Brush-like Polyaniline with Optical and Electroactive Properties at Neutral pH and High Temperature
In this research, a brush-like polyaniline (poly(2-acrylamide-2-methyl-1-propanesulfonate)-g-polyaniline)-b-poly(N-vinylcarbazole) (BL PAni) was developed as a strategy to overcome the limited processability and dedoping above pH 4 of conventional polyaniline (PAni). For the BL PAni synthesis, RAFT...
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| Veröffentlicht in: | International journal of molecular sciences 2022-08, Vol.23 (15), p.8085 |
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| creator | Conejo-Dávila, Alain Salvador Casas-Soto, Carlos Rafael Aparicio-Martínez, Eider Pedro Chávez-Flores, David Ramos-Sánchez, Víctor Hugo Dominguez, Rocio Berenice Osuna, Velia Carolina Estrada-Monje, Anayansi Vega-Rios, Alejandro Zaragoza-Contreras, Erasto Armando |
| description | In this research, a brush-like polyaniline (poly(2-acrylamide-2-methyl-1-propanesulfonate)-g-polyaniline)-b-poly(N-vinylcarbazole) (BL PAni) was developed as a strategy to overcome the limited processability and dedoping above pH 4 of conventional polyaniline (PAni). For the BL PAni synthesis, RAFT polymerization (homopolymer), RAFT-mediated surfactant-free emulsion polymerization (block copolymer), and interfacial oxidative polymerization were applied to graft the PAni chains. NMR and FT-IR spectroscopies were performed to confirm the structural elucidation of the reaction pathways, while the thermal properties were analyzed by TGA and DSC. Notably, the BL PAni presents absorption throughout the visible region and up to the near-infrared, showing dedoping resistance at up to 80 °C and at a neutral pH. The absorption range of the BL PAni, block copolymer, and homopolymer were studied by UV–Vis spectroscopy in solid-state and dispersion/solution, highlighting BL PAni and poly(anilinium 2-acrylamide-2-methyl-1-propanesulfonate)-b-poly(N-vinylcarbazole) (PAAMP-b-PVK) due to the π-stacking between the anilinium and carbazole groups. The cyclic voltammetry confirmed the persistence of electroactivity at a pH near 7. |
| doi_str_mv | 10.3390/ijms23158085 |
| format | Article |
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For the BL PAni synthesis, RAFT polymerization (homopolymer), RAFT-mediated surfactant-free emulsion polymerization (block copolymer), and interfacial oxidative polymerization were applied to graft the PAni chains. NMR and FT-IR spectroscopies were performed to confirm the structural elucidation of the reaction pathways, while the thermal properties were analyzed by TGA and DSC. Notably, the BL PAni presents absorption throughout the visible region and up to the near-infrared, showing dedoping resistance at up to 80 °C and at a neutral pH. The absorption range of the BL PAni, block copolymer, and homopolymer were studied by UV–Vis spectroscopy in solid-state and dispersion/solution, highlighting BL PAni and poly(anilinium 2-acrylamide-2-methyl-1-propanesulfonate)-b-poly(N-vinylcarbazole) (PAAMP-b-PVK) due to the π-stacking between the anilinium and carbazole groups. The cyclic voltammetry confirmed the persistence of electroactivity at a pH near 7.</description><identifier>ISSN: 1422-0067</identifier><identifier>ISSN: 1661-6596</identifier><identifier>EISSN: 1422-0067</identifier><identifier>DOI: 10.3390/ijms23158085</identifier><identifier>PMID: 35897666</identifier><language>eng</language><publisher>Basel: MDPI AG</publisher><subject>Absorption ; Acrylamide ; Addition polymerization ; Block copolymers ; Carbazole ; Carbazoles ; Carbon ; Copolymers ; Electroactivity ; Emulsion polymerization ; Graft copolymers ; Heat resistance ; High temperature ; NMR ; Nuclear magnetic resonance ; Polyanilines ; Polymerization ; Polymers ; Polyvinyl carbazole ; Quantum dots ; Spectroscopy ; Spectrum analysis ; Surfactants ; Vibration</subject><ispartof>International journal of molecular sciences, 2022-08, Vol.23 (15), p.8085</ispartof><rights>2022 by the authors. Licensee MDPI, Basel, Switzerland. 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For the BL PAni synthesis, RAFT polymerization (homopolymer), RAFT-mediated surfactant-free emulsion polymerization (block copolymer), and interfacial oxidative polymerization were applied to graft the PAni chains. NMR and FT-IR spectroscopies were performed to confirm the structural elucidation of the reaction pathways, while the thermal properties were analyzed by TGA and DSC. Notably, the BL PAni presents absorption throughout the visible region and up to the near-infrared, showing dedoping resistance at up to 80 °C and at a neutral pH. The absorption range of the BL PAni, block copolymer, and homopolymer were studied by UV–Vis spectroscopy in solid-state and dispersion/solution, highlighting BL PAni and poly(anilinium 2-acrylamide-2-methyl-1-propanesulfonate)-b-poly(N-vinylcarbazole) (PAAMP-b-PVK) due to the π-stacking between the anilinium and carbazole groups. The cyclic voltammetry confirmed the persistence of electroactivity at a pH near 7.</description><subject>Absorption</subject><subject>Acrylamide</subject><subject>Addition polymerization</subject><subject>Block copolymers</subject><subject>Carbazole</subject><subject>Carbazoles</subject><subject>Carbon</subject><subject>Copolymers</subject><subject>Electroactivity</subject><subject>Emulsion polymerization</subject><subject>Graft copolymers</subject><subject>Heat resistance</subject><subject>High temperature</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Polyanilines</subject><subject>Polymerization</subject><subject>Polymers</subject><subject>Polyvinyl carbazole</subject><subject>Quantum dots</subject><subject>Spectroscopy</subject><subject>Spectrum 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For the BL PAni synthesis, RAFT polymerization (homopolymer), RAFT-mediated surfactant-free emulsion polymerization (block copolymer), and interfacial oxidative polymerization were applied to graft the PAni chains. NMR and FT-IR spectroscopies were performed to confirm the structural elucidation of the reaction pathways, while the thermal properties were analyzed by TGA and DSC. Notably, the BL PAni presents absorption throughout the visible region and up to the near-infrared, showing dedoping resistance at up to 80 °C and at a neutral pH. The absorption range of the BL PAni, block copolymer, and homopolymer were studied by UV–Vis spectroscopy in solid-state and dispersion/solution, highlighting BL PAni and poly(anilinium 2-acrylamide-2-methyl-1-propanesulfonate)-b-poly(N-vinylcarbazole) (PAAMP-b-PVK) due to the π-stacking between the anilinium and carbazole groups. 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| source | MDPI - Multidisciplinary Digital Publishing Institute; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; PubMed Central |
| subjects | Absorption Acrylamide Addition polymerization Block copolymers Carbazole Carbazoles Carbon Copolymers Electroactivity Emulsion polymerization Graft copolymers Heat resistance High temperature NMR Nuclear magnetic resonance Polyanilines Polymerization Polymers Polyvinyl carbazole Quantum dots Spectroscopy Spectrum analysis Surfactants Vibration |
| title | Brush-like Polyaniline with Optical and Electroactive Properties at Neutral pH and High Temperature |
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