Synthesis of bio-oil from waste Trichosanthes cucumerina seeds: a substitute for conventional fuel
The present study explores the methodology for the synthesis of bio-oil from waste trichosanthes cucumerina seeds by the solvent extraction method. It investigates the yield percentage, concentration of free fatty acids and acid contents in the extracted bio-oil. Effects of size of the crushed seeds...
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| Veröffentlicht in: | Scientific reports 2020-10, Vol.10 (1), p.17815-12, Article 17815 |
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| creator | Manimaran, Rajayokkiam Murugu Mohan Kumar, Kandasamy Sathiya Narayanan, Nagarajan |
| description | The present study explores the methodology for the synthesis of bio-oil from waste trichosanthes cucumerina seeds by the solvent extraction method. It investigates the yield percentage, concentration of free fatty acids and acid contents in the extracted bio-oil. Effects of size of the crushed seeds, moisture content, extraction time, solvent to seed ratio and extraction temperatures were examined. The non-polar hexane solvent resulted in a higher percentage of oil yield (28.4 ± 0.4%) for the crushed seed size of 0.21 mm, 6% moisture content, 270 min extraction time, 68 °C temperature and 6:1(ml/g) of solvent to seed ratio. The synthesized bio-oil was characterized using Fourier Transform Infra-Red spectrum and Gas Chromatography–Mass Spectroscopy analysis. The properties of the bio-oil and biodiesel were assessed according to the American Society for Testing and Materials and the Association of Official Analytical Chemists standards. The obtained methyl-ester by trans-esterification process results in the fuel properties closer to the conventional fuel. Thus, Trichosanthes cucumerina bio-diesel can be used as a potential substitute. |
| doi_str_mv | 10.1038/s41598-020-74130-9 |
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It investigates the yield percentage, concentration of free fatty acids and acid contents in the extracted bio-oil. Effects of size of the crushed seeds, moisture content, extraction time, solvent to seed ratio and extraction temperatures were examined. The non-polar hexane solvent resulted in a higher percentage of oil yield (28.4 ± 0.4%) for the crushed seed size of 0.21 mm, 6% moisture content, 270 min extraction time, 68 °C temperature and 6:1(ml/g) of solvent to seed ratio. The synthesized bio-oil was characterized using Fourier Transform Infra-Red spectrum and Gas Chromatography–Mass Spectroscopy analysis. The properties of the bio-oil and biodiesel were assessed according to the American Society for Testing and Materials and the Association of Official Analytical Chemists standards. The obtained methyl-ester by trans-esterification process results in the fuel properties closer to the conventional fuel. 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Murugu Mohan Kumar, Kandasamy ; Sathiya Narayanan, Nagarajan</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c549t-3aebe84dfc926141d0e1d740024f0f8cff9cd492a965db887ca9ddd40940d3f73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>639/166/988</topic><topic>639/4077/909</topic><topic>639/4077/909/4053/906/4052</topic><topic>Biofuels</topic><topic>Catalysis</topic><topic>Esterification</topic><topic>Gas Chromatography-Mass Spectrometry</topic><topic>Gasoline</topic><topic>Humanities and Social Sciences</topic><topic>multidisciplinary</topic><topic>Multidisciplinary Sciences</topic><topic>Plant Oils - chemical synthesis</topic><topic>Polyphenols - chemical synthesis</topic><topic>Renewable Energy</topic><topic>Science</topic><topic>Science & Technology</topic><topic>Science & Technology - Other Topics</topic><topic>Science (multidisciplinary)</topic><topic>Seeds</topic><topic>Spectroscopy, Fourier Transform Infrared</topic><topic>Trichosanthes - physiology</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Manimaran, Rajayokkiam</creatorcontrib><creatorcontrib>Murugu Mohan Kumar, Kandasamy</creatorcontrib><creatorcontrib>Sathiya Narayanan, Nagarajan</creatorcontrib><collection>Springer Nature OA Free Journals</collection><collection>Web of Science - Science Citation Index Expanded - 2020</collection><collection>Web of Science Core Collection</collection><collection>Science Citation Index Expanded</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>PubMed Central (Full Participant titles)</collection><collection>DOAJ Directory of Open Access Journals</collection><jtitle>Scientific reports</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Manimaran, Rajayokkiam</au><au>Murugu Mohan Kumar, Kandasamy</au><au>Sathiya Narayanan, Nagarajan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of bio-oil from waste Trichosanthes cucumerina seeds: a substitute for conventional fuel</atitle><jtitle>Scientific reports</jtitle><stitle>Sci Rep</stitle><stitle>SCI REP-UK</stitle><addtitle>Sci Rep</addtitle><date>2020-10-20</date><risdate>2020</risdate><volume>10</volume><issue>1</issue><spage>17815</spage><epage>12</epage><pages>17815-12</pages><artnum>17815</artnum><issn>2045-2322</issn><eissn>2045-2322</eissn><abstract>The present study explores the methodology for the synthesis of bio-oil from waste trichosanthes cucumerina seeds by the solvent extraction method. It investigates the yield percentage, concentration of free fatty acids and acid contents in the extracted bio-oil. Effects of size of the crushed seeds, moisture content, extraction time, solvent to seed ratio and extraction temperatures were examined. The non-polar hexane solvent resulted in a higher percentage of oil yield (28.4 ± 0.4%) for the crushed seed size of 0.21 mm, 6% moisture content, 270 min extraction time, 68 °C temperature and 6:1(ml/g) of solvent to seed ratio. The synthesized bio-oil was characterized using Fourier Transform Infra-Red spectrum and Gas Chromatography–Mass Spectroscopy analysis. The properties of the bio-oil and biodiesel were assessed according to the American Society for Testing and Materials and the Association of Official Analytical Chemists standards. The obtained methyl-ester by trans-esterification process results in the fuel properties closer to the conventional fuel. 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| subjects | 639/166/988 639/4077/909 639/4077/909/4053/906/4052 Biofuels Catalysis Esterification Gas Chromatography-Mass Spectrometry Gasoline Humanities and Social Sciences multidisciplinary Multidisciplinary Sciences Plant Oils - chemical synthesis Polyphenols - chemical synthesis Renewable Energy Science Science & Technology Science & Technology - Other Topics Science (multidisciplinary) Seeds Spectroscopy, Fourier Transform Infrared Trichosanthes - physiology |
| title | Synthesis of bio-oil from waste Trichosanthes cucumerina seeds: a substitute for conventional fuel |
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