A new polymorph of 1-({[1,3-dihy-droxy-2-(hy-droxy-meth-yl)propan-2-yl]iminio}meth-yl)naphthalen-2-olate

The title compound, C15H17NO4, containing two mol-ecules in the asymmetric unit is a polymorph of the crystal structure published by Martínez et al. [(2011). Eur. J. Org. Chem. pp. 3137-3145] which at 120 K is monoclinic with one mol-ecule in the asymmetric unit. Both mol-ecules in the title compoun...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Acta crystallographica. Section E, Crystallographic communications Crystallographic communications, 2015-09, Vol.71 (Pt 9), p.o686-o687
Hauptverfasser: Guo, Ailing, Zhang, Shurong, Wang, Kun, Zhu, Ruitao
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page o687
container_issue Pt 9
container_start_page o686
container_title Acta crystallographica. Section E, Crystallographic communications
container_volume 71
creator Guo, Ailing
Zhang, Shurong
Wang, Kun
Zhu, Ruitao
description The title compound, C15H17NO4, containing two mol-ecules in the asymmetric unit is a polymorph of the crystal structure published by Martínez et al. [(2011). Eur. J. Org. Chem. pp. 3137-3145] which at 120 K is monoclinic with one mol-ecule in the asymmetric unit. Both mol-ecules in the title compound are in the trans form. In the crystal, N-H⋯O and O-H⋯O hydrogen bonds connect mol-ecules, forming a two-dimensional network parallel to (001).
doi_str_mv 10.1107/S205698901501539X
format Article
fullrecord <record><control><sourceid>proquest_pubme</sourceid><recordid>TN_cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_4555412</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1716257103</sourcerecordid><originalsourceid>FETCH-LOGICAL-p1112-c8736c7d457423a67661033af34afee33b22fe694924df74f0106c2cdb6678353</originalsourceid><addsrcrecordid>eNpVkFtLw0AQhRdRbKn9Ab5IHyu4urPX5kUoxRsUfFBBEAnbZGNWNtk1SdUg_ncbrKXCwBzOB-cMg9AhkFMAos7uKBEymkQExGpY9LiD-p2FO293S_fQsK5fCSHABZOC7qMelSySERF9lE9HpfkYBe_awlchH_lsBHj89QQnDKc2b3Fa-c8WUzze6MI0OW7dcah80OUKte7ZFra0_vsPlTrkTa6d6bB3ujEHaC_TrjbD9R6gh8uL-9k1nt9e3cymcxwAgOJkophMVMqF4pRpqaQEwpjOGNeZMYwtKM2MjHhEeZopnhEgMqFJupBSTZhgA3T-mxuWi8KkiSmbSrs4VLbQVRt7beP_pLR5_OLfYy6E4EBXAeN1QOXflqZu4sLWiXFOl8Yv6xgUSCpUd9UAHW13bUr-3st-AM67fUQ</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1716257103</pqid></control><display><type>article</type><title>A new polymorph of 1-({[1,3-dihy-droxy-2-(hy-droxy-meth-yl)propan-2-yl]iminio}meth-yl)naphthalen-2-olate</title><source>DOAJ Directory of Open Access Journals</source><source>PubMed Central Open Access</source><source>PubMed Central</source><source>Free Full-Text Journals in Chemistry</source><creator>Guo, Ailing ; Zhang, Shurong ; Wang, Kun ; Zhu, Ruitao</creator><creatorcontrib>Guo, Ailing ; Zhang, Shurong ; Wang, Kun ; Zhu, Ruitao</creatorcontrib><description>The title compound, C15H17NO4, containing two mol-ecules in the asymmetric unit is a polymorph of the crystal structure published by Martínez et al. [(2011). Eur. J. Org. Chem. pp. 3137-3145] which at 120 K is monoclinic with one mol-ecule in the asymmetric unit. Both mol-ecules in the title compound are in the trans form. In the crystal, N-H⋯O and O-H⋯O hydrogen bonds connect mol-ecules, forming a two-dimensional network parallel to (001).</description><identifier>ISSN: 2056-9890</identifier><identifier>EISSN: 2056-9890</identifier><identifier>DOI: 10.1107/S205698901501539X</identifier><identifier>PMID: 26396905</identifier><language>eng</language><publisher>England: International Union of Crystallography</publisher><subject>Data Reports</subject><ispartof>Acta crystallographica. Section E, Crystallographic communications, 2015-09, Vol.71 (Pt 9), p.o686-o687</ispartof><rights>Guo et al. 2015 2015</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC4555412/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC4555412/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,727,780,784,864,885,27924,27925,53791,53793</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/26396905$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Guo, Ailing</creatorcontrib><creatorcontrib>Zhang, Shurong</creatorcontrib><creatorcontrib>Wang, Kun</creatorcontrib><creatorcontrib>Zhu, Ruitao</creatorcontrib><title>A new polymorph of 1-({[1,3-dihy-droxy-2-(hy-droxy-meth-yl)propan-2-yl]iminio}meth-yl)naphthalen-2-olate</title><title>Acta crystallographica. Section E, Crystallographic communications</title><addtitle>Acta Crystallogr E Crystallogr Commun</addtitle><description>The title compound, C15H17NO4, containing two mol-ecules in the asymmetric unit is a polymorph of the crystal structure published by Martínez et al. [(2011). Eur. J. Org. Chem. pp. 3137-3145] which at 120 K is monoclinic with one mol-ecule in the asymmetric unit. Both mol-ecules in the title compound are in the trans form. In the crystal, N-H⋯O and O-H⋯O hydrogen bonds connect mol-ecules, forming a two-dimensional network parallel to (001).</description><subject>Data Reports</subject><issn>2056-9890</issn><issn>2056-9890</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><recordid>eNpVkFtLw0AQhRdRbKn9Ab5IHyu4urPX5kUoxRsUfFBBEAnbZGNWNtk1SdUg_ncbrKXCwBzOB-cMg9AhkFMAos7uKBEymkQExGpY9LiD-p2FO293S_fQsK5fCSHABZOC7qMelSySERF9lE9HpfkYBe_awlchH_lsBHj89QQnDKc2b3Fa-c8WUzze6MI0OW7dcah80OUKte7ZFra0_vsPlTrkTa6d6bB3ujEHaC_TrjbD9R6gh8uL-9k1nt9e3cymcxwAgOJkophMVMqF4pRpqaQEwpjOGNeZMYwtKM2MjHhEeZopnhEgMqFJupBSTZhgA3T-mxuWi8KkiSmbSrs4VLbQVRt7beP_pLR5_OLfYy6E4EBXAeN1QOXflqZu4sLWiXFOl8Yv6xgUSCpUd9UAHW13bUr-3st-AM67fUQ</recordid><startdate>20150901</startdate><enddate>20150901</enddate><creator>Guo, Ailing</creator><creator>Zhang, Shurong</creator><creator>Wang, Kun</creator><creator>Zhu, Ruitao</creator><general>International Union of Crystallography</general><scope>NPM</scope><scope>7X8</scope><scope>5PM</scope></search><sort><creationdate>20150901</creationdate><title>A new polymorph of 1-({[1,3-dihy-droxy-2-(hy-droxy-meth-yl)propan-2-yl]iminio}meth-yl)naphthalen-2-olate</title><author>Guo, Ailing ; Zhang, Shurong ; Wang, Kun ; Zhu, Ruitao</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p1112-c8736c7d457423a67661033af34afee33b22fe694924df74f0106c2cdb6678353</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>Data Reports</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Guo, Ailing</creatorcontrib><creatorcontrib>Zhang, Shurong</creatorcontrib><creatorcontrib>Wang, Kun</creatorcontrib><creatorcontrib>Zhu, Ruitao</creatorcontrib><collection>PubMed</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Acta crystallographica. Section E, Crystallographic communications</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Guo, Ailing</au><au>Zhang, Shurong</au><au>Wang, Kun</au><au>Zhu, Ruitao</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A new polymorph of 1-({[1,3-dihy-droxy-2-(hy-droxy-meth-yl)propan-2-yl]iminio}meth-yl)naphthalen-2-olate</atitle><jtitle>Acta crystallographica. Section E, Crystallographic communications</jtitle><addtitle>Acta Crystallogr E Crystallogr Commun</addtitle><date>2015-09-01</date><risdate>2015</risdate><volume>71</volume><issue>Pt 9</issue><spage>o686</spage><epage>o687</epage><pages>o686-o687</pages><issn>2056-9890</issn><eissn>2056-9890</eissn><abstract>The title compound, C15H17NO4, containing two mol-ecules in the asymmetric unit is a polymorph of the crystal structure published by Martínez et al. [(2011). Eur. J. Org. Chem. pp. 3137-3145] which at 120 K is monoclinic with one mol-ecule in the asymmetric unit. Both mol-ecules in the title compound are in the trans form. In the crystal, N-H⋯O and O-H⋯O hydrogen bonds connect mol-ecules, forming a two-dimensional network parallel to (001).</abstract><cop>England</cop><pub>International Union of Crystallography</pub><pmid>26396905</pmid><doi>10.1107/S205698901501539X</doi><oa>free_for_read</oa></addata></record>
fulltext fulltext
identifier ISSN: 2056-9890
ispartof Acta crystallographica. Section E, Crystallographic communications, 2015-09, Vol.71 (Pt 9), p.o686-o687
issn 2056-9890
2056-9890
language eng
recordid cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_4555412
source DOAJ Directory of Open Access Journals; PubMed Central Open Access; PubMed Central; Free Full-Text Journals in Chemistry
subjects Data Reports
title A new polymorph of 1-({[1,3-dihy-droxy-2-(hy-droxy-meth-yl)propan-2-yl]iminio}meth-yl)naphthalen-2-olate
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-04T05%3A46%3A02IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_pubme&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=A%20new%20polymorph%20of%201-(%7B%5B1,3-dihy-droxy-2-(hy-droxy-meth-yl)propan-2-yl%5Diminio%7Dmeth-yl)naphthalen-2-olate&rft.jtitle=Acta%20crystallographica.%20Section%20E,%20Crystallographic%20communications&rft.au=Guo,%20Ailing&rft.date=2015-09-01&rft.volume=71&rft.issue=Pt%209&rft.spage=o686&rft.epage=o687&rft.pages=o686-o687&rft.issn=2056-9890&rft.eissn=2056-9890&rft_id=info:doi/10.1107/S205698901501539X&rft_dat=%3Cproquest_pubme%3E1716257103%3C/proquest_pubme%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1716257103&rft_id=info:pmid/26396905&rfr_iscdi=true