Kinetics and Adsorption Isotherms of Amine-Functionalized Magnesium Ferrite Produced Using Sol-Gel Method for Treatment of Heavy Metals in Wastewater
This study is focused on the kinetics and adsorption isotherms of amine-functionalized magnesium ferrite (MgFe O ) for treating the heavy metals in wastewater. A sol-gel route was adopted to produce MgFe O nanoparticles. The surfaces of the MgFe O nanoparticles were functionalized using primary amin...
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| Veröffentlicht in: | Materials 2022-06, Vol.15 (11), p.4009 |
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| creator | Irfan, Muhammad Zaheer, Fareeda Hussain, Humaira Naz, Muhammad Yasin Shukrullah, Shazia Legutko, Stanislaw Mahnashi, Mater H Alsaiari, Mabkhoot A Ghanim, Abdulnour Ali Jazem Rahman, Saifur Alshorman, Omar Alkahtani, Fahad Salem Khan, Mohammad K A Kruszelnicka, Izabela Ginter-Kramarczyk, Dobrochna |
| description | This study is focused on the kinetics and adsorption isotherms of amine-functionalized magnesium ferrite (MgFe
O
) for treating the heavy metals in wastewater. A sol-gel route was adopted to produce MgFe
O
nanoparticles. The surfaces of the MgFe
O
nanoparticles were functionalized using primary amine (ethanolamine). The surface morphology, phase formation, and functionality of the MgFe
O
nano-adsorbents were studied using the SEM, UV-visible, FTIR, and TGA techniques. The characterized nanoparticles were tested on their ability to adsorb the Pb
, Cu
, and Zn
ions from the wastewater. The kinetic parameters and adsorption isotherms for the adsorption of the metal ions by the amine-functionalized MgFe
O
were obtained using the pseudo-first-order, pseudo-second-order, Langmuir, and Freundlich models. The pseudo-second order and Langmuir models best described the adsorption kinetics and isotherms, implying strong chemisorption via the formation of coordinative bonds between the amine groups and metal ions. The Langmuir equation revealed the highest adsorption capacity of 0.7 mmol/g for the amine-functionalized MgFe
O
nano-adsorbents. The adsorption capacity of the nanoadsorbent also changed with the calcination temperature. The MgFe
O
sample, calcined at 500 °C, removed the most of the Pb
(73%), Cu
(59%), and Zn
(62%) ions from the water. |
| doi_str_mv | 10.3390/ma15114009 |
| format | Article |
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O
) for treating the heavy metals in wastewater. A sol-gel route was adopted to produce MgFe
O
nanoparticles. The surfaces of the MgFe
O
nanoparticles were functionalized using primary amine (ethanolamine). The surface morphology, phase formation, and functionality of the MgFe
O
nano-adsorbents were studied using the SEM, UV-visible, FTIR, and TGA techniques. The characterized nanoparticles were tested on their ability to adsorb the Pb
, Cu
, and Zn
ions from the wastewater. The kinetic parameters and adsorption isotherms for the adsorption of the metal ions by the amine-functionalized MgFe
O
were obtained using the pseudo-first-order, pseudo-second-order, Langmuir, and Freundlich models. The pseudo-second order and Langmuir models best described the adsorption kinetics and isotherms, implying strong chemisorption via the formation of coordinative bonds between the amine groups and metal ions. The Langmuir equation revealed the highest adsorption capacity of 0.7 mmol/g for the amine-functionalized MgFe
O
nano-adsorbents. The adsorption capacity of the nanoadsorbent also changed with the calcination temperature. The MgFe
O
sample, calcined at 500 °C, removed the most of the Pb
(73%), Cu
(59%), and Zn
(62%) ions from the water.</description><identifier>ISSN: 1996-1944</identifier><identifier>EISSN: 1996-1944</identifier><identifier>DOI: 10.3390/ma15114009</identifier><identifier>PMID: 35683307</identifier><language>eng</language><publisher>Switzerland: MDPI AG</publisher><subject>Adsorbents ; Adsorption ; Aqueous solutions ; Atoms & subatomic particles ; Bonding strength ; Chemical bonds ; Chemisorption ; Copper ; Heavy metals ; Isotherms ; Kinetics ; Magnesium ; Magnesium ferrites ; Magnetic fields ; Metal ions ; Metals ; Morphology ; Nanoparticles ; Nitrates ; Particle size ; Roasting ; Sol-gel processes ; Spectrum analysis ; Surface chemistry ; Wastewater</subject><ispartof>Materials, 2022-06, Vol.15 (11), p.4009</ispartof><rights>2022 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>2022 by the authors. 2022</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c406t-f1676dd9f13b0ccbf3a6be484878891644671ce085d66c9772d9e2dcb1f7f2da3</citedby><cites>FETCH-LOGICAL-c406t-f1676dd9f13b0ccbf3a6be484878891644671ce085d66c9772d9e2dcb1f7f2da3</cites><orcidid>0000-0002-7143-6085 ; 0000-0002-7262-183X ; 0000-0003-4400-2553 ; 0000-0001-8973-5035 ; 0000-0002-4366-3256 ; 0000-0002-4020-9402 ; 0000-0003-4161-6875</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC9181868/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC9181868/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,727,780,784,885,27923,27924,53790,53792</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/35683307$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Irfan, Muhammad</creatorcontrib><creatorcontrib>Zaheer, Fareeda</creatorcontrib><creatorcontrib>Hussain, Humaira</creatorcontrib><creatorcontrib>Naz, Muhammad Yasin</creatorcontrib><creatorcontrib>Shukrullah, Shazia</creatorcontrib><creatorcontrib>Legutko, Stanislaw</creatorcontrib><creatorcontrib>Mahnashi, Mater H</creatorcontrib><creatorcontrib>Alsaiari, Mabkhoot A</creatorcontrib><creatorcontrib>Ghanim, Abdulnour Ali Jazem</creatorcontrib><creatorcontrib>Rahman, Saifur</creatorcontrib><creatorcontrib>Alshorman, Omar</creatorcontrib><creatorcontrib>Alkahtani, Fahad Salem</creatorcontrib><creatorcontrib>Khan, Mohammad K A</creatorcontrib><creatorcontrib>Kruszelnicka, Izabela</creatorcontrib><creatorcontrib>Ginter-Kramarczyk, Dobrochna</creatorcontrib><title>Kinetics and Adsorption Isotherms of Amine-Functionalized Magnesium Ferrite Produced Using Sol-Gel Method for Treatment of Heavy Metals in Wastewater</title><title>Materials</title><addtitle>Materials (Basel)</addtitle><description>This study is focused on the kinetics and adsorption isotherms of amine-functionalized magnesium ferrite (MgFe
O
) for treating the heavy metals in wastewater. A sol-gel route was adopted to produce MgFe
O
nanoparticles. The surfaces of the MgFe
O
nanoparticles were functionalized using primary amine (ethanolamine). The surface morphology, phase formation, and functionality of the MgFe
O
nano-adsorbents were studied using the SEM, UV-visible, FTIR, and TGA techniques. The characterized nanoparticles were tested on their ability to adsorb the Pb
, Cu
, and Zn
ions from the wastewater. The kinetic parameters and adsorption isotherms for the adsorption of the metal ions by the amine-functionalized MgFe
O
were obtained using the pseudo-first-order, pseudo-second-order, Langmuir, and Freundlich models. The pseudo-second order and Langmuir models best described the adsorption kinetics and isotherms, implying strong chemisorption via the formation of coordinative bonds between the amine groups and metal ions. The Langmuir equation revealed the highest adsorption capacity of 0.7 mmol/g for the amine-functionalized MgFe
O
nano-adsorbents. The adsorption capacity of the nanoadsorbent also changed with the calcination temperature. The MgFe
O
sample, calcined at 500 °C, removed the most of the Pb
(73%), Cu
(59%), and Zn
(62%) ions from the water.</description><subject>Adsorbents</subject><subject>Adsorption</subject><subject>Aqueous solutions</subject><subject>Atoms & subatomic particles</subject><subject>Bonding strength</subject><subject>Chemical bonds</subject><subject>Chemisorption</subject><subject>Copper</subject><subject>Heavy metals</subject><subject>Isotherms</subject><subject>Kinetics</subject><subject>Magnesium</subject><subject>Magnesium ferrites</subject><subject>Magnetic fields</subject><subject>Metal ions</subject><subject>Metals</subject><subject>Morphology</subject><subject>Nanoparticles</subject><subject>Nitrates</subject><subject>Particle size</subject><subject>Roasting</subject><subject>Sol-gel processes</subject><subject>Spectrum analysis</subject><subject>Surface chemistry</subject><subject>Wastewater</subject><issn>1996-1944</issn><issn>1996-1944</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNpdkVFLHDEUhUOpVFl96Q8ogb6UwthkkkkmL4VFXBWVFqr0ccgkd3YjM8k2yVjs_-j_dUattb0vueR8HA73IPSWkkPGFPk0aFpRyglRr9AeVUoUVHH--sW-iw5SuiHTMEbrUr1Bu6wSNWNE7qHf585DdiZh7S1e2hTiNrvg8VkKeQNxSDh0eDlMVLEavZk13btfYPGlXntIbhzwCmJ0GfDXGOxoJuk6Ob_G30JfnECPLyFvgsVdiPgqgs4D-Dy7noK-vZtV3SfsPP6uU4afOkPcRzvd9AkHT-8CXa-Or45Oi4svJ2dHy4vCcCJy0VEhhbWqo6wlxrQd06IFXvNa1rWignMhqQFSV1YIo6QsrYLSmpZ2siutZgv0-dF3O7YDWDMFi7pvttENOt41QbvmX8W7TbMOt42iNa2nGy7QhyeDGH6MkHIzuGSg77WHMKamFLIStGKCT-j7_9CbMMbpmA8UZ5LLaqY-PlImhpQidM9hKGnmwpu_hU_wu5fxn9E_9bJ7xauohw</recordid><startdate>20220605</startdate><enddate>20220605</enddate><creator>Irfan, Muhammad</creator><creator>Zaheer, Fareeda</creator><creator>Hussain, Humaira</creator><creator>Naz, Muhammad Yasin</creator><creator>Shukrullah, Shazia</creator><creator>Legutko, Stanislaw</creator><creator>Mahnashi, Mater H</creator><creator>Alsaiari, Mabkhoot A</creator><creator>Ghanim, Abdulnour Ali Jazem</creator><creator>Rahman, Saifur</creator><creator>Alshorman, Omar</creator><creator>Alkahtani, Fahad Salem</creator><creator>Khan, Mohammad K A</creator><creator>Kruszelnicka, Izabela</creator><creator>Ginter-Kramarczyk, Dobrochna</creator><general>MDPI AG</general><general>MDPI</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>7X8</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0002-7143-6085</orcidid><orcidid>https://orcid.org/0000-0002-7262-183X</orcidid><orcidid>https://orcid.org/0000-0003-4400-2553</orcidid><orcidid>https://orcid.org/0000-0001-8973-5035</orcidid><orcidid>https://orcid.org/0000-0002-4366-3256</orcidid><orcidid>https://orcid.org/0000-0002-4020-9402</orcidid><orcidid>https://orcid.org/0000-0003-4161-6875</orcidid></search><sort><creationdate>20220605</creationdate><title>Kinetics and Adsorption Isotherms of Amine-Functionalized Magnesium Ferrite Produced Using Sol-Gel Method for Treatment of Heavy Metals in Wastewater</title><author>Irfan, Muhammad ; Zaheer, Fareeda ; Hussain, Humaira ; Naz, Muhammad Yasin ; Shukrullah, Shazia ; Legutko, Stanislaw ; Mahnashi, Mater H ; Alsaiari, Mabkhoot A ; Ghanim, Abdulnour Ali Jazem ; Rahman, Saifur ; Alshorman, Omar ; Alkahtani, Fahad Salem ; Khan, Mohammad K A ; Kruszelnicka, Izabela ; Ginter-Kramarczyk, Dobrochna</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c406t-f1676dd9f13b0ccbf3a6be484878891644671ce085d66c9772d9e2dcb1f7f2da3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Adsorbents</topic><topic>Adsorption</topic><topic>Aqueous solutions</topic><topic>Atoms & subatomic particles</topic><topic>Bonding strength</topic><topic>Chemical bonds</topic><topic>Chemisorption</topic><topic>Copper</topic><topic>Heavy metals</topic><topic>Isotherms</topic><topic>Kinetics</topic><topic>Magnesium</topic><topic>Magnesium ferrites</topic><topic>Magnetic fields</topic><topic>Metal ions</topic><topic>Metals</topic><topic>Morphology</topic><topic>Nanoparticles</topic><topic>Nitrates</topic><topic>Particle size</topic><topic>Roasting</topic><topic>Sol-gel processes</topic><topic>Spectrum analysis</topic><topic>Surface chemistry</topic><topic>Wastewater</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Irfan, Muhammad</creatorcontrib><creatorcontrib>Zaheer, Fareeda</creatorcontrib><creatorcontrib>Hussain, Humaira</creatorcontrib><creatorcontrib>Naz, Muhammad Yasin</creatorcontrib><creatorcontrib>Shukrullah, Shazia</creatorcontrib><creatorcontrib>Legutko, Stanislaw</creatorcontrib><creatorcontrib>Mahnashi, Mater H</creatorcontrib><creatorcontrib>Alsaiari, Mabkhoot A</creatorcontrib><creatorcontrib>Ghanim, Abdulnour Ali Jazem</creatorcontrib><creatorcontrib>Rahman, Saifur</creatorcontrib><creatorcontrib>Alshorman, Omar</creatorcontrib><creatorcontrib>Alkahtani, Fahad Salem</creatorcontrib><creatorcontrib>Khan, Mohammad K A</creatorcontrib><creatorcontrib>Kruszelnicka, Izabela</creatorcontrib><creatorcontrib>Ginter-Kramarczyk, Dobrochna</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Irfan, Muhammad</au><au>Zaheer, Fareeda</au><au>Hussain, Humaira</au><au>Naz, Muhammad Yasin</au><au>Shukrullah, Shazia</au><au>Legutko, Stanislaw</au><au>Mahnashi, Mater H</au><au>Alsaiari, Mabkhoot A</au><au>Ghanim, Abdulnour Ali Jazem</au><au>Rahman, Saifur</au><au>Alshorman, Omar</au><au>Alkahtani, Fahad Salem</au><au>Khan, Mohammad K A</au><au>Kruszelnicka, Izabela</au><au>Ginter-Kramarczyk, Dobrochna</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Kinetics and Adsorption Isotherms of Amine-Functionalized Magnesium Ferrite Produced Using Sol-Gel Method for Treatment of Heavy Metals in Wastewater</atitle><jtitle>Materials</jtitle><addtitle>Materials (Basel)</addtitle><date>2022-06-05</date><risdate>2022</risdate><volume>15</volume><issue>11</issue><spage>4009</spage><pages>4009-</pages><issn>1996-1944</issn><eissn>1996-1944</eissn><abstract>This study is focused on the kinetics and adsorption isotherms of amine-functionalized magnesium ferrite (MgFe
O
) for treating the heavy metals in wastewater. A sol-gel route was adopted to produce MgFe
O
nanoparticles. The surfaces of the MgFe
O
nanoparticles were functionalized using primary amine (ethanolamine). The surface morphology, phase formation, and functionality of the MgFe
O
nano-adsorbents were studied using the SEM, UV-visible, FTIR, and TGA techniques. The characterized nanoparticles were tested on their ability to adsorb the Pb
, Cu
, and Zn
ions from the wastewater. The kinetic parameters and adsorption isotherms for the adsorption of the metal ions by the amine-functionalized MgFe
O
were obtained using the pseudo-first-order, pseudo-second-order, Langmuir, and Freundlich models. The pseudo-second order and Langmuir models best described the adsorption kinetics and isotherms, implying strong chemisorption via the formation of coordinative bonds between the amine groups and metal ions. The Langmuir equation revealed the highest adsorption capacity of 0.7 mmol/g for the amine-functionalized MgFe
O
nano-adsorbents. The adsorption capacity of the nanoadsorbent also changed with the calcination temperature. The MgFe
O
sample, calcined at 500 °C, removed the most of the Pb
(73%), Cu
(59%), and Zn
(62%) ions from the water.</abstract><cop>Switzerland</cop><pub>MDPI AG</pub><pmid>35683307</pmid><doi>10.3390/ma15114009</doi><orcidid>https://orcid.org/0000-0002-7143-6085</orcidid><orcidid>https://orcid.org/0000-0002-7262-183X</orcidid><orcidid>https://orcid.org/0000-0003-4400-2553</orcidid><orcidid>https://orcid.org/0000-0001-8973-5035</orcidid><orcidid>https://orcid.org/0000-0002-4366-3256</orcidid><orcidid>https://orcid.org/0000-0002-4020-9402</orcidid><orcidid>https://orcid.org/0000-0003-4161-6875</orcidid><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1996-1944 |
| ispartof | Materials, 2022-06, Vol.15 (11), p.4009 |
| issn | 1996-1944 1996-1944 |
| language | eng |
| recordid | cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_9181868 |
| source | PubMed Central Open Access; MDPI - Multidisciplinary Digital Publishing Institute; EZB-FREE-00999 freely available EZB journals; PubMed Central; Free Full-Text Journals in Chemistry |
| subjects | Adsorbents Adsorption Aqueous solutions Atoms & subatomic particles Bonding strength Chemical bonds Chemisorption Copper Heavy metals Isotherms Kinetics Magnesium Magnesium ferrites Magnetic fields Metal ions Metals Morphology Nanoparticles Nitrates Particle size Roasting Sol-gel processes Spectrum analysis Surface chemistry Wastewater |
| title | Kinetics and Adsorption Isotherms of Amine-Functionalized Magnesium Ferrite Produced Using Sol-Gel Method for Treatment of Heavy Metals in Wastewater |
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