The Optimization of Alternating Current Electrospun PA 6 Solutions Using a Visual Analysis System
The electrospinning process that produces fine nanofibrous materials have a major disadvantage in the area of productivity. However, alternating current (AC) electrospinning might help to solve the problem via the modification of high voltage signal. The aforementioned productivity aspect can be obs...
Gespeichert in:
Veröffentlicht in: | Polymers 2021-06, Vol.13 (13), p.2098 |
---|---|
Hauptverfasser: | , , , , , , , |
Format: | Artikel |
Sprache: | eng |
Schlagworte: | |
Online-Zugang: | Volltext |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
container_end_page | |
---|---|
container_issue | 13 |
container_start_page | 2098 |
container_title | Polymers |
container_volume | 13 |
creator | Kalous, Tomas Holec, Pavel Erben, Jakub Bilek, Martin Batka, Ondrej Pokorny, Pavel Chaloupek, Jiri Chvojka, Jiri |
description | The electrospinning process that produces fine nanofibrous materials have a major disadvantage in the area of productivity. However, alternating current (AC) electrospinning might help to solve the problem via the modification of high voltage signal. The aforementioned productivity aspect can be observed via a camera system that focuses on the jet creation area and that measures the average lifespan. The paper describes the optimization of polyamide 6 (PA 6) solutions and demonstrates the change in the behavior of the process following the addition of a minor dose of oxoacid. This addition served to convert the previously unspinnable (using AC) solution to a high-quality electrospinning solution. The visual analysis of the AC electrospinning of polymeric solutions using a high-speed camera and a programmable power source was chosen as the method for the evaluation of the quality of the process. The solutions were exposed to high voltage applying two types of AC signal, i.e., the sine wave and the step change. All the recordings presented in the paper contained two sets of data: firstly, camera recordings that showed the visual expression of electrospinning and, secondly, signal recordings that provided information on the data position in the signal function. |
doi_str_mv | 10.3390/polym13132098 |
format | Article |
fullrecord | <record><control><sourceid>proquest_pubme</sourceid><recordid>TN_cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_8271821</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2548405434</sourcerecordid><originalsourceid>FETCH-LOGICAL-c322t-6c60c19564fdd8e9d17714fbb370d491b23e879132d8e64fdb7015c3fb91884b3</originalsourceid><addsrcrecordid>eNpdkUtLxDAQx4Mo7rLu0XvAi5dqXm2Si7AsvkBYwcc1pG2qkbSpSSusn95URdS5zAzzmz_zAOAQoxNKJTrtvdu2mGJKkBQ7YE4QpxmjBdr9Fc_AMsYXlIzlRYH5PphRRhDBks-Bvn82cNMPtrXverC-g76BKzeY0KW0e4LrMQTTDfDcmWoIPvZjB29XsIB33o1TQ4QPcQI1fLRx1A6uOu220UZ4t42DaQ_AXqNdNMtvvwAPF-f366vsZnN5vV7dZBUlZMiKqkAVlnnBmroWRtaYc8yasqQc1UziklAjuEyrpuoElRzhvKJNKbEQrKQLcPal249la-oqDR20U32wrQ5b5bVVfyudfVZP_k0JwrEgOAkcfwsE_zqaOKjWxso4pzvjx6hIzgRDOaMsoUf_0Bc_pou5T0rmlAo2CWZfVJXuFoNpfobBSE3_U3_-Rz8ApAqNUA</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2549533841</pqid></control><display><type>article</type><title>The Optimization of Alternating Current Electrospun PA 6 Solutions Using a Visual Analysis System</title><source>PubMed Central Open Access</source><source>MDPI - Multidisciplinary Digital Publishing Institute</source><source>EZB-FREE-00999 freely available EZB journals</source><source>PubMed Central</source><creator>Kalous, Tomas ; Holec, Pavel ; Erben, Jakub ; Bilek, Martin ; Batka, Ondrej ; Pokorny, Pavel ; Chaloupek, Jiri ; Chvojka, Jiri</creator><creatorcontrib>Kalous, Tomas ; Holec, Pavel ; Erben, Jakub ; Bilek, Martin ; Batka, Ondrej ; Pokorny, Pavel ; Chaloupek, Jiri ; Chvojka, Jiri</creatorcontrib><description>The electrospinning process that produces fine nanofibrous materials have a major disadvantage in the area of productivity. However, alternating current (AC) electrospinning might help to solve the problem via the modification of high voltage signal. The aforementioned productivity aspect can be observed via a camera system that focuses on the jet creation area and that measures the average lifespan. The paper describes the optimization of polyamide 6 (PA 6) solutions and demonstrates the change in the behavior of the process following the addition of a minor dose of oxoacid. This addition served to convert the previously unspinnable (using AC) solution to a high-quality electrospinning solution. The visual analysis of the AC electrospinning of polymeric solutions using a high-speed camera and a programmable power source was chosen as the method for the evaluation of the quality of the process. The solutions were exposed to high voltage applying two types of AC signal, i.e., the sine wave and the step change. All the recordings presented in the paper contained two sets of data: firstly, camera recordings that showed the visual expression of electrospinning and, secondly, signal recordings that provided information on the data position in the signal function.</description><identifier>ISSN: 2073-4360</identifier><identifier>EISSN: 2073-4360</identifier><identifier>DOI: 10.3390/polym13132098</identifier><identifier>PMID: 34202197</identifier><language>eng</language><publisher>Basel: MDPI AG</publisher><subject>Alternating current ; Cameras ; Electrodes ; Electrospinning ; Experiments ; High speed cameras ; High voltages ; Optimization ; Polyamide resins ; Productivity ; Sine waves ; Software ; Sulfur ; Visual signals</subject><ispartof>Polymers, 2021-06, Vol.13 (13), p.2098</ispartof><rights>2021 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>2021 by the authors. 2021</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c322t-6c60c19564fdd8e9d17714fbb370d491b23e879132d8e64fdb7015c3fb91884b3</citedby><cites>FETCH-LOGICAL-c322t-6c60c19564fdd8e9d17714fbb370d491b23e879132d8e64fdb7015c3fb91884b3</cites><orcidid>0000-0002-9368-1161 ; 0000-0001-5421-1063 ; 0000-0001-9856-1604 ; 0000-0002-0258-1238</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC8271821/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC8271821/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,727,780,784,885,27924,27925,53791,53793</link.rule.ids></links><search><creatorcontrib>Kalous, Tomas</creatorcontrib><creatorcontrib>Holec, Pavel</creatorcontrib><creatorcontrib>Erben, Jakub</creatorcontrib><creatorcontrib>Bilek, Martin</creatorcontrib><creatorcontrib>Batka, Ondrej</creatorcontrib><creatorcontrib>Pokorny, Pavel</creatorcontrib><creatorcontrib>Chaloupek, Jiri</creatorcontrib><creatorcontrib>Chvojka, Jiri</creatorcontrib><title>The Optimization of Alternating Current Electrospun PA 6 Solutions Using a Visual Analysis System</title><title>Polymers</title><description>The electrospinning process that produces fine nanofibrous materials have a major disadvantage in the area of productivity. However, alternating current (AC) electrospinning might help to solve the problem via the modification of high voltage signal. The aforementioned productivity aspect can be observed via a camera system that focuses on the jet creation area and that measures the average lifespan. The paper describes the optimization of polyamide 6 (PA 6) solutions and demonstrates the change in the behavior of the process following the addition of a minor dose of oxoacid. This addition served to convert the previously unspinnable (using AC) solution to a high-quality electrospinning solution. The visual analysis of the AC electrospinning of polymeric solutions using a high-speed camera and a programmable power source was chosen as the method for the evaluation of the quality of the process. The solutions were exposed to high voltage applying two types of AC signal, i.e., the sine wave and the step change. All the recordings presented in the paper contained two sets of data: firstly, camera recordings that showed the visual expression of electrospinning and, secondly, signal recordings that provided information on the data position in the signal function.</description><subject>Alternating current</subject><subject>Cameras</subject><subject>Electrodes</subject><subject>Electrospinning</subject><subject>Experiments</subject><subject>High speed cameras</subject><subject>High voltages</subject><subject>Optimization</subject><subject>Polyamide resins</subject><subject>Productivity</subject><subject>Sine waves</subject><subject>Software</subject><subject>Sulfur</subject><subject>Visual signals</subject><issn>2073-4360</issn><issn>2073-4360</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNpdkUtLxDAQx4Mo7rLu0XvAi5dqXm2Si7AsvkBYwcc1pG2qkbSpSSusn95URdS5zAzzmz_zAOAQoxNKJTrtvdu2mGJKkBQ7YE4QpxmjBdr9Fc_AMsYXlIzlRYH5PphRRhDBks-Bvn82cNMPtrXverC-g76BKzeY0KW0e4LrMQTTDfDcmWoIPvZjB29XsIB33o1TQ4QPcQI1fLRx1A6uOu220UZ4t42DaQ_AXqNdNMtvvwAPF-f366vsZnN5vV7dZBUlZMiKqkAVlnnBmroWRtaYc8yasqQc1UziklAjuEyrpuoElRzhvKJNKbEQrKQLcPal249la-oqDR20U32wrQ5b5bVVfyudfVZP_k0JwrEgOAkcfwsE_zqaOKjWxso4pzvjx6hIzgRDOaMsoUf_0Bc_pou5T0rmlAo2CWZfVJXuFoNpfobBSE3_U3_-Rz8ApAqNUA</recordid><startdate>20210625</startdate><enddate>20210625</enddate><creator>Kalous, Tomas</creator><creator>Holec, Pavel</creator><creator>Erben, Jakub</creator><creator>Bilek, Martin</creator><creator>Batka, Ondrej</creator><creator>Pokorny, Pavel</creator><creator>Chaloupek, Jiri</creator><creator>Chvojka, Jiri</creator><general>MDPI AG</general><general>MDPI</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>7X8</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0002-9368-1161</orcidid><orcidid>https://orcid.org/0000-0001-5421-1063</orcidid><orcidid>https://orcid.org/0000-0001-9856-1604</orcidid><orcidid>https://orcid.org/0000-0002-0258-1238</orcidid></search><sort><creationdate>20210625</creationdate><title>The Optimization of Alternating Current Electrospun PA 6 Solutions Using a Visual Analysis System</title><author>Kalous, Tomas ; Holec, Pavel ; Erben, Jakub ; Bilek, Martin ; Batka, Ondrej ; Pokorny, Pavel ; Chaloupek, Jiri ; Chvojka, Jiri</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c322t-6c60c19564fdd8e9d17714fbb370d491b23e879132d8e64fdb7015c3fb91884b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2021</creationdate><topic>Alternating current</topic><topic>Cameras</topic><topic>Electrodes</topic><topic>Electrospinning</topic><topic>Experiments</topic><topic>High speed cameras</topic><topic>High voltages</topic><topic>Optimization</topic><topic>Polyamide resins</topic><topic>Productivity</topic><topic>Sine waves</topic><topic>Software</topic><topic>Sulfur</topic><topic>Visual signals</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kalous, Tomas</creatorcontrib><creatorcontrib>Holec, Pavel</creatorcontrib><creatorcontrib>Erben, Jakub</creatorcontrib><creatorcontrib>Bilek, Martin</creatorcontrib><creatorcontrib>Batka, Ondrej</creatorcontrib><creatorcontrib>Pokorny, Pavel</creatorcontrib><creatorcontrib>Chaloupek, Jiri</creatorcontrib><creatorcontrib>Chvojka, Jiri</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Polymers</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kalous, Tomas</au><au>Holec, Pavel</au><au>Erben, Jakub</au><au>Bilek, Martin</au><au>Batka, Ondrej</au><au>Pokorny, Pavel</au><au>Chaloupek, Jiri</au><au>Chvojka, Jiri</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The Optimization of Alternating Current Electrospun PA 6 Solutions Using a Visual Analysis System</atitle><jtitle>Polymers</jtitle><date>2021-06-25</date><risdate>2021</risdate><volume>13</volume><issue>13</issue><spage>2098</spage><pages>2098-</pages><issn>2073-4360</issn><eissn>2073-4360</eissn><abstract>The electrospinning process that produces fine nanofibrous materials have a major disadvantage in the area of productivity. However, alternating current (AC) electrospinning might help to solve the problem via the modification of high voltage signal. The aforementioned productivity aspect can be observed via a camera system that focuses on the jet creation area and that measures the average lifespan. The paper describes the optimization of polyamide 6 (PA 6) solutions and demonstrates the change in the behavior of the process following the addition of a minor dose of oxoacid. This addition served to convert the previously unspinnable (using AC) solution to a high-quality electrospinning solution. The visual analysis of the AC electrospinning of polymeric solutions using a high-speed camera and a programmable power source was chosen as the method for the evaluation of the quality of the process. The solutions were exposed to high voltage applying two types of AC signal, i.e., the sine wave and the step change. All the recordings presented in the paper contained two sets of data: firstly, camera recordings that showed the visual expression of electrospinning and, secondly, signal recordings that provided information on the data position in the signal function.</abstract><cop>Basel</cop><pub>MDPI AG</pub><pmid>34202197</pmid><doi>10.3390/polym13132098</doi><orcidid>https://orcid.org/0000-0002-9368-1161</orcidid><orcidid>https://orcid.org/0000-0001-5421-1063</orcidid><orcidid>https://orcid.org/0000-0001-9856-1604</orcidid><orcidid>https://orcid.org/0000-0002-0258-1238</orcidid><oa>free_for_read</oa></addata></record> |
fulltext | fulltext |
identifier | ISSN: 2073-4360 |
ispartof | Polymers, 2021-06, Vol.13 (13), p.2098 |
issn | 2073-4360 2073-4360 |
language | eng |
recordid | cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_8271821 |
source | PubMed Central Open Access; MDPI - Multidisciplinary Digital Publishing Institute; EZB-FREE-00999 freely available EZB journals; PubMed Central |
subjects | Alternating current Cameras Electrodes Electrospinning Experiments High speed cameras High voltages Optimization Polyamide resins Productivity Sine waves Software Sulfur Visual signals |
title | The Optimization of Alternating Current Electrospun PA 6 Solutions Using a Visual Analysis System |
url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-22T04%3A43%3A34IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_pubme&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=The%20Optimization%20of%20Alternating%20Current%20Electrospun%20PA%206%20Solutions%20Using%20a%20Visual%20Analysis%20System&rft.jtitle=Polymers&rft.au=Kalous,%20Tomas&rft.date=2021-06-25&rft.volume=13&rft.issue=13&rft.spage=2098&rft.pages=2098-&rft.issn=2073-4360&rft.eissn=2073-4360&rft_id=info:doi/10.3390/polym13132098&rft_dat=%3Cproquest_pubme%3E2548405434%3C/proquest_pubme%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2549533841&rft_id=info:pmid/34202197&rfr_iscdi=true |