal structure refinement parameters, bond valence sum (BVS) calculations, EDS-analysis data, sorption isotherms, PXRD-data. See DOI: 10.1039/c3dt50952d
A porous oxohalide, Fe 6 Ca 2 (SeO 3 ) 9 Cl 4 , has been synthesized by solid state reactions using concentrated HCl as the Cl-source. It crystallizes in the hexagonal space group P 6 3 / m with unit cell parameters a = 12.118(2) , c = 12.703(4) , Z = 2. The crystal structure is an open framework ha...
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