Preparation and Comprehensive Characterization of a Calcium Hydroxyapatite Reference Material

Preparation and Comprehensive Characterization of a Calcium Hydroxyapatite Reference Material

Numerous biological and chemical studies involve the use of calcium hydroxyapatite (HA), Ca10(PO4)6(OH)2. In this study detailed physicochemical characterization of HA, prepared from an aqueous solution, was carried out employing different methods and techniques: chemical and thermal analyses, x-ray...

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Veröffentlicht in:Journal of research of the National Institute of Standards and Technology 2004-11, Vol.109 (6), p.553-568
Hauptverfasser: Markovic, Milenko, Fowler, Bruce O, Tung, Ming S
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Analytical chemistry
Calcium
Chemistry, Analytic
Crystal structure
Heat conductivity
Infrared imaging systems
Minerals
X-rays
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creator Markovic, Milenko
Fowler, Bruce O
Tung, Ming S
description Numerous biological and chemical studies involve the use of calcium hydroxyapatite (HA), Ca10(PO4)6(OH)2. In this study detailed physicochemical characterization of HA, prepared from an aqueous solution, was carried out employing different methods and techniques: chemical and thermal analyses, x-ray diffraction, infrared and Raman spectroscopies, scanning and transmission microscopies, and Brunauer, Emmett, and Teller (BET) surface-area method. The contents of calcium (Ca(2+)), phosphate (PO4 (3-)), hydroxide (OH(-)), hydrogenphosphate (HPO4 (2-)), water (H2O), carbonate (CO3 (2-)), and trace constituents, the Ca/P molar ratio, crystal size and morphology, surface area, unit-cell parameters, crystallinity, and solubility of this HA were determined. This highly pure, homogeneous, and highly crystalline HA is certified as a National Institute of Standards and Technology (NIST) standard reference material, SRM 2910.
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subjects Analytical chemistry
Calcium
Chemistry, Analytic
Crystal structure
Heat conductivity
Infrared imaging systems
Minerals
X-rays
title Preparation and Comprehensive Characterization of a Calcium Hydroxyapatite Reference Material
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