Beamline P02.1 at PETRA III for high-resolution and high-energy powder diffraction

Powder X‐ray diffraction techniques largely benefit from the superior beam quality provided by high‐brilliance synchrotron light sources in terms of photon flux and angular resolution. The High Resolution Powder Diffraction Beamline P02.1 at the storage ring PETRA III (DESY, Hamburg, Germany) combines these strengths with the power of high‐energy X‐rays for materials research. The beamline is operated at a fixed photon energy of 60 keV (0.207 Å wavelength). A high‐resolution monochromator generates the highly collimated X‐ray beam of narrow energy bandwidth. Classic crystal structure determination in reciprocal space at standard and non‐ambient conditions are an essential part of the scientific scope as well as total scattering analysis using the real space information of the pair distribution function. Both methods are complemented by in situ capabilities with time‐resolution in the sub‐second regime owing to the high beam intensity and the advanced detector technology for high‐energy X‐rays. P02.1's efficiency in solving chemical and crystallographic problems is illustrated by presenting key experiments that were carried out within these fields during the early stage of beamline operation.