Crystal structures of Mosher's salt and ester elucidated by X-ray crystallographyElectronic supplementary information (ESI) available: Supplementary Fig. S1 and S2, supplementary Scheme S1, supplementary Tables S1 and S2. CCDC 934003. For ESI and crystallographic data in CIF or other electronic format see DOI: 10.1039/c3ce41160e

The crystal structure of Mosher's salt 3 , prepared from ( R )-3,3,3-trifluoro-2-methoxy-2-phenylpropanoic acid [( R )-MTPA, ( R )- 1 ] and ( R )-1-phenylethylamine [( R )-PEA, ( R )- 2 ], was determined using X-ray crystallography. In crystalline salt 3 , the bifurcated hydrogen bond ( i.e. ,...

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Hauptverfasser: Ichikawa, Akio, Ono, Hiroshi, Mikata, Yuji
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Sprache:eng
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