High-resolution solid-state 13C NMR spectroscopy of the paramagnetic metal-organic frameworks, STAM-1 and HKUST-1Electronic supplementary information (ESI) available: Synthesis details, analysis of in situ hydration during NMR experiments, information on inversion recovery experiments, solution- and solid-state spectra of diamagnetic model systems, further NMR spectra of CD3-STAM-1, XRD pattern for 13C(1,3,4,5)-STAM-1, details of extraction of 13C-enriched Na2mmbtc from enriched STAM-1, 13C spec

High-resolution solid-state 13C NMR spectroscopy of the paramagnetic metal-organic frameworks, STAM-1 and HKUST-1Electronic supplementary information (ESI) available: Synthesis details, analysis of in situ hydration during NMR experiments, information on inversion recovery experiments, solution- and solid-state spectra of diamagnetic model systems, further NMR spectra of CD3-STAM-1, XRD pattern for 13C(1,3,4,5)-STAM-1, details of extraction of 13C-enriched Na2mmbtc from enriched STAM-1, 13C spec

Solid-state 13 C magic-angle spinning (MAS) NMR spectroscopy is used to investigate the structure of the Cu( ii )-based metal-organic frameworks (MOFs), HKUST-1 and STAM-1, and the structural changes occurring within these MOFs upon activation (dehydration). NMR spectroscopy is an attractive techniq...

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Bibliographische Detailangaben
Hauptverfasser: Dawson, Daniel M, Jamieson, Lauren E, Mohideen, M. Infas H, McKinlay, Alistair C, Smellie, Iain A, Cadou, Romain, Keddie, Neil S, Morris, Russell E, Ashbrook, Sharon E
Format: Artikel
Sprache:eng
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