Carbon Nanoparticles' Impact on Processability and Physical Properties of Epoxy Resins-A Comprehensive Study Covering Rheological, Electrical, Thermo-Mechanical, and Fracture Properties (Mode I and II)
A trade-off between enhancement of physical properties of the final part and the processability during manufacturing always exists for the application of nanocarbon materials in thermoset-based composites. For different epoxy resins, this study elaborates the impact of nanocarbon particle type, func...
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| Veröffentlicht in: | Polymers 2019-02, Vol.11 (2), p.231 |
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| creator | Meeuw, Hauke Körbelin, Johann Wisniewski, Valea Kim Nia, Ali Shaygan Vázquez, Adrián Romaní Lohe, Martin Rudolf Feng, Xinliang Fiedler, Bodo |
| description | A trade-off between enhancement of physical properties of the final part and the processability during manufacturing always exists for the application of nanocarbon materials in thermoset-based composites. For different epoxy resins, this study elaborates the impact of nanocarbon particle type, functionalization, and filler loading on the resulting properties, i.e., rheological, electrical, thermo-mechanical, as well as the fracture toughness in mode I and mode II loading. Therefore, a comprehensive set of carbon nanoparticles, consisting of carbon black (CB), single-walled carbon nanotubes (SWCNT), multi-walled carbon nanotubes (MWCNT), few layer graphene (FLG), and electrochemically expanded graphite (ExG), in purified or functionalized configuration was introduced in various epoxy resins, with different molecular weight distributions. A novel technique to introduce sharp cracks into single-edge notched bending (SENB) fracture toughness specimens led to true values. SWCNT show highest potential for increasing electrical properties without an increase in viscosity. Functionalized MWCNT and planar particles significantly increase the fracture toughness in mode I by a factor of two. |
| doi_str_mv | 10.3390/polym11020231 |
| format | Article |
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For different epoxy resins, this study elaborates the impact of nanocarbon particle type, functionalization, and filler loading on the resulting properties, i.e., rheological, electrical, thermo-mechanical, as well as the fracture toughness in mode I and mode II loading. Therefore, a comprehensive set of carbon nanoparticles, consisting of carbon black (CB), single-walled carbon nanotubes (SWCNT), multi-walled carbon nanotubes (MWCNT), few layer graphene (FLG), and electrochemically expanded graphite (ExG), in purified or functionalized configuration was introduced in various epoxy resins, with different molecular weight distributions. A novel technique to introduce sharp cracks into single-edge notched bending (SENB) fracture toughness specimens led to true values. SWCNT show highest potential for increasing electrical properties without an increase in viscosity. Functionalized MWCNT and planar particles significantly increase the fracture toughness in mode I by a factor of two.</description><identifier>ISSN: 2073-4360</identifier><identifier>EISSN: 2073-4360</identifier><identifier>DOI: 10.3390/polym11020231</identifier><identifier>PMID: 30960215</identifier><language>eng</language><publisher>Switzerland: MDPI AG</publisher><subject>Carbon black ; Curing ; Electrical properties ; Energy industry ; Epoxy resins ; Fracture toughness ; Graphene ; Molecular weight distribution ; Multi wall carbon nanotubes ; Nanocomposites ; Nanoparticles ; Nitrogen ; Physical properties ; Polymer matrix composites ; Rheological properties ; Rheology ; Scanning electron microscopy ; Single wall carbon nanotubes ; Thermomechanical properties ; Thermosetting resins ; Viscosity</subject><ispartof>Polymers, 2019-02, Vol.11 (2), p.231</ispartof><rights>2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/). 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For different epoxy resins, this study elaborates the impact of nanocarbon particle type, functionalization, and filler loading on the resulting properties, i.e., rheological, electrical, thermo-mechanical, as well as the fracture toughness in mode I and mode II loading. Therefore, a comprehensive set of carbon nanoparticles, consisting of carbon black (CB), single-walled carbon nanotubes (SWCNT), multi-walled carbon nanotubes (MWCNT), few layer graphene (FLG), and electrochemically expanded graphite (ExG), in purified or functionalized configuration was introduced in various epoxy resins, with different molecular weight distributions. A novel technique to introduce sharp cracks into single-edge notched bending (SENB) fracture toughness specimens led to true values. SWCNT show highest potential for increasing electrical properties without an increase in viscosity. Functionalized MWCNT and planar particles significantly increase the fracture toughness in mode I by a factor of two.</abstract><cop>Switzerland</cop><pub>MDPI AG</pub><pmid>30960215</pmid><doi>10.3390/polym11020231</doi><orcidid>https://orcid.org/0000-0002-6106-6164</orcidid><orcidid>https://orcid.org/0000-0002-1546-0398</orcidid><orcidid>https://orcid.org/0000-0002-7031-3577</orcidid><orcidid>https://orcid.org/0000-0002-2734-1353</orcidid><orcidid>https://orcid.org/0000-0003-3885-2703</orcidid><orcidid>https://orcid.org/0000-0001-5458-779X</orcidid><oa>free_for_read</oa></addata></record> |
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| subjects | Carbon black Curing Electrical properties Energy industry Epoxy resins Fracture toughness Graphene Molecular weight distribution Multi wall carbon nanotubes Nanocomposites Nanoparticles Nitrogen Physical properties Polymer matrix composites Rheological properties Rheology Scanning electron microscopy Single wall carbon nanotubes Thermomechanical properties Thermosetting resins Viscosity |
| title | Carbon Nanoparticles' Impact on Processability and Physical Properties of Epoxy Resins-A Comprehensive Study Covering Rheological, Electrical, Thermo-Mechanical, and Fracture Properties (Mode I and II) |
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