Effect of Laccase-Mediated Biopolymer Grafting on Kraft Pulp Fibers for Enhancing Paper's Mechanical Properties
High-resistance paper was manufactured by laccase-grafting of carboxymethyl cellulose (CMC) and chitosan (CPX) on Kraft pulp fiber. The reaction was mediated in the presence of laccase by one of the following polyphenols in the presence of air: gallic acid (GA), vanillic acid (VA) and catechol (1,2⁻...
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| Veröffentlicht in: | Polymers 2017-11, Vol.9 (11), p.570 |
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| creator | Ballinas-Casarrubias, Lourdes Villanueva-Solís, Luis Espinoza-Hicks, Carlos Camacho-Dávila, Alejandro Castillo, Hilda Amelia Piñón Pérez, Samuel B Villa, Eduardo Duarte Hernández, Miguel De Dios González-Sánchez, Guillermo |
| description | High-resistance paper was manufactured by laccase-grafting of carboxymethyl cellulose (CMC) and chitosan (CPX) on Kraft pulp fiber. The reaction was mediated in the presence of laccase by one of the following polyphenols in the presence of air: gallic acid (GA), vanillic acid (VA) and catechol (1,2⁻DHB). Enzyme was added at constant loading (24 kg ton
), 1% pulp consistency, 0.005% CMC, pH = 6.3 ± 0.5 and 2 mM of mediator. CPX content was assessed at two levels (0% and 0.005%). Treated pulps were analyzed by different mechanical tests (ring crush, mullen, corrugating medium test (CMT) flat crush of corrugating medium test and tension). An improvement in these parameters was obtained by biopolymer coupling and selected mediator. When using GA, three parameters increased more than 40%, while ring crush increased 120%. For the case of VA, properties were enhanced from 74% to 88% when CPX was added. For 1,2⁻DHB, there was not found a statistically significant difference between the results in the presence of CPX. Scanning electron microscopy, confocal microscopy, FTIR and
C NMR were used in all papers in order to evaluate grafting. Hence, it was possible to correlate polymerization with an improvement of paper's mechanical properties. |
| doi_str_mv | 10.3390/polym9110570 |
| format | Article |
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), 1% pulp consistency, 0.005% CMC, pH = 6.3 ± 0.5 and 2 mM of mediator. CPX content was assessed at two levels (0% and 0.005%). Treated pulps were analyzed by different mechanical tests (ring crush, mullen, corrugating medium test (CMT) flat crush of corrugating medium test and tension). An improvement in these parameters was obtained by biopolymer coupling and selected mediator. When using GA, three parameters increased more than 40%, while ring crush increased 120%. For the case of VA, properties were enhanced from 74% to 88% when CPX was added. For 1,2⁻DHB, there was not found a statistically significant difference between the results in the presence of CPX. Scanning electron microscopy, confocal microscopy, FTIR and
C NMR were used in all papers in order to evaluate grafting. Hence, it was possible to correlate polymerization with an improvement of paper's mechanical properties.</description><identifier>ISSN: 2073-4360</identifier><identifier>EISSN: 2073-4360</identifier><identifier>DOI: 10.3390/polym9110570</identifier><identifier>PMID: 30965872</identifier><language>eng</language><publisher>Switzerland: MDPI AG</publisher><subject>Biopolymers ; Carboxymethyl cellulose ; Case crushing ; Catechol ; Cellulose fibers ; Chitosan ; Crush tests ; Electron microscopy ; Gallic acid ; Grafting ; Kraft pulp ; Laccase ; Mechanical properties ; Mechanical tests ; Microscopy ; NMR ; Nuclear magnetic resonance ; Polyphenols</subject><ispartof>Polymers, 2017-11, Vol.9 (11), p.570</ispartof><rights>Copyright MDPI AG 2017</rights><rights>2017 by the authors. 2017</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c412t-ca81de6f365c3a13ba1fce2e725340063167ff54aced6cd773b6c8e851236b6a3</citedby><cites>FETCH-LOGICAL-c412t-ca81de6f365c3a13ba1fce2e725340063167ff54aced6cd773b6c8e851236b6a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC6418782/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC6418782/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,727,780,784,885,27924,27925,53791,53793</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/30965872$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Ballinas-Casarrubias, Lourdes</creatorcontrib><creatorcontrib>Villanueva-Solís, Luis</creatorcontrib><creatorcontrib>Espinoza-Hicks, Carlos</creatorcontrib><creatorcontrib>Camacho-Dávila, Alejandro</creatorcontrib><creatorcontrib>Castillo, Hilda Amelia Piñón</creatorcontrib><creatorcontrib>Pérez, Samuel B</creatorcontrib><creatorcontrib>Villa, Eduardo Duarte</creatorcontrib><creatorcontrib>Hernández, Miguel De Dios</creatorcontrib><creatorcontrib>González-Sánchez, Guillermo</creatorcontrib><title>Effect of Laccase-Mediated Biopolymer Grafting on Kraft Pulp Fibers for Enhancing Paper's Mechanical Properties</title><title>Polymers</title><addtitle>Polymers (Basel)</addtitle><description>High-resistance paper was manufactured by laccase-grafting of carboxymethyl cellulose (CMC) and chitosan (CPX) on Kraft pulp fiber. The reaction was mediated in the presence of laccase by one of the following polyphenols in the presence of air: gallic acid (GA), vanillic acid (VA) and catechol (1,2⁻DHB). Enzyme was added at constant loading (24 kg ton
), 1% pulp consistency, 0.005% CMC, pH = 6.3 ± 0.5 and 2 mM of mediator. CPX content was assessed at two levels (0% and 0.005%). Treated pulps were analyzed by different mechanical tests (ring crush, mullen, corrugating medium test (CMT) flat crush of corrugating medium test and tension). An improvement in these parameters was obtained by biopolymer coupling and selected mediator. When using GA, three parameters increased more than 40%, while ring crush increased 120%. For the case of VA, properties were enhanced from 74% to 88% when CPX was added. For 1,2⁻DHB, there was not found a statistically significant difference between the results in the presence of CPX. Scanning electron microscopy, confocal microscopy, FTIR and
C NMR were used in all papers in order to evaluate grafting. Hence, it was possible to correlate polymerization with an improvement of paper's mechanical properties.</description><subject>Biopolymers</subject><subject>Carboxymethyl cellulose</subject><subject>Case crushing</subject><subject>Catechol</subject><subject>Cellulose fibers</subject><subject>Chitosan</subject><subject>Crush tests</subject><subject>Electron microscopy</subject><subject>Gallic acid</subject><subject>Grafting</subject><subject>Kraft pulp</subject><subject>Laccase</subject><subject>Mechanical properties</subject><subject>Mechanical tests</subject><subject>Microscopy</subject><subject>NMR</subject><subject>Nuclear magnetic resonance</subject><subject>Polyphenols</subject><issn>2073-4360</issn><issn>2073-4360</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNpdkUFP5DAMhSPEChDLjTOKxAEOdDdp2iRzQQI0zK520M4BzpGbOhDUaUrSIvHv6TCABnyxZX96sv0IOeTslxAT9rsLzctywjkrFdsiezlTIiuEZNsb9S45SOmRjVGUUnK1Q3YFm8hSq3yPhKlzaHsaHJ2DtZAwu8HaQ481vfThTR8jnUVwvW_vaWjpv1VNF0PT0WtfYUzUhUin7QO0doUsoMN4kugN2rHlLTR0EcPY6z2mn-SHgybhwXveJ3fX09urP9n8_-zv1cU8swXP-8yC5jVKJ2RpBXBRAXcWc1R5KQrGpOBSOVcWYLGWtlZKVNJq1CXPhawkiH1yvtbthmqJtcW2j9CYLvolxBcTwJuvk9Y_mPvwbGTBtdL5KHD6LhDD04CpN0ufLDYNtBiGZPLxv1xxLtSIHn9DH8MQ2_E8wydKaS21WlFna8rGkFJE97kMZ2Zlptk0c8SPNg_4hD-sE6_ma5wd</recordid><startdate>20171102</startdate><enddate>20171102</enddate><creator>Ballinas-Casarrubias, Lourdes</creator><creator>Villanueva-Solís, Luis</creator><creator>Espinoza-Hicks, Carlos</creator><creator>Camacho-Dávila, Alejandro</creator><creator>Castillo, Hilda Amelia Piñón</creator><creator>Pérez, Samuel B</creator><creator>Villa, Eduardo Duarte</creator><creator>Hernández, Miguel De Dios</creator><creator>González-Sánchez, Guillermo</creator><general>MDPI AG</general><general>MDPI</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>7X8</scope><scope>5PM</scope></search><sort><creationdate>20171102</creationdate><title>Effect of Laccase-Mediated Biopolymer Grafting on Kraft Pulp Fibers for Enhancing Paper's Mechanical Properties</title><author>Ballinas-Casarrubias, Lourdes ; Villanueva-Solís, Luis ; Espinoza-Hicks, Carlos ; Camacho-Dávila, Alejandro ; Castillo, Hilda Amelia Piñón ; Pérez, Samuel B ; Villa, Eduardo Duarte ; Hernández, Miguel De Dios ; González-Sánchez, Guillermo</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c412t-ca81de6f365c3a13ba1fce2e725340063167ff54aced6cd773b6c8e851236b6a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Biopolymers</topic><topic>Carboxymethyl cellulose</topic><topic>Case crushing</topic><topic>Catechol</topic><topic>Cellulose fibers</topic><topic>Chitosan</topic><topic>Crush tests</topic><topic>Electron microscopy</topic><topic>Gallic acid</topic><topic>Grafting</topic><topic>Kraft pulp</topic><topic>Laccase</topic><topic>Mechanical properties</topic><topic>Mechanical tests</topic><topic>Microscopy</topic><topic>NMR</topic><topic>Nuclear magnetic resonance</topic><topic>Polyphenols</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ballinas-Casarrubias, Lourdes</creatorcontrib><creatorcontrib>Villanueva-Solís, Luis</creatorcontrib><creatorcontrib>Espinoza-Hicks, Carlos</creatorcontrib><creatorcontrib>Camacho-Dávila, Alejandro</creatorcontrib><creatorcontrib>Castillo, Hilda Amelia Piñón</creatorcontrib><creatorcontrib>Pérez, Samuel B</creatorcontrib><creatorcontrib>Villa, Eduardo Duarte</creatorcontrib><creatorcontrib>Hernández, Miguel De Dios</creatorcontrib><creatorcontrib>González-Sánchez, Guillermo</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Polymers</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ballinas-Casarrubias, Lourdes</au><au>Villanueva-Solís, Luis</au><au>Espinoza-Hicks, Carlos</au><au>Camacho-Dávila, Alejandro</au><au>Castillo, Hilda Amelia Piñón</au><au>Pérez, Samuel B</au><au>Villa, Eduardo Duarte</au><au>Hernández, Miguel De Dios</au><au>González-Sánchez, Guillermo</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effect of Laccase-Mediated Biopolymer Grafting on Kraft Pulp Fibers for Enhancing Paper's Mechanical Properties</atitle><jtitle>Polymers</jtitle><addtitle>Polymers (Basel)</addtitle><date>2017-11-02</date><risdate>2017</risdate><volume>9</volume><issue>11</issue><spage>570</spage><pages>570-</pages><issn>2073-4360</issn><eissn>2073-4360</eissn><abstract>High-resistance paper was manufactured by laccase-grafting of carboxymethyl cellulose (CMC) and chitosan (CPX) on Kraft pulp fiber. The reaction was mediated in the presence of laccase by one of the following polyphenols in the presence of air: gallic acid (GA), vanillic acid (VA) and catechol (1,2⁻DHB). Enzyme was added at constant loading (24 kg ton
), 1% pulp consistency, 0.005% CMC, pH = 6.3 ± 0.5 and 2 mM of mediator. CPX content was assessed at two levels (0% and 0.005%). Treated pulps were analyzed by different mechanical tests (ring crush, mullen, corrugating medium test (CMT) flat crush of corrugating medium test and tension). An improvement in these parameters was obtained by biopolymer coupling and selected mediator. When using GA, three parameters increased more than 40%, while ring crush increased 120%. For the case of VA, properties were enhanced from 74% to 88% when CPX was added. For 1,2⁻DHB, there was not found a statistically significant difference between the results in the presence of CPX. Scanning electron microscopy, confocal microscopy, FTIR and
C NMR were used in all papers in order to evaluate grafting. Hence, it was possible to correlate polymerization with an improvement of paper's mechanical properties.</abstract><cop>Switzerland</cop><pub>MDPI AG</pub><pmid>30965872</pmid><doi>10.3390/polym9110570</doi><oa>free_for_read</oa></addata></record> |
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| source | Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; PubMed Central Open Access; MDPI - Multidisciplinary Digital Publishing Institute; PubMed Central |
| subjects | Biopolymers Carboxymethyl cellulose Case crushing Catechol Cellulose fibers Chitosan Crush tests Electron microscopy Gallic acid Grafting Kraft pulp Laccase Mechanical properties Mechanical tests Microscopy NMR Nuclear magnetic resonance Polyphenols |
| title | Effect of Laccase-Mediated Biopolymer Grafting on Kraft Pulp Fibers for Enhancing Paper's Mechanical Properties |
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