Development of a sample preparation procedure for Sr isotope analysis of Portland cements
The 87 Sr/ 86 Sr isotope ratio can, in principle, be used for provenancing of cement. However, while commercial cements consist of multiple components, no detailed investigation into their individual 87 Sr/ 86 Sr isotope ratios or their influence on the integral 87 Sr/ 86 Sr isotope ratio of the res...
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| Veröffentlicht in: | Analytical and bioanalytical chemistry 2022-06, Vol.414 (15), p.4379-4389 |
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| creator | Kazlagić, Anera Russo, Francesco F. Vogl, Jochen Sturm, Patrick Stephan, Dietmar Gluth, Gregor J. G. |
| description | The
87
Sr/
86
Sr isotope ratio can, in principle, be used for provenancing of cement. However, while commercial cements consist of multiple components, no detailed investigation into their individual
87
Sr/
86
Sr isotope ratios or their influence on the integral
87
Sr/
86
Sr isotope ratio of the resulting cement was conducted previously. Therefore, the present study aimed at determining and comparing the conventional
87
Sr/
86
Sr isotope ratios of a diverse set of Portland cements and their corresponding Portland clinkers, the major component of these cements. Two approaches to remove the additives from the cements, i.e. to measure the conventional
87
Sr/
86
Sr isotopic fingerprint of the clinker only, were tested, namely, treatment with a potassium hydroxide/sucrose solution and sieving on a 11-µm sieve. Dissolution in concentrated hydrochloric acid/nitric acid and in diluted nitric acid was employed to determine the
87
Sr/
86
Sr isotope ratios of the cements and the individual clinkers. The aim was to find the most appropriate sample preparation procedure for cement provenancing, and the selection was realised by comparing the
87
Sr/
86
Sr isotope ratios of differently treated cements with those of the corresponding clinkers. None of the methods to separate the clinkers from the cements proved to be satisfactory. However, it was found that the
87
Sr/
86
Sr isotope ratios of clinker and cement generally corresponded, meaning that the latter can be used as a proxy for the clinker
87
Sr/
86
Sr isotope ratio. Finally, the concentrated hydrochloric acid/nitric acid dissolution method was found to be the most suitable sample preparation method for the cements; it is thus recommended for
87
Sr/
86
Sr isotope analyses for cement provenancing.
Graphical abstract |
| doi_str_mv | 10.1007/s00216-021-03821-7 |
| format | Article |
| fullrecord | <record><control><sourceid>gale_pubme</sourceid><recordid>TN_cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_9142479</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><galeid>A705233133</galeid><sourcerecordid>A705233133</sourcerecordid><originalsourceid>FETCH-LOGICAL-c513t-2427bde6e85e27d5836c680c4bf6581f1d0bac36e96989f3d6984651cb0b4a693</originalsourceid><addsrcrecordid>eNp9UUFv1jAMjRCIjcEf4IAqceHSzUmatL0gTRsMpEkgAQdOUZq6H5napiTtpP37uXT72DigSI4Vv_f8HDP2msMxByhPEoDgOqeQg6wolk_YIde8yoVW8HSfF-KAvUjpCoCriuvn7EAqELWuxSH7eY7X2IdpwHHOQpfZLNlh6jGbIk422tmHkfLgsF0iZl2I2beY-RTmMGFmR9vfJJ9W5tcQ596ObeZwFUsv2bPO9glf3d1H7MfHD9_PPuWXXy4-n51e5k5xOeeiEGXTosZKoShbVUntdAWuaDpNbjveQmOd1Eh-q7qTLV2FVtw10BRW1_KIvd90p6UZsHXUO9reTNEPNt6YYL15XBn9L7ML16bmhSjKVeDdnUAMvxdMsxl8ctjTMBiWZIQWAJVQGgj69h_oVVgifcKKKkFBoWRBqOMNtbM9Gj92gfo6Oi0O3oURO0_vp4QXUnIpiSA2goshpYjd3j0Hs67abKs2FMyfVZuSSG8ezr2n3O-WAHIDJCqNO4x_zf5H9hb7ArSA</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2670504534</pqid></control><display><type>article</type><title>Development of a sample preparation procedure for Sr isotope analysis of Portland cements</title><source>SpringerLink Journals - AutoHoldings</source><creator>Kazlagić, Anera ; Russo, Francesco F. ; Vogl, Jochen ; Sturm, Patrick ; Stephan, Dietmar ; Gluth, Gregor J. G.</creator><creatorcontrib>Kazlagić, Anera ; Russo, Francesco F. ; Vogl, Jochen ; Sturm, Patrick ; Stephan, Dietmar ; Gluth, Gregor J. G.</creatorcontrib><description>The
87
Sr/
86
Sr isotope ratio can, in principle, be used for provenancing of cement. However, while commercial cements consist of multiple components, no detailed investigation into their individual
87
Sr/
86
Sr isotope ratios or their influence on the integral
87
Sr/
86
Sr isotope ratio of the resulting cement was conducted previously. Therefore, the present study aimed at determining and comparing the conventional
87
Sr/
86
Sr isotope ratios of a diverse set of Portland cements and their corresponding Portland clinkers, the major component of these cements. Two approaches to remove the additives from the cements, i.e. to measure the conventional
87
Sr/
86
Sr isotopic fingerprint of the clinker only, were tested, namely, treatment with a potassium hydroxide/sucrose solution and sieving on a 11-µm sieve. Dissolution in concentrated hydrochloric acid/nitric acid and in diluted nitric acid was employed to determine the
87
Sr/
86
Sr isotope ratios of the cements and the individual clinkers. The aim was to find the most appropriate sample preparation procedure for cement provenancing, and the selection was realised by comparing the
87
Sr/
86
Sr isotope ratios of differently treated cements with those of the corresponding clinkers. None of the methods to separate the clinkers from the cements proved to be satisfactory. However, it was found that the
87
Sr/
86
Sr isotope ratios of clinker and cement generally corresponded, meaning that the latter can be used as a proxy for the clinker
87
Sr/
86
Sr isotope ratio. Finally, the concentrated hydrochloric acid/nitric acid dissolution method was found to be the most suitable sample preparation method for the cements; it is thus recommended for
87
Sr/
86
Sr isotope analyses for cement provenancing.
Graphical abstract</description><identifier>ISSN: 1618-2642</identifier><identifier>EISSN: 1618-2650</identifier><identifier>DOI: 10.1007/s00216-021-03821-7</identifier><identifier>PMID: 35029692</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Acid dissolution ; Additives ; Analysis ; Analytical Chemistry ; Analytical Methods and Applications in the Materials and Life Sciences ; Biochemistry ; Cement ; Characterization and Evaluation of Materials ; Chemistry ; Chemistry and Materials Science ; Clinker ; Composition ; Dissolution ; Food Science ; Hydrochloric acid ; Isotope analysis ; Isotope ratios ; Isotopes ; Laboratory Medicine ; Methods ; Monitoring/Environmental Analysis ; Nitric acid ; Portland cements ; Potassium hydroxide ; Potassium hydroxides ; Research Paper ; Sample preparation ; Separation (Technology) ; Strontium ; Strontium 87 ; Strontium isotopes ; Sucrose</subject><ispartof>Analytical and bioanalytical chemistry, 2022-06, Vol.414 (15), p.4379-4389</ispartof><rights>The Author(s) 2022</rights><rights>2022. The Author(s).</rights><rights>COPYRIGHT 2022 Springer</rights><rights>The Author(s) 2022. This work is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c513t-2427bde6e85e27d5836c680c4bf6581f1d0bac36e96989f3d6984651cb0b4a693</citedby><cites>FETCH-LOGICAL-c513t-2427bde6e85e27d5836c680c4bf6581f1d0bac36e96989f3d6984651cb0b4a693</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00216-021-03821-7$$EPDF$$P50$$Gspringer$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00216-021-03821-7$$EHTML$$P50$$Gspringer$$Hfree_for_read</linktohtml><link.rule.ids>230,314,780,784,885,27923,27924,41487,42556,51318</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/35029692$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Kazlagić, Anera</creatorcontrib><creatorcontrib>Russo, Francesco F.</creatorcontrib><creatorcontrib>Vogl, Jochen</creatorcontrib><creatorcontrib>Sturm, Patrick</creatorcontrib><creatorcontrib>Stephan, Dietmar</creatorcontrib><creatorcontrib>Gluth, Gregor J. G.</creatorcontrib><title>Development of a sample preparation procedure for Sr isotope analysis of Portland cements</title><title>Analytical and bioanalytical chemistry</title><addtitle>Anal Bioanal Chem</addtitle><addtitle>Anal Bioanal Chem</addtitle><description>The
87
Sr/
86
Sr isotope ratio can, in principle, be used for provenancing of cement. However, while commercial cements consist of multiple components, no detailed investigation into their individual
87
Sr/
86
Sr isotope ratios or their influence on the integral
87
Sr/
86
Sr isotope ratio of the resulting cement was conducted previously. Therefore, the present study aimed at determining and comparing the conventional
87
Sr/
86
Sr isotope ratios of a diverse set of Portland cements and their corresponding Portland clinkers, the major component of these cements. Two approaches to remove the additives from the cements, i.e. to measure the conventional
87
Sr/
86
Sr isotopic fingerprint of the clinker only, were tested, namely, treatment with a potassium hydroxide/sucrose solution and sieving on a 11-µm sieve. Dissolution in concentrated hydrochloric acid/nitric acid and in diluted nitric acid was employed to determine the
87
Sr/
86
Sr isotope ratios of the cements and the individual clinkers. The aim was to find the most appropriate sample preparation procedure for cement provenancing, and the selection was realised by comparing the
87
Sr/
86
Sr isotope ratios of differently treated cements with those of the corresponding clinkers. None of the methods to separate the clinkers from the cements proved to be satisfactory. However, it was found that the
87
Sr/
86
Sr isotope ratios of clinker and cement generally corresponded, meaning that the latter can be used as a proxy for the clinker
87
Sr/
86
Sr isotope ratio. Finally, the concentrated hydrochloric acid/nitric acid dissolution method was found to be the most suitable sample preparation method for the cements; it is thus recommended for
87
Sr/
86
Sr isotope analyses for cement provenancing.
Graphical abstract</description><subject>Acid dissolution</subject><subject>Additives</subject><subject>Analysis</subject><subject>Analytical Chemistry</subject><subject>Analytical Methods and Applications in the Materials and Life Sciences</subject><subject>Biochemistry</subject><subject>Cement</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Clinker</subject><subject>Composition</subject><subject>Dissolution</subject><subject>Food Science</subject><subject>Hydrochloric acid</subject><subject>Isotope analysis</subject><subject>Isotope ratios</subject><subject>Isotopes</subject><subject>Laboratory Medicine</subject><subject>Methods</subject><subject>Monitoring/Environmental Analysis</subject><subject>Nitric acid</subject><subject>Portland cements</subject><subject>Potassium hydroxide</subject><subject>Potassium hydroxides</subject><subject>Research Paper</subject><subject>Sample preparation</subject><subject>Separation (Technology)</subject><subject>Strontium</subject><subject>Strontium 87</subject><subject>Strontium isotopes</subject><subject>Sucrose</subject><issn>1618-2642</issn><issn>1618-2650</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><sourceid>C6C</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNp9UUFv1jAMjRCIjcEf4IAqceHSzUmatL0gTRsMpEkgAQdOUZq6H5napiTtpP37uXT72DigSI4Vv_f8HDP2msMxByhPEoDgOqeQg6wolk_YIde8yoVW8HSfF-KAvUjpCoCriuvn7EAqELWuxSH7eY7X2IdpwHHOQpfZLNlh6jGbIk422tmHkfLgsF0iZl2I2beY-RTmMGFmR9vfJJ9W5tcQ596ObeZwFUsv2bPO9glf3d1H7MfHD9_PPuWXXy4-n51e5k5xOeeiEGXTosZKoShbVUntdAWuaDpNbjveQmOd1Eh-q7qTLV2FVtw10BRW1_KIvd90p6UZsHXUO9reTNEPNt6YYL15XBn9L7ML16bmhSjKVeDdnUAMvxdMsxl8ctjTMBiWZIQWAJVQGgj69h_oVVgifcKKKkFBoWRBqOMNtbM9Gj92gfo6Oi0O3oURO0_vp4QXUnIpiSA2goshpYjd3j0Hs67abKs2FMyfVZuSSG8ezr2n3O-WAHIDJCqNO4x_zf5H9hb7ArSA</recordid><startdate>20220601</startdate><enddate>20220601</enddate><creator>Kazlagić, Anera</creator><creator>Russo, Francesco F.</creator><creator>Vogl, Jochen</creator><creator>Sturm, Patrick</creator><creator>Stephan, Dietmar</creator><creator>Gluth, Gregor J. G.</creator><general>Springer Berlin Heidelberg</general><general>Springer</general><general>Springer Nature B.V</general><scope>C6C</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7QF</scope><scope>7QO</scope><scope>7QQ</scope><scope>7SC</scope><scope>7SE</scope><scope>7SP</scope><scope>7SR</scope><scope>7TA</scope><scope>7TB</scope><scope>7U5</scope><scope>7U7</scope><scope>7X7</scope><scope>7XB</scope><scope>88E</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FH</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AEUYN</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BBNVY</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>C1K</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F28</scope><scope>FR3</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>H8D</scope><scope>H8G</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>JQ2</scope><scope>K9.</scope><scope>KB.</scope><scope>KR7</scope><scope>L7M</scope><scope>LK8</scope><scope>L~C</scope><scope>L~D</scope><scope>M0S</scope><scope>M1P</scope><scope>M7P</scope><scope>P64</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>7X8</scope><scope>5PM</scope></search><sort><creationdate>20220601</creationdate><title>Development of a sample preparation procedure for Sr isotope analysis of Portland cements</title><author>Kazlagić, Anera ; Russo, Francesco F. ; Vogl, Jochen ; Sturm, Patrick ; Stephan, Dietmar ; Gluth, Gregor J. G.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c513t-2427bde6e85e27d5836c680c4bf6581f1d0bac36e96989f3d6984651cb0b4a693</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Acid dissolution</topic><topic>Additives</topic><topic>Analysis</topic><topic>Analytical Chemistry</topic><topic>Analytical Methods and Applications in the Materials and Life Sciences</topic><topic>Biochemistry</topic><topic>Cement</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Clinker</topic><topic>Composition</topic><topic>Dissolution</topic><topic>Food Science</topic><topic>Hydrochloric acid</topic><topic>Isotope analysis</topic><topic>Isotope ratios</topic><topic>Isotopes</topic><topic>Laboratory Medicine</topic><topic>Methods</topic><topic>Monitoring/Environmental Analysis</topic><topic>Nitric acid</topic><topic>Portland cements</topic><topic>Potassium hydroxide</topic><topic>Potassium hydroxides</topic><topic>Research Paper</topic><topic>Sample preparation</topic><topic>Separation (Technology)</topic><topic>Strontium</topic><topic>Strontium 87</topic><topic>Strontium isotopes</topic><topic>Sucrose</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kazlagić, Anera</creatorcontrib><creatorcontrib>Russo, Francesco F.</creatorcontrib><creatorcontrib>Vogl, Jochen</creatorcontrib><creatorcontrib>Sturm, Patrick</creatorcontrib><creatorcontrib>Stephan, Dietmar</creatorcontrib><creatorcontrib>Gluth, Gregor J. 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G.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Development of a sample preparation procedure for Sr isotope analysis of Portland cements</atitle><jtitle>Analytical and bioanalytical chemistry</jtitle><stitle>Anal Bioanal Chem</stitle><addtitle>Anal Bioanal Chem</addtitle><date>2022-06-01</date><risdate>2022</risdate><volume>414</volume><issue>15</issue><spage>4379</spage><epage>4389</epage><pages>4379-4389</pages><issn>1618-2642</issn><eissn>1618-2650</eissn><abstract>The
87
Sr/
86
Sr isotope ratio can, in principle, be used for provenancing of cement. However, while commercial cements consist of multiple components, no detailed investigation into their individual
87
Sr/
86
Sr isotope ratios or their influence on the integral
87
Sr/
86
Sr isotope ratio of the resulting cement was conducted previously. Therefore, the present study aimed at determining and comparing the conventional
87
Sr/
86
Sr isotope ratios of a diverse set of Portland cements and their corresponding Portland clinkers, the major component of these cements. Two approaches to remove the additives from the cements, i.e. to measure the conventional
87
Sr/
86
Sr isotopic fingerprint of the clinker only, were tested, namely, treatment with a potassium hydroxide/sucrose solution and sieving on a 11-µm sieve. Dissolution in concentrated hydrochloric acid/nitric acid and in diluted nitric acid was employed to determine the
87
Sr/
86
Sr isotope ratios of the cements and the individual clinkers. The aim was to find the most appropriate sample preparation procedure for cement provenancing, and the selection was realised by comparing the
87
Sr/
86
Sr isotope ratios of differently treated cements with those of the corresponding clinkers. None of the methods to separate the clinkers from the cements proved to be satisfactory. However, it was found that the
87
Sr/
86
Sr isotope ratios of clinker and cement generally corresponded, meaning that the latter can be used as a proxy for the clinker
87
Sr/
86
Sr isotope ratio. Finally, the concentrated hydrochloric acid/nitric acid dissolution method was found to be the most suitable sample preparation method for the cements; it is thus recommended for
87
Sr/
86
Sr isotope analyses for cement provenancing.
Graphical abstract</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><pmid>35029692</pmid><doi>10.1007/s00216-021-03821-7</doi><tpages>11</tpages><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1618-2642 |
| ispartof | Analytical and bioanalytical chemistry, 2022-06, Vol.414 (15), p.4379-4389 |
| issn | 1618-2642 1618-2650 |
| language | eng |
| recordid | cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_9142479 |
| source | SpringerLink Journals - AutoHoldings |
| subjects | Acid dissolution Additives Analysis Analytical Chemistry Analytical Methods and Applications in the Materials and Life Sciences Biochemistry Cement Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Clinker Composition Dissolution Food Science Hydrochloric acid Isotope analysis Isotope ratios Isotopes Laboratory Medicine Methods Monitoring/Environmental Analysis Nitric acid Portland cements Potassium hydroxide Potassium hydroxides Research Paper Sample preparation Separation (Technology) Strontium Strontium 87 Strontium isotopes Sucrose |
| title | Development of a sample preparation procedure for Sr isotope analysis of Portland cements |
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