Microstructure, Texture and Mechanical Properties of Mg-6Sn Alloy Processed by Differential Speed Rolling
The effect of shear deformation introduced by differential speed rolling (DSR) on the microstructure, texture and mechanical properties of Mg-6Sn alloy was investigated. Mg-6Sn sheets were obtained by DSR at speed ratio between upper and lower rolls of R = 1, 1.25, 2 and 3 (R = 1 refers to symmetric...
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description | The effect of shear deformation introduced by differential speed rolling (DSR) on the microstructure, texture and mechanical properties of Mg-6Sn alloy was investigated. Mg-6Sn sheets were obtained by DSR at speed ratio between upper and lower rolls of R = 1, 1.25, 2 and 3 (R = 1 refers to symmetric rolling). The microstructural and textural changes were investigated by electron backscattered diffraction (EBSD) and XRD, while the mechanical performance was evaluated based on tensile tests and calculated Lankford parameters. DSR resulted in the pronounced grain refinement of Mg-6Sn sheets and spreading of basal texture as compared to conventionally rolled one. The average grain size and basal texture intensity gradually decreased with increasing speed ratio. The basal poles splitting to transverse direction (TD) or rolling direction (RD) was observed for all Mg-6Sn sheets. For the as-rolled sheets, YS and UTS increased with increasing speed ratio, but a significant anisotropy of strength and ductility between RD and TD has been observed. After annealing at 300 °C, Mg-6Sn sheets became more homogeneous, and the elongation to failure was increased with higher speed ratios. Moreover, the annealed Mg-6Sn sheets were characterized by a very low normal anisotropy (0.91-1.16), which is normally not achieved for the most common Mg-Al-Zn alloys. |
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Mg-6Sn sheets were obtained by DSR at speed ratio between upper and lower rolls of R = 1, 1.25, 2 and 3 (R = 1 refers to symmetric rolling). The microstructural and textural changes were investigated by electron backscattered diffraction (EBSD) and XRD, while the mechanical performance was evaluated based on tensile tests and calculated Lankford parameters. DSR resulted in the pronounced grain refinement of Mg-6Sn sheets and spreading of basal texture as compared to conventionally rolled one. The average grain size and basal texture intensity gradually decreased with increasing speed ratio. The basal poles splitting to transverse direction (TD) or rolling direction (RD) was observed for all Mg-6Sn sheets. For the as-rolled sheets, YS and UTS increased with increasing speed ratio, but a significant anisotropy of strength and ductility between RD and TD has been observed. After annealing at 300 °C, Mg-6Sn sheets became more homogeneous, and the elongation to failure was increased with higher speed ratios. Moreover, the annealed Mg-6Sn sheets were characterized by a very low normal anisotropy (0.91-1.16), which is normally not achieved for the most common Mg-Al-Zn alloys.</description><identifier>ISSN: 1996-1944</identifier><identifier>EISSN: 1996-1944</identifier><identifier>DOI: 10.3390/ma14010083</identifier><identifier>PMID: 33375316</identifier><language>eng</language><publisher>Switzerland: MDPI AG</publisher><subject>Alloys ; Aluminum base alloys ; Anisotropy ; Annealing ; Asymmetry ; Deformation effects ; Ductility ; Electron backscatter diffraction ; Elongation ; Grain boundaries ; Grain refinement ; Grain size ; Magnesium ; Mechanical properties ; Microstructure ; Rolling direction ; Shear deformation ; Shear strain ; Shear strength ; Sheets ; Strain hardening ; Tensile tests ; Texture ; Zinc</subject><ispartof>Materials, 2020-12, Vol.14 (1), p.83</ispartof><rights>2021. This work is licensed under http://creativecommons.org/licenses/by/3.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>2020 by the authors. 2020</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c406t-5dac7156f45ed41b329e775bcd1a422fd1940c201e5c926828bdf63344d6c0833</citedby><cites>FETCH-LOGICAL-c406t-5dac7156f45ed41b329e775bcd1a422fd1940c201e5c926828bdf63344d6c0833</cites><orcidid>0000-0003-3090-0619 ; 0000-0003-3664-8741 ; 0000-0002-1209-0256</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC7794780/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC7794780/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,724,777,781,882,27905,27906,53772,53774</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/33375316$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Majchrowicz, Kamil</creatorcontrib><creatorcontrib>Jóźwik, Paweł</creatorcontrib><creatorcontrib>Chromiński, Witold</creatorcontrib><creatorcontrib>Adamczyk-Cieślak, Bogusława</creatorcontrib><creatorcontrib>Pakieła, Zbigniew</creatorcontrib><title>Microstructure, Texture and Mechanical Properties of Mg-6Sn Alloy Processed by Differential Speed Rolling</title><title>Materials</title><addtitle>Materials (Basel)</addtitle><description>The effect of shear deformation introduced by differential speed rolling (DSR) on the microstructure, texture and mechanical properties of Mg-6Sn alloy was investigated. Mg-6Sn sheets were obtained by DSR at speed ratio between upper and lower rolls of R = 1, 1.25, 2 and 3 (R = 1 refers to symmetric rolling). The microstructural and textural changes were investigated by electron backscattered diffraction (EBSD) and XRD, while the mechanical performance was evaluated based on tensile tests and calculated Lankford parameters. DSR resulted in the pronounced grain refinement of Mg-6Sn sheets and spreading of basal texture as compared to conventionally rolled one. The average grain size and basal texture intensity gradually decreased with increasing speed ratio. The basal poles splitting to transverse direction (TD) or rolling direction (RD) was observed for all Mg-6Sn sheets. For the as-rolled sheets, YS and UTS increased with increasing speed ratio, but a significant anisotropy of strength and ductility between RD and TD has been observed. After annealing at 300 °C, Mg-6Sn sheets became more homogeneous, and the elongation to failure was increased with higher speed ratios. Moreover, the annealed Mg-6Sn sheets were characterized by a very low normal anisotropy (0.91-1.16), which is normally not achieved for the most common Mg-Al-Zn alloys.</description><subject>Alloys</subject><subject>Aluminum base alloys</subject><subject>Anisotropy</subject><subject>Annealing</subject><subject>Asymmetry</subject><subject>Deformation effects</subject><subject>Ductility</subject><subject>Electron backscatter diffraction</subject><subject>Elongation</subject><subject>Grain boundaries</subject><subject>Grain refinement</subject><subject>Grain size</subject><subject>Magnesium</subject><subject>Mechanical properties</subject><subject>Microstructure</subject><subject>Rolling direction</subject><subject>Shear deformation</subject><subject>Shear strain</subject><subject>Shear strength</subject><subject>Sheets</subject><subject>Strain hardening</subject><subject>Tensile tests</subject><subject>Texture</subject><subject>Zinc</subject><issn>1996-1944</issn><issn>1996-1944</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNpdkVFPHCEUhUmjqUb3pT-gIemLaToKAzMML002aquJmzZqnwkDd1YMO2xhxrj_vkzUrcoLN9yPk3PvQegTJceMSXKy0pQTSkjDPqB9KmVdUMn5zqt6D81Suif5MEabUn5Ee4wxUTFa7yO3cCaGNMTRDGOEb_gWHqcC697iBZg73TujPf4dwxri4CDh0OHFsqhvejz3PmymloGUwOJ2g89c10GEfnD5080a8ut18N71y0O022mfYPZ8H6A_P85vTy-Kq18_L0_nV4XhpB6KymojaFV3vALLactKCUJUrbFU87LsbB6JmJJQqIws66ZsWtvVjHFua5O3wA7Q9yfd9diuwJrsJWqv1tGtdNyooJ162-ndnVqGByWE5KIhWeDoWSCGvyOkQa1cMuC97iGMSZVcsEbKSvCMfnmH3ocx9nm8ieJMNJRPjr4-UdOmU4Rua4YSNYWo_oeY4c-v7W_Rl8jYP2FKlz8</recordid><startdate>20201226</startdate><enddate>20201226</enddate><creator>Majchrowicz, Kamil</creator><creator>Jóźwik, Paweł</creator><creator>Chromiński, Witold</creator><creator>Adamczyk-Cieślak, Bogusława</creator><creator>Pakieła, Zbigniew</creator><general>MDPI AG</general><general>MDPI</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>7X8</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0003-3090-0619</orcidid><orcidid>https://orcid.org/0000-0003-3664-8741</orcidid><orcidid>https://orcid.org/0000-0002-1209-0256</orcidid></search><sort><creationdate>20201226</creationdate><title>Microstructure, Texture and Mechanical Properties of Mg-6Sn Alloy Processed by Differential Speed Rolling</title><author>Majchrowicz, Kamil ; Jóźwik, Paweł ; Chromiński, Witold ; Adamczyk-Cieślak, Bogusława ; Pakieła, Zbigniew</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c406t-5dac7156f45ed41b329e775bcd1a422fd1940c201e5c926828bdf63344d6c0833</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Alloys</topic><topic>Aluminum base alloys</topic><topic>Anisotropy</topic><topic>Annealing</topic><topic>Asymmetry</topic><topic>Deformation effects</topic><topic>Ductility</topic><topic>Electron backscatter diffraction</topic><topic>Elongation</topic><topic>Grain boundaries</topic><topic>Grain refinement</topic><topic>Grain size</topic><topic>Magnesium</topic><topic>Mechanical properties</topic><topic>Microstructure</topic><topic>Rolling direction</topic><topic>Shear deformation</topic><topic>Shear strain</topic><topic>Shear strength</topic><topic>Sheets</topic><topic>Strain hardening</topic><topic>Tensile tests</topic><topic>Texture</topic><topic>Zinc</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Majchrowicz, Kamil</creatorcontrib><creatorcontrib>Jóźwik, Paweł</creatorcontrib><creatorcontrib>Chromiński, Witold</creatorcontrib><creatorcontrib>Adamczyk-Cieślak, Bogusława</creatorcontrib><creatorcontrib>Pakieła, Zbigniew</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Majchrowicz, Kamil</au><au>Jóźwik, Paweł</au><au>Chromiński, Witold</au><au>Adamczyk-Cieślak, Bogusława</au><au>Pakieła, Zbigniew</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Microstructure, Texture and Mechanical Properties of Mg-6Sn Alloy Processed by Differential Speed Rolling</atitle><jtitle>Materials</jtitle><addtitle>Materials (Basel)</addtitle><date>2020-12-26</date><risdate>2020</risdate><volume>14</volume><issue>1</issue><spage>83</spage><pages>83-</pages><issn>1996-1944</issn><eissn>1996-1944</eissn><abstract>The effect of shear deformation introduced by differential speed rolling (DSR) on the microstructure, texture and mechanical properties of Mg-6Sn alloy was investigated. Mg-6Sn sheets were obtained by DSR at speed ratio between upper and lower rolls of R = 1, 1.25, 2 and 3 (R = 1 refers to symmetric rolling). The microstructural and textural changes were investigated by electron backscattered diffraction (EBSD) and XRD, while the mechanical performance was evaluated based on tensile tests and calculated Lankford parameters. DSR resulted in the pronounced grain refinement of Mg-6Sn sheets and spreading of basal texture as compared to conventionally rolled one. The average grain size and basal texture intensity gradually decreased with increasing speed ratio. The basal poles splitting to transverse direction (TD) or rolling direction (RD) was observed for all Mg-6Sn sheets. For the as-rolled sheets, YS and UTS increased with increasing speed ratio, but a significant anisotropy of strength and ductility between RD and TD has been observed. After annealing at 300 °C, Mg-6Sn sheets became more homogeneous, and the elongation to failure was increased with higher speed ratios. Moreover, the annealed Mg-6Sn sheets were characterized by a very low normal anisotropy (0.91-1.16), which is normally not achieved for the most common Mg-Al-Zn alloys.</abstract><cop>Switzerland</cop><pub>MDPI AG</pub><pmid>33375316</pmid><doi>10.3390/ma14010083</doi><orcidid>https://orcid.org/0000-0003-3090-0619</orcidid><orcidid>https://orcid.org/0000-0003-3664-8741</orcidid><orcidid>https://orcid.org/0000-0002-1209-0256</orcidid><oa>free_for_read</oa></addata></record> |
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subjects | Alloys Aluminum base alloys Anisotropy Annealing Asymmetry Deformation effects Ductility Electron backscatter diffraction Elongation Grain boundaries Grain refinement Grain size Magnesium Mechanical properties Microstructure Rolling direction Shear deformation Shear strain Shear strength Sheets Strain hardening Tensile tests Texture Zinc |
title | Microstructure, Texture and Mechanical Properties of Mg-6Sn Alloy Processed by Differential Speed Rolling |
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