Effect of Various Heat Treatments on the Microstructure of 316L Austenitic Stainless Steel Coatings Obtained by Cold Spray
Industries developing cold spray aim at dense and resistant coatings for component repair. However, as-sprayed 316L coatings display non-equilibrium microstructure and brittle fracture behavior. Improving their mechanical properties requires controlling their microstructure; post-spraying heat treat...
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| Veröffentlicht in: | Journal of thermal spray technology 2022, Vol.31 (5), p.1725-1746 |
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| creator | Brassart, Laury-Hann Besson, Jacques Delloro, Francesco Haboussa, David Delabrouille, Frédéric Rolland, Gilles Shen, Yang Gourgues-Lorenzon, Anne-Françoise |
| description | Industries developing cold spray aim at dense and resistant coatings for component repair. However, as-sprayed 316L coatings display non-equilibrium microstructure and brittle fracture behavior. Improving their mechanical properties requires controlling their microstructure; post-spraying heat treatment is a promising approach. The recovery and recrystallization of coatings were little studied, and heat treatments reported in literature mostly used holding for long time in furnaces, not adapted to on-site repairs. This study aimed at gaining insights into recovery and recrystallization mechanisms of 316L coatings, for a broader range of heat treatment kinetics. A study of powders and as-sprayed coatings was conducted to characterize the initial state.
In situ
XRD measurements provided input for heat treatment definition. Microscopy, room temperature XRD and hardness measurements allowed to better understand the microstructural evolutions and to select treatments leading to original microstructures. In this work, a variety of microstructures were produced by adapting heat treatment conditions for a given set of spraying parameters. The recrystallization path of the heterogeneous skin-core microstructure of deposited particles, as well as the interaction between grain growth and precipitation was revealed. A novel, optimized fast heat treatment led to a fully recrystallized, fine-grained coating and significantly reduced hardness. |
| doi_str_mv | 10.1007/s11666-022-01402-3 |
| format | Article |
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In situ
XRD measurements provided input for heat treatment definition. Microscopy, room temperature XRD and hardness measurements allowed to better understand the microstructural evolutions and to select treatments leading to original microstructures. In this work, a variety of microstructures were produced by adapting heat treatment conditions for a given set of spraying parameters. The recrystallization path of the heterogeneous skin-core microstructure of deposited particles, as well as the interaction between grain growth and precipitation was revealed. A novel, optimized fast heat treatment led to a fully recrystallized, fine-grained coating and significantly reduced hardness.</description><identifier>ISSN: 1059-9630</identifier><identifier>EISSN: 1544-1016</identifier><identifier>DOI: 10.1007/s11666-022-01402-3</identifier><identifier>PMID: 37519327</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Analytical Chemistry ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Corrosion and Coatings ; Engineering Sciences ; Machines ; Manufacturing ; Materials ; Materials Science ; Peer Reviewed ; Processes ; Surfaces and Interfaces ; Thin Films ; Tribology</subject><ispartof>Journal of thermal spray technology, 2022, Vol.31 (5), p.1725-1746</ispartof><rights>ASM International 2022</rights><rights>ASM International 2022.</rights><rights>Distributed under a Creative Commons Attribution 4.0 International License</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c480t-263c9af06a17cee7a3ccab195aa3ead7a148eefac38f72746d1749e6a86777d53</citedby><cites>FETCH-LOGICAL-c480t-263c9af06a17cee7a3ccab195aa3ead7a148eefac38f72746d1749e6a86777d53</cites><orcidid>0000-0002-3068-180X ; 0000-0003-1975-2408 ; 0000-0002-5671-9415</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11666-022-01402-3$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11666-022-01402-3$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>230,314,777,781,882,27905,27906,41469,42538,51300</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/37519327$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink><backlink>$$Uhttps://minesparis-psl.hal.science/hal-03701332$$DView record in HAL$$Hfree_for_read</backlink></links><search><creatorcontrib>Brassart, Laury-Hann</creatorcontrib><creatorcontrib>Besson, Jacques</creatorcontrib><creatorcontrib>Delloro, Francesco</creatorcontrib><creatorcontrib>Haboussa, David</creatorcontrib><creatorcontrib>Delabrouille, Frédéric</creatorcontrib><creatorcontrib>Rolland, Gilles</creatorcontrib><creatorcontrib>Shen, Yang</creatorcontrib><creatorcontrib>Gourgues-Lorenzon, Anne-Françoise</creatorcontrib><title>Effect of Various Heat Treatments on the Microstructure of 316L Austenitic Stainless Steel Coatings Obtained by Cold Spray</title><title>Journal of thermal spray technology</title><addtitle>J Therm Spray Tech</addtitle><addtitle>J Therm Spray Technol</addtitle><description>Industries developing cold spray aim at dense and resistant coatings for component repair. However, as-sprayed 316L coatings display non-equilibrium microstructure and brittle fracture behavior. Improving their mechanical properties requires controlling their microstructure; post-spraying heat treatment is a promising approach. The recovery and recrystallization of coatings were little studied, and heat treatments reported in literature mostly used holding for long time in furnaces, not adapted to on-site repairs. This study aimed at gaining insights into recovery and recrystallization mechanisms of 316L coatings, for a broader range of heat treatment kinetics. A study of powders and as-sprayed coatings was conducted to characterize the initial state.
In situ
XRD measurements provided input for heat treatment definition. Microscopy, room temperature XRD and hardness measurements allowed to better understand the microstructural evolutions and to select treatments leading to original microstructures. In this work, a variety of microstructures were produced by adapting heat treatment conditions for a given set of spraying parameters. The recrystallization path of the heterogeneous skin-core microstructure of deposited particles, as well as the interaction between grain growth and precipitation was revealed. A novel, optimized fast heat treatment led to a fully recrystallized, fine-grained coating and significantly reduced hardness.</description><subject>Analytical Chemistry</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Corrosion and Coatings</subject><subject>Engineering Sciences</subject><subject>Machines</subject><subject>Manufacturing</subject><subject>Materials</subject><subject>Materials Science</subject><subject>Peer Reviewed</subject><subject>Processes</subject><subject>Surfaces and Interfaces</subject><subject>Thin Films</subject><subject>Tribology</subject><issn>1059-9630</issn><issn>1544-1016</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><recordid>eNp9UUtv1DAQjhCIlsIf4IB8pIfA-BE7uSCtVoVFWtRDC1dr1pnsusomi-1UWn49Dlsq4MDFHs33GM18RfGawzsOYN5HzrXWJQhRAlcgSvmkOOeVUiUHrp_mGqqmbLSEs-JFjHcAUGlRPS_OpKl4I4U5L35cdR25xMaOfcPgxymyFWFityG_expSZOPA0o7YF-_CGFOYXJoCzQLJ9Zotppho8Mk7dpPQDz3FmCuini1HTH7YRna9mRFq2eaYm33Lbg4Bjy-LZx32kV49_BfF149Xt8tVub7-9Hm5WJdO1ZBKoaVrsAON3Dgig9I53PCmQpSErUGuaqIOnaw7I4zSLTeqIY21Nsa0lbwoPpx8D9NmT63LSwXs7SH4PYajHdHbv5HB7-x2vLcNSCk0zwaXJ4PdP7LVYm3nHkgDPHPvZ-7bh2Fh_D5RTHbvo6O-x4Hyca2olYLa1GqmihN1vmsM1D16c7BzwPYUsM0B218BW5lFb_5c5lHyO9FMkCdCzNCwpWDvxikM-cD_s_0JcceyWg</recordid><startdate>2022</startdate><enddate>2022</enddate><creator>Brassart, Laury-Hann</creator><creator>Besson, Jacques</creator><creator>Delloro, Francesco</creator><creator>Haboussa, David</creator><creator>Delabrouille, Frédéric</creator><creator>Rolland, Gilles</creator><creator>Shen, Yang</creator><creator>Gourgues-Lorenzon, Anne-Françoise</creator><general>Springer US</general><general>ASM International/Springer</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>1XC</scope><scope>VOOES</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0002-3068-180X</orcidid><orcidid>https://orcid.org/0000-0003-1975-2408</orcidid><orcidid>https://orcid.org/0000-0002-5671-9415</orcidid></search><sort><creationdate>2022</creationdate><title>Effect of Various Heat Treatments on the Microstructure of 316L Austenitic Stainless Steel Coatings Obtained by Cold Spray</title><author>Brassart, Laury-Hann ; Besson, Jacques ; Delloro, Francesco ; Haboussa, David ; Delabrouille, Frédéric ; Rolland, Gilles ; Shen, Yang ; Gourgues-Lorenzon, Anne-Françoise</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c480t-263c9af06a17cee7a3ccab195aa3ead7a148eefac38f72746d1749e6a86777d53</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Analytical Chemistry</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Corrosion and Coatings</topic><topic>Engineering Sciences</topic><topic>Machines</topic><topic>Manufacturing</topic><topic>Materials</topic><topic>Materials Science</topic><topic>Peer Reviewed</topic><topic>Processes</topic><topic>Surfaces and Interfaces</topic><topic>Thin Films</topic><topic>Tribology</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Brassart, Laury-Hann</creatorcontrib><creatorcontrib>Besson, Jacques</creatorcontrib><creatorcontrib>Delloro, Francesco</creatorcontrib><creatorcontrib>Haboussa, David</creatorcontrib><creatorcontrib>Delabrouille, Frédéric</creatorcontrib><creatorcontrib>Rolland, Gilles</creatorcontrib><creatorcontrib>Shen, Yang</creatorcontrib><creatorcontrib>Gourgues-Lorenzon, Anne-Françoise</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Hyper Article en Ligne (HAL)</collection><collection>Hyper Article en Ligne (HAL) (Open Access)</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Journal of thermal spray technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Brassart, Laury-Hann</au><au>Besson, Jacques</au><au>Delloro, Francesco</au><au>Haboussa, David</au><au>Delabrouille, Frédéric</au><au>Rolland, Gilles</au><au>Shen, Yang</au><au>Gourgues-Lorenzon, Anne-Françoise</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effect of Various Heat Treatments on the Microstructure of 316L Austenitic Stainless Steel Coatings Obtained by Cold Spray</atitle><jtitle>Journal of thermal spray technology</jtitle><stitle>J Therm Spray Tech</stitle><addtitle>J Therm Spray Technol</addtitle><date>2022</date><risdate>2022</risdate><volume>31</volume><issue>5</issue><spage>1725</spage><epage>1746</epage><pages>1725-1746</pages><issn>1059-9630</issn><eissn>1544-1016</eissn><abstract>Industries developing cold spray aim at dense and resistant coatings for component repair. However, as-sprayed 316L coatings display non-equilibrium microstructure and brittle fracture behavior. Improving their mechanical properties requires controlling their microstructure; post-spraying heat treatment is a promising approach. The recovery and recrystallization of coatings were little studied, and heat treatments reported in literature mostly used holding for long time in furnaces, not adapted to on-site repairs. This study aimed at gaining insights into recovery and recrystallization mechanisms of 316L coatings, for a broader range of heat treatment kinetics. A study of powders and as-sprayed coatings was conducted to characterize the initial state.
In situ
XRD measurements provided input for heat treatment definition. Microscopy, room temperature XRD and hardness measurements allowed to better understand the microstructural evolutions and to select treatments leading to original microstructures. In this work, a variety of microstructures were produced by adapting heat treatment conditions for a given set of spraying parameters. The recrystallization path of the heterogeneous skin-core microstructure of deposited particles, as well as the interaction between grain growth and precipitation was revealed. A novel, optimized fast heat treatment led to a fully recrystallized, fine-grained coating and significantly reduced hardness.</abstract><cop>New York</cop><pub>Springer US</pub><pmid>37519327</pmid><doi>10.1007/s11666-022-01402-3</doi><tpages>22</tpages><orcidid>https://orcid.org/0000-0002-3068-180X</orcidid><orcidid>https://orcid.org/0000-0003-1975-2408</orcidid><orcidid>https://orcid.org/0000-0002-5671-9415</orcidid><oa>free_for_read</oa></addata></record> |
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| subjects | Analytical Chemistry Characterization and Evaluation of Materials Chemistry and Materials Science Corrosion and Coatings Engineering Sciences Machines Manufacturing Materials Materials Science Peer Reviewed Processes Surfaces and Interfaces Thin Films Tribology |
| title | Effect of Various Heat Treatments on the Microstructure of 316L Austenitic Stainless Steel Coatings Obtained by Cold Spray |
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