Design and assembly of ternary Pt/Re/SnO2 NPs by controlling the zeta potential of individual Pt, Re, and SnO2 NPs
In this study Pt, Re, and SnO 2 nanoparticles (NPs) were combined in a controlled manner into binary and ternary combinations for a possible application for ethanol oxidation. For this purpose, zeta potentials as a function of the pH of the individual NPs solutions were measured. In order to success...
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| Veröffentlicht in: | Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology 2018-05, Vol.20 (5), p.1-13, Article 144 |
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| creator | Drzymała, Elżbieta Gruzeł, Grzegorz Pajor-Świerzy, Anna Depciuch, Joanna Socha, Robert Kowal, Andrzej Warszyński, Piotr Parlinska-Wojtan, Magdalena |
| description | In this study Pt, Re, and SnO
2
nanoparticles (NPs) were combined in a controlled manner into binary and ternary combinations for a possible application for ethanol oxidation. For this purpose, zeta potentials as a function of the pH of the individual NPs solutions were measured. In order to successfully combine the NPs into Pt/SnO
2
and Re/SnO
2
NPs, the solutions were mixed together at a pH guaranteeing opposite zeta potentials of the metal and oxide NPs. The individually synthesized NPs and their binary/ternary combinations were characterized by Fourier transform infrared spectroscopy (FTIR) and scanning transmission electron microscopy (STEM) combined with energy dispersive X-ray spectroscopy (EDS) analysis. FTIR and XPS spectroscopy showed that the individually synthesized Pt and Re NPs are metallic and the Sn component was oxidized to SnO
2
. STEM showed that all NPs are well crystallized and the sizes of the Pt, Re, and SnO
2
NPs were 2.2, 1.0, and 3.4 nm, respectively. Moreover, EDS analysis confirmed the successful formation of binary Pt/SnO
2
and Re/SnO
2
NP, as well as ternary Pt/Re/SnO
2
NP combinations. This study shows that by controlling the zeta potential of individual metal and oxide NPs, it is possible to assemble them into binary and ternary combinations.
Graphical abstract
ᅟ |
| doi_str_mv | 10.1007/s11051-018-4244-0 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_pubme</sourceid><recordid>TN_cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_5949135</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2037920137</sourcerecordid><originalsourceid>FETCH-LOGICAL-c447t-828c5add00dac35566fac556b7ebb239a00a134877493b2857aa4db5f960a95f3</originalsourceid><addsrcrecordid>eNp1kV1rFDEUhgex2A_9Ad4FvPGi4558TZIbQarVQrFLVfAuZGYy25RssiaZwvrrzbptRcGrJOR5H07yNs1LDG8wgFhkjIHjFrBsGWGshSfNEeaCtFJ135_WPZWyBdGxw-Y451sA3BFFnjWHRAkJRHRHTXpvs1sFZMKITM523fstihMqNgWTtmhZFtd28SVcEfR5mVG_RUMMJUXvXVihcmPRT1sM2sRiQ3HG77IujO7OjXM9Lcspuranv_UPkufNwWR8ti_u15Pm2_mHr2ef2surjxdn7y7bgTFRWknkwM04AoxmoJx33WSGuvTC9j2hygAYTJkUginaE8mFMWzs-aQ6MIpP9KR5u_du5n5tx6EOmIzXm-TW9WU6Gqf_vgnuRq_ineaKKUx5Fby-F6T4Y7a56LXLg_XeBBvnrAkwQqjslKzoq3_Q2zjXH_Q7igpFAFNRKbynhhRzTnZ6HAaD3jWq943q2qjeNaqhZsg-kysbVjb9Mf8_9AsG5aEf</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2037920137</pqid></control><display><type>article</type><title>Design and assembly of ternary Pt/Re/SnO2 NPs by controlling the zeta potential of individual Pt, Re, and SnO2 NPs</title><source>Springer Nature - Complete Springer Journals</source><creator>Drzymała, Elżbieta ; Gruzeł, Grzegorz ; Pajor-Świerzy, Anna ; Depciuch, Joanna ; Socha, Robert ; Kowal, Andrzej ; Warszyński, Piotr ; Parlinska-Wojtan, Magdalena</creator><creatorcontrib>Drzymała, Elżbieta ; Gruzeł, Grzegorz ; Pajor-Świerzy, Anna ; Depciuch, Joanna ; Socha, Robert ; Kowal, Andrzej ; Warszyński, Piotr ; Parlinska-Wojtan, Magdalena</creatorcontrib><description>In this study Pt, Re, and SnO
2
nanoparticles (NPs) were combined in a controlled manner into binary and ternary combinations for a possible application for ethanol oxidation. For this purpose, zeta potentials as a function of the pH of the individual NPs solutions were measured. In order to successfully combine the NPs into Pt/SnO
2
and Re/SnO
2
NPs, the solutions were mixed together at a pH guaranteeing opposite zeta potentials of the metal and oxide NPs. The individually synthesized NPs and their binary/ternary combinations were characterized by Fourier transform infrared spectroscopy (FTIR) and scanning transmission electron microscopy (STEM) combined with energy dispersive X-ray spectroscopy (EDS) analysis. FTIR and XPS spectroscopy showed that the individually synthesized Pt and Re NPs are metallic and the Sn component was oxidized to SnO
2
. STEM showed that all NPs are well crystallized and the sizes of the Pt, Re, and SnO
2
NPs were 2.2, 1.0, and 3.4 nm, respectively. Moreover, EDS analysis confirmed the successful formation of binary Pt/SnO
2
and Re/SnO
2
NP, as well as ternary Pt/Re/SnO
2
NP combinations. This study shows that by controlling the zeta potential of individual metal and oxide NPs, it is possible to assemble them into binary and ternary combinations.
Graphical abstract
ᅟ</description><identifier>ISSN: 1388-0764</identifier><identifier>EISSN: 1572-896X</identifier><identifier>DOI: 10.1007/s11051-018-4244-0</identifier><identifier>PMID: 29780276</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Crystallization ; Energy transmission ; Ethanol ; Fourier transforms ; Infrared spectroscopy ; Inorganic Chemistry ; Lasers ; Materials Science ; Nanoparticles ; Nanotechnology ; Optical Devices ; Optics ; Oxidation ; pH effects ; Photonics ; Physical Chemistry ; Research Paper ; Scanning electron microscopy ; Scanning transmission electron microscopy ; Spectrum analysis ; Synthesis ; Tin dioxide ; Transmission electron microscopy ; X ray photoelectron spectroscopy ; X-ray spectroscopy ; Zeta potential</subject><ispartof>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology, 2018-05, Vol.20 (5), p.1-13, Article 144</ispartof><rights>The Author(s) 2018</rights><rights>Journal of Nanoparticle Research is a copyright of Springer, (2018). All Rights Reserved.</rights><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c447t-828c5add00dac35566fac556b7ebb239a00a134877493b2857aa4db5f960a95f3</citedby><cites>FETCH-LOGICAL-c447t-828c5add00dac35566fac556b7ebb239a00a134877493b2857aa4db5f960a95f3</cites><orcidid>0000-0001-6181-9181</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11051-018-4244-0$$EPDF$$P50$$Gspringer$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11051-018-4244-0$$EHTML$$P50$$Gspringer$$Hfree_for_read</linktohtml><link.rule.ids>230,314,778,782,883,27911,27912,41475,42544,51306</link.rule.ids></links><search><creatorcontrib>Drzymała, Elżbieta</creatorcontrib><creatorcontrib>Gruzeł, Grzegorz</creatorcontrib><creatorcontrib>Pajor-Świerzy, Anna</creatorcontrib><creatorcontrib>Depciuch, Joanna</creatorcontrib><creatorcontrib>Socha, Robert</creatorcontrib><creatorcontrib>Kowal, Andrzej</creatorcontrib><creatorcontrib>Warszyński, Piotr</creatorcontrib><creatorcontrib>Parlinska-Wojtan, Magdalena</creatorcontrib><title>Design and assembly of ternary Pt/Re/SnO2 NPs by controlling the zeta potential of individual Pt, Re, and SnO2 NPs</title><title>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology</title><addtitle>J Nanopart Res</addtitle><description>In this study Pt, Re, and SnO
2
nanoparticles (NPs) were combined in a controlled manner into binary and ternary combinations for a possible application for ethanol oxidation. For this purpose, zeta potentials as a function of the pH of the individual NPs solutions were measured. In order to successfully combine the NPs into Pt/SnO
2
and Re/SnO
2
NPs, the solutions were mixed together at a pH guaranteeing opposite zeta potentials of the metal and oxide NPs. The individually synthesized NPs and their binary/ternary combinations were characterized by Fourier transform infrared spectroscopy (FTIR) and scanning transmission electron microscopy (STEM) combined with energy dispersive X-ray spectroscopy (EDS) analysis. FTIR and XPS spectroscopy showed that the individually synthesized Pt and Re NPs are metallic and the Sn component was oxidized to SnO
2
. STEM showed that all NPs are well crystallized and the sizes of the Pt, Re, and SnO
2
NPs were 2.2, 1.0, and 3.4 nm, respectively. Moreover, EDS analysis confirmed the successful formation of binary Pt/SnO
2
and Re/SnO
2
NP, as well as ternary Pt/Re/SnO
2
NP combinations. This study shows that by controlling the zeta potential of individual metal and oxide NPs, it is possible to assemble them into binary and ternary combinations.
Graphical abstract
ᅟ</description><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Crystallization</subject><subject>Energy transmission</subject><subject>Ethanol</subject><subject>Fourier transforms</subject><subject>Infrared spectroscopy</subject><subject>Inorganic Chemistry</subject><subject>Lasers</subject><subject>Materials Science</subject><subject>Nanoparticles</subject><subject>Nanotechnology</subject><subject>Optical Devices</subject><subject>Optics</subject><subject>Oxidation</subject><subject>pH effects</subject><subject>Photonics</subject><subject>Physical Chemistry</subject><subject>Research Paper</subject><subject>Scanning electron microscopy</subject><subject>Scanning transmission electron microscopy</subject><subject>Spectrum analysis</subject><subject>Synthesis</subject><subject>Tin dioxide</subject><subject>Transmission electron microscopy</subject><subject>X ray photoelectron spectroscopy</subject><subject>X-ray spectroscopy</subject><subject>Zeta potential</subject><issn>1388-0764</issn><issn>1572-896X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><sourceid>C6C</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNp1kV1rFDEUhgex2A_9Ad4FvPGi4558TZIbQarVQrFLVfAuZGYy25RssiaZwvrrzbptRcGrJOR5H07yNs1LDG8wgFhkjIHjFrBsGWGshSfNEeaCtFJ135_WPZWyBdGxw-Y451sA3BFFnjWHRAkJRHRHTXpvs1sFZMKITM523fstihMqNgWTtmhZFtd28SVcEfR5mVG_RUMMJUXvXVihcmPRT1sM2sRiQ3HG77IujO7OjXM9Lcspuranv_UPkufNwWR8ti_u15Pm2_mHr2ef2surjxdn7y7bgTFRWknkwM04AoxmoJx33WSGuvTC9j2hygAYTJkUginaE8mFMWzs-aQ6MIpP9KR5u_du5n5tx6EOmIzXm-TW9WU6Gqf_vgnuRq_ineaKKUx5Fby-F6T4Y7a56LXLg_XeBBvnrAkwQqjslKzoq3_Q2zjXH_Q7igpFAFNRKbynhhRzTnZ6HAaD3jWq943q2qjeNaqhZsg-kysbVjb9Mf8_9AsG5aEf</recordid><startdate>20180501</startdate><enddate>20180501</enddate><creator>Drzymała, 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and assembly of ternary Pt/Re/SnO2 NPs by controlling the zeta potential of individual Pt, Re, and SnO2 NPs</title><author>Drzymała, Elżbieta ; Gruzeł, Grzegorz ; Pajor-Świerzy, Anna ; Depciuch, Joanna ; Socha, Robert ; Kowal, Andrzej ; Warszyński, Piotr ; Parlinska-Wojtan, Magdalena</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c447t-828c5add00dac35566fac556b7ebb239a00a134877493b2857aa4db5f960a95f3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Crystallization</topic><topic>Energy transmission</topic><topic>Ethanol</topic><topic>Fourier transforms</topic><topic>Infrared spectroscopy</topic><topic>Inorganic Chemistry</topic><topic>Lasers</topic><topic>Materials Science</topic><topic>Nanoparticles</topic><topic>Nanotechnology</topic><topic>Optical Devices</topic><topic>Optics</topic><topic>Oxidation</topic><topic>pH effects</topic><topic>Photonics</topic><topic>Physical Chemistry</topic><topic>Research Paper</topic><topic>Scanning electron microscopy</topic><topic>Scanning transmission electron microscopy</topic><topic>Spectrum analysis</topic><topic>Synthesis</topic><topic>Tin dioxide</topic><topic>Transmission electron microscopy</topic><topic>X ray photoelectron spectroscopy</topic><topic>X-ray spectroscopy</topic><topic>Zeta potential</topic><toplevel>online_resources</toplevel><creatorcontrib>Drzymała, Elżbieta</creatorcontrib><creatorcontrib>Gruzeł, Grzegorz</creatorcontrib><creatorcontrib>Pajor-Świerzy, Anna</creatorcontrib><creatorcontrib>Depciuch, Joanna</creatorcontrib><creatorcontrib>Socha, Robert</creatorcontrib><creatorcontrib>Kowal, Andrzej</creatorcontrib><creatorcontrib>Warszyński, Piotr</creatorcontrib><creatorcontrib>Parlinska-Wojtan, Magdalena</creatorcontrib><collection>Springer Nature OA Free 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NPs</atitle><jtitle>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology</jtitle><stitle>J Nanopart Res</stitle><date>2018-05-01</date><risdate>2018</risdate><volume>20</volume><issue>5</issue><spage>1</spage><epage>13</epage><pages>1-13</pages><artnum>144</artnum><issn>1388-0764</issn><eissn>1572-896X</eissn><abstract>In this study Pt, Re, and SnO
2
nanoparticles (NPs) were combined in a controlled manner into binary and ternary combinations for a possible application for ethanol oxidation. For this purpose, zeta potentials as a function of the pH of the individual NPs solutions were measured. In order to successfully combine the NPs into Pt/SnO
2
and Re/SnO
2
NPs, the solutions were mixed together at a pH guaranteeing opposite zeta potentials of the metal and oxide NPs. The individually synthesized NPs and their binary/ternary combinations were characterized by Fourier transform infrared spectroscopy (FTIR) and scanning transmission electron microscopy (STEM) combined with energy dispersive X-ray spectroscopy (EDS) analysis. FTIR and XPS spectroscopy showed that the individually synthesized Pt and Re NPs are metallic and the Sn component was oxidized to SnO
2
. STEM showed that all NPs are well crystallized and the sizes of the Pt, Re, and SnO
2
NPs were 2.2, 1.0, and 3.4 nm, respectively. Moreover, EDS analysis confirmed the successful formation of binary Pt/SnO
2
and Re/SnO
2
NP, as well as ternary Pt/Re/SnO
2
NP combinations. This study shows that by controlling the zeta potential of individual metal and oxide NPs, it is possible to assemble them into binary and ternary combinations.
Graphical abstract
ᅟ</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><pmid>29780276</pmid><doi>10.1007/s11051-018-4244-0</doi><tpages>13</tpages><orcidid>https://orcid.org/0000-0001-6181-9181</orcidid><oa>free_for_read</oa></addata></record> |
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| identifier | ISSN: 1388-0764 |
| ispartof | Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology, 2018-05, Vol.20 (5), p.1-13, Article 144 |
| issn | 1388-0764 1572-896X |
| language | eng |
| recordid | cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_5949135 |
| source | Springer Nature - Complete Springer Journals |
| subjects | Characterization and Evaluation of Materials Chemistry and Materials Science Crystallization Energy transmission Ethanol Fourier transforms Infrared spectroscopy Inorganic Chemistry Lasers Materials Science Nanoparticles Nanotechnology Optical Devices Optics Oxidation pH effects Photonics Physical Chemistry Research Paper Scanning electron microscopy Scanning transmission electron microscopy Spectrum analysis Synthesis Tin dioxide Transmission electron microscopy X ray photoelectron spectroscopy X-ray spectroscopy Zeta potential |
| title | Design and assembly of ternary Pt/Re/SnO2 NPs by controlling the zeta potential of individual Pt, Re, and SnO2 NPs |
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