Surface Structure Analysis of Initial High-Temperature Oxidation of SS441 Stainless Steel
Chromia-forming ferritic stainless steel (FSS) is a highly promising interconnect material for application in solid oxide fuel cells. In this study, initial oxidation of chromium oxides was performed at 500–800 °C to understand the evolution of materials at an early stage. The structural variations...
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| Veröffentlicht in: | Materials 2021-10, Vol.14 (20), p.6136 |
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| creator | Yung, Tung-Yuan Tseng, Hui-Ping Lu, Wen-Feng Tsai, Kun-Chao Shen, Tien Cheng, Hsin-Ming Chen, Jeng-Shiung Chen, Po-Tuan |
| description | Chromia-forming ferritic stainless steel (FSS) is a highly promising interconnect material for application in solid oxide fuel cells. In this study, initial oxidation of chromium oxides was performed at 500–800 °C to understand the evolution of materials at an early stage. The structural variations in oxide scales were analyzed through scanning electron microscopy, energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), X-ray diffractometry (XRD), laser confocal microscopy (LSCM), X-ray photoelectron spectroscopy (XPS), and Raman spectroscopy. Surface electrochemical properties were investigated through electrochemical impedance spectroscopy to understand how the heat treatment temperature affected surface impedance. Treatment temperatures higher than 700 °C facilitate the diffusion of Cr and Mn, thus allowing ferritic spinels to form on the surface and leading to high electrical conductivity. |
| doi_str_mv | 10.3390/ma14206136 |
| format | Article |
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In this study, initial oxidation of chromium oxides was performed at 500–800 °C to understand the evolution of materials at an early stage. The structural variations in oxide scales were analyzed through scanning electron microscopy, energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), X-ray diffractometry (XRD), laser confocal microscopy (LSCM), X-ray photoelectron spectroscopy (XPS), and Raman spectroscopy. Surface electrochemical properties were investigated through electrochemical impedance spectroscopy to understand how the heat treatment temperature affected surface impedance. Treatment temperatures higher than 700 °C facilitate the diffusion of Cr and Mn, thus allowing ferritic spinels to form on the surface and leading to high electrical conductivity.</description><identifier>ISSN: 1996-1944</identifier><identifier>EISSN: 1996-1944</identifier><identifier>DOI: 10.3390/ma14206136</identifier><identifier>PMID: 34683728</identifier><language>eng</language><publisher>Basel: MDPI AG</publisher><subject>Alloys ; Chromium oxides ; Corrosion ; Electrical resistivity ; Electrochemical analysis ; Electrochemical impedance spectroscopy ; Electrodes ; Electrolytes ; Electron microscopy ; Ferritic stainless steel ; Ferritic stainless steels ; Fuel cells ; Heat ; Heat treatment ; High temperature ; Lasers ; Microscopy ; Morphology ; Oxidation ; Photoelectrons ; Raman spectroscopy ; Scale (corrosion) ; Solid oxide fuel cells ; Spectrum analysis ; Structural analysis ; Surface structure ; X ray photoelectron spectroscopy</subject><ispartof>Materials, 2021-10, Vol.14 (20), p.6136</ispartof><rights>2021 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). 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In this study, initial oxidation of chromium oxides was performed at 500–800 °C to understand the evolution of materials at an early stage. The structural variations in oxide scales were analyzed through scanning electron microscopy, energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), X-ray diffractometry (XRD), laser confocal microscopy (LSCM), X-ray photoelectron spectroscopy (XPS), and Raman spectroscopy. Surface electrochemical properties were investigated through electrochemical impedance spectroscopy to understand how the heat treatment temperature affected surface impedance. Treatment temperatures higher than 700 °C facilitate the diffusion of Cr and Mn, thus allowing ferritic spinels to form on the surface and leading to high electrical conductivity.</description><subject>Alloys</subject><subject>Chromium oxides</subject><subject>Corrosion</subject><subject>Electrical resistivity</subject><subject>Electrochemical analysis</subject><subject>Electrochemical impedance spectroscopy</subject><subject>Electrodes</subject><subject>Electrolytes</subject><subject>Electron microscopy</subject><subject>Ferritic stainless steel</subject><subject>Ferritic stainless steels</subject><subject>Fuel cells</subject><subject>Heat</subject><subject>Heat treatment</subject><subject>High temperature</subject><subject>Lasers</subject><subject>Microscopy</subject><subject>Morphology</subject><subject>Oxidation</subject><subject>Photoelectrons</subject><subject>Raman spectroscopy</subject><subject>Scale (corrosion)</subject><subject>Solid oxide fuel cells</subject><subject>Spectrum analysis</subject><subject>Structural analysis</subject><subject>Surface structure</subject><subject>X ray photoelectron spectroscopy</subject><issn>1996-1944</issn><issn>1996-1944</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNpdkctKBDEQRYMoKqMbv6DBjQitSSedTjaCiI8BwcXowlWoSVdmIv0Yk27Rvzc64qs2VVCHS9W9hBwwesK5pqctMFFQybjcILtMa5kzLcTmr3mH7Mf4RFNxzlSht8kOF1LxqlC75HE2BgcWs9kQRjuMAbPzDpq36GPWu2za-cFDk934xTK_x3aFAT6hu1dfw-D77oOazYRgSQF812CMaUJs9siWgybi_lefkIery_uLm_z27np6cX6bW674kDvJqKsrSVXBlADkSlmLNVDnKqQcnUAtAFjJAGVdco2S6UowZxmIcq75hJytdVfjvMXaYjcEaMwq-BbCm-nBm7-bzi_Non8xquQq-ZMEjr4EQv88YhxM66PFpoEO-zGaolSiUlLqKqGH_9CnfgzJrzWVXGDpqQk5XlM29DEGdN_HMGo-QjM_ofF3_-WIHA</recordid><startdate>20211015</startdate><enddate>20211015</enddate><creator>Yung, Tung-Yuan</creator><creator>Tseng, Hui-Ping</creator><creator>Lu, Wen-Feng</creator><creator>Tsai, Kun-Chao</creator><creator>Shen, Tien</creator><creator>Cheng, Hsin-Ming</creator><creator>Chen, Jeng-Shiung</creator><creator>Chen, Po-Tuan</creator><general>MDPI AG</general><general>MDPI</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>7X8</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0001-8837-7846</orcidid><orcidid>https://orcid.org/0000-0002-4332-4721</orcidid></search><sort><creationdate>20211015</creationdate><title>Surface Structure Analysis of Initial High-Temperature Oxidation of SS441 Stainless Steel</title><author>Yung, Tung-Yuan ; 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| subjects | Alloys Chromium oxides Corrosion Electrical resistivity Electrochemical analysis Electrochemical impedance spectroscopy Electrodes Electrolytes Electron microscopy Ferritic stainless steel Ferritic stainless steels Fuel cells Heat Heat treatment High temperature Lasers Microscopy Morphology Oxidation Photoelectrons Raman spectroscopy Scale (corrosion) Solid oxide fuel cells Spectrum analysis Structural analysis Surface structure X ray photoelectron spectroscopy |
| title | Surface Structure Analysis of Initial High-Temperature Oxidation of SS441 Stainless Steel |
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