Sample chamber for synchrotron based in‐situ X‐ray diffraction experiments under electric fields and temperatures between 100 K and 1250 K
Many scientific questions require X‐ray experiments conducted at varying temperatures, sometimes combined with the application of electric fields. Here, a customized sample chamber developed for beamlines P23 and P24 of PETRA III at DESY to suit these demands is presented. The chamber body consists...
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| Veröffentlicht in: | Journal of synchrotron radiation 2021-01, Vol.28 (1), p.158-168 |
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| container_title | Journal of synchrotron radiation |
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| creator | Nentwich, Melanie Weigel, Tina Richter, Carsten Stöcker, Hartmut Mehner, Erik Jachalke, Sven Novikov, Dmitri V. Zschornak, Matthias Meyer, Dirk C. |
| description | Many scientific questions require X‐ray experiments conducted at varying temperatures, sometimes combined with the application of electric fields. Here, a customized sample chamber developed for beamlines P23 and P24 of PETRA III at DESY to suit these demands is presented. The chamber body consists mainly of standard vacuum parts housing the heater/cooler assembly supplying a temperature range of 100 K to 1250 K and an xyz manipulator holding an electric contact needle for electric measurements at both high voltage and low current. The chamber is closed by an exchangeable hemispherical dome offering all degrees of freedom for single‐crystal experiments within one hemisphere of solid angle. The currently available dome materials (PC, PS, PEEK polymers) differ in their absorption and scattering characteristics, with PEEK providing the best overall performance. The article further describes heating and cooling capabilities, electric characteristics, and plans for future upgrades of the chamber. Examples of applications are discussed.
A custom sample chamber developed for synchrotron X‐ray experiments conducted at varying temperatures combined with the application of electric fields is presented. The chamber features an exchangeable hemispherical dome and an xyz manipulator for electric contacting of the sample. The article describes heating and cooling capabilities, exemplary experiments and plans for future upgrades of the chamber. |
| doi_str_mv | 10.1107/S1600577520014344 |
| format | Article |
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A custom sample chamber developed for synchrotron X‐ray experiments conducted at varying temperatures combined with the application of electric fields is presented. The chamber features an exchangeable hemispherical dome and an xyz manipulator for electric contacting of the sample. The article describes heating and cooling capabilities, exemplary experiments and plans for future upgrades of the chamber.</description><identifier>ISSN: 1600-5775</identifier><identifier>ISSN: 0909-0495</identifier><identifier>EISSN: 1600-5775</identifier><identifier>DOI: 10.1107/S1600577520014344</identifier><identifier>PMID: 33399564</identifier><language>eng</language><publisher>5 Abbey Square, Chester, Cheshire CH1 2HU, England: International Union of Crystallography</publisher><subject>Chambers ; Domes (structural forms) ; Electric contacts ; electric field ; Electric fields ; Experiments ; instrumentation ; Low currents ; Polystyrene resins ; Research Papers ; sample environment ; Synchrotrons ; X‐ray diffraction</subject><ispartof>Journal of synchrotron radiation, 2021-01, Vol.28 (1), p.158-168</ispartof><rights>2021 Melanie Nentwich et al. published by IUCr Journals.</rights><rights>open access.</rights><rights>2021. This article is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>Melanie Nentwich et al. 2021 2021</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c5257-27fbf47fd85944770f01abf3202156a1861265ba0b2f90cc7de081d34e90006d3</citedby><cites>FETCH-LOGICAL-c5257-27fbf47fd85944770f01abf3202156a1861265ba0b2f90cc7de081d34e90006d3</cites><orcidid>0000-0002-7590-5336 ; 0000-0002-4230-215X</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC7842228/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC7842228/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,723,776,780,881,1411,11541,27901,27902,45550,45551,46027,46451,53766,53768</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/33399564$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Nentwich, Melanie</creatorcontrib><creatorcontrib>Weigel, Tina</creatorcontrib><creatorcontrib>Richter, Carsten</creatorcontrib><creatorcontrib>Stöcker, Hartmut</creatorcontrib><creatorcontrib>Mehner, Erik</creatorcontrib><creatorcontrib>Jachalke, Sven</creatorcontrib><creatorcontrib>Novikov, Dmitri V.</creatorcontrib><creatorcontrib>Zschornak, Matthias</creatorcontrib><creatorcontrib>Meyer, Dirk C.</creatorcontrib><title>Sample chamber for synchrotron based in‐situ X‐ray diffraction experiments under electric fields and temperatures between 100 K and 1250 K</title><title>Journal of synchrotron radiation</title><addtitle>J Synchrotron Radiat</addtitle><description>Many scientific questions require X‐ray experiments conducted at varying temperatures, sometimes combined with the application of electric fields. Here, a customized sample chamber developed for beamlines P23 and P24 of PETRA III at DESY to suit these demands is presented. The chamber body consists mainly of standard vacuum parts housing the heater/cooler assembly supplying a temperature range of 100 K to 1250 K and an xyz manipulator holding an electric contact needle for electric measurements at both high voltage and low current. The chamber is closed by an exchangeable hemispherical dome offering all degrees of freedom for single‐crystal experiments within one hemisphere of solid angle. The currently available dome materials (PC, PS, PEEK polymers) differ in their absorption and scattering characteristics, with PEEK providing the best overall performance. The article further describes heating and cooling capabilities, electric characteristics, and plans for future upgrades of the chamber. Examples of applications are discussed.
A custom sample chamber developed for synchrotron X‐ray experiments conducted at varying temperatures combined with the application of electric fields is presented. The chamber features an exchangeable hemispherical dome and an xyz manipulator for electric contacting of the sample. The article describes heating and cooling capabilities, exemplary experiments and plans for future upgrades of the chamber.</description><subject>Chambers</subject><subject>Domes (structural forms)</subject><subject>Electric contacts</subject><subject>electric field</subject><subject>Electric fields</subject><subject>Experiments</subject><subject>instrumentation</subject><subject>Low currents</subject><subject>Polystyrene resins</subject><subject>Research Papers</subject><subject>sample environment</subject><subject>Synchrotrons</subject><subject>X‐ray diffraction</subject><issn>1600-5775</issn><issn>0909-0495</issn><issn>1600-5775</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2021</creationdate><recordtype>article</recordtype><sourceid>24P</sourceid><recordid>eNqFkT1vFDEQhlcIRELgB9AgSzQ0B-Ov9W2DhKLwESJRHCCoLK895hzteg97l3BdGnqUn5hfgu8uRAEKKo9nnnk1r96qekjhKaWgni1oDSCVkgyACi7ErWp_05pterdv1HvVvZxPC1Qrxu9We5zzppG12K8uFqZfdUjs0vQtJuKHRPI62mUaxjRE0pqMjoR4ef4zh3Ein0qRzJq44H0ydgyFwe8rTKHHOGYyRVdUsEM7pmCJD9i5TEx0ZMS-YGacEmbS4niGGAkFuDz_8XYLUCa3n_vVHW-6jA-u3oPqw8uj94evZyfvXr05fHEys5JJNWPKt14o7-ayEUIp8EBN6zkDRmVt6LymrJatgZb5BqxVDmFOHRfYAEDt-EH1fKe7mtoenS33J9PpVbFi0loPJug_JzEs9Zfhm1ZzwRibF4EnVwJp-DphHnUfssWuMxGHKWsmlORNrQQU9PFf6OkwpVjsbSkKFIQqFN1RNg05J_TXx1DQm8T1P4mXnUc3XVxv_I64AM0OOAsdrv-vqI8Xn9nHI0mZ4r8Azxi7Fg</recordid><startdate>202101</startdate><enddate>202101</enddate><creator>Nentwich, Melanie</creator><creator>Weigel, Tina</creator><creator>Richter, Carsten</creator><creator>Stöcker, Hartmut</creator><creator>Mehner, Erik</creator><creator>Jachalke, Sven</creator><creator>Novikov, Dmitri V.</creator><creator>Zschornak, Matthias</creator><creator>Meyer, Dirk C.</creator><general>International Union of Crystallography</general><general>John Wiley & Sons, Inc</general><scope>24P</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>JQ2</scope><scope>L7M</scope><scope>7X8</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0002-7590-5336</orcidid><orcidid>https://orcid.org/0000-0002-4230-215X</orcidid></search><sort><creationdate>202101</creationdate><title>Sample chamber for synchrotron based in‐situ X‐ray diffraction experiments under electric fields and temperatures between 100 K and 1250 K</title><author>Nentwich, Melanie ; 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Here, a customized sample chamber developed for beamlines P23 and P24 of PETRA III at DESY to suit these demands is presented. The chamber body consists mainly of standard vacuum parts housing the heater/cooler assembly supplying a temperature range of 100 K to 1250 K and an xyz manipulator holding an electric contact needle for electric measurements at both high voltage and low current. The chamber is closed by an exchangeable hemispherical dome offering all degrees of freedom for single‐crystal experiments within one hemisphere of solid angle. The currently available dome materials (PC, PS, PEEK polymers) differ in their absorption and scattering characteristics, with PEEK providing the best overall performance. The article further describes heating and cooling capabilities, electric characteristics, and plans for future upgrades of the chamber. Examples of applications are discussed.
A custom sample chamber developed for synchrotron X‐ray experiments conducted at varying temperatures combined with the application of electric fields is presented. The chamber features an exchangeable hemispherical dome and an xyz manipulator for electric contacting of the sample. The article describes heating and cooling capabilities, exemplary experiments and plans for future upgrades of the chamber.</abstract><cop>5 Abbey Square, Chester, Cheshire CH1 2HU, England</cop><pub>International Union of Crystallography</pub><pmid>33399564</pmid><doi>10.1107/S1600577520014344</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0002-7590-5336</orcidid><orcidid>https://orcid.org/0000-0002-4230-215X</orcidid><oa>free_for_read</oa></addata></record> |
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| source | Wiley Online Library Open Access; Wiley Online Library Journals Frontfile Complete; PubMed Central; Free Full-Text Journals in Chemistry |
| subjects | Chambers Domes (structural forms) Electric contacts electric field Electric fields Experiments instrumentation Low currents Polystyrene resins Research Papers sample environment Synchrotrons X‐ray diffraction |
| title | Sample chamber for synchrotron based in‐situ X‐ray diffraction experiments under electric fields and temperatures between 100 K and 1250 K |
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