Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source
Multiplexing of the Linac Coherent Light Source beam was demonstrated for hard X‐rays by spectral division using a near‐perfect diamond thin‐crystal monochromator operating in the Bragg geometry. The wavefront and coherence properties of both the reflected and transmitted beams were well preserved,...
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| Veröffentlicht in: | Journal of synchrotron radiation 2015-05, Vol.22 (3), p.626-633 |
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| creator | Feng, Y. Alonso-Mori, R. Barends, T. R. M. Blank, V. D. Botha, S. Chollet, M. Damiani, D. S. Doak, R. B. Glownia, J. M. Koglin, J. M. Lemke, H. T. Messerschmidt, M. Nass, K. Nelson, S. Schlichting, I. Shoeman, R. L. Shvyd'ko, Yu. V. Sikorski, M. Song, S. Stoupin, S. Terentyev, S. Williams, G. J. Zhu, D. Robert, A. Boutet, S. |
| description | Multiplexing of the Linac Coherent Light Source beam was demonstrated for hard X‐rays by spectral division using a near‐perfect diamond thin‐crystal monochromator operating in the Bragg geometry. The wavefront and coherence properties of both the reflected and transmitted beams were well preserved, thus allowing simultaneous measurements at two separate instruments. In this report, the structure determination of a prototypical protein was performed using serial femtosecond crystallography simultaneously with a femtosecond time‐resolved XANES studies of photoexcited spin transition dynamics in an iron spin‐crossover system. The results of both experiments using the multiplexed beams are similar to those obtained separately, using a dedicated beam, with no significant differences in quality. |
| doi_str_mv | 10.1107/S1600577515003999 |
| format | Article |
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R. M. ; Blank, V. D. ; Botha, S. ; Chollet, M. ; Damiani, D. S. ; Doak, R. B. ; Glownia, J. M. ; Koglin, J. M. ; Lemke, H. T. ; Messerschmidt, M. ; Nass, K. ; Nelson, S. ; Schlichting, I. ; Shoeman, R. L. ; Shvyd'ko, Yu. V. ; Sikorski, M. ; Song, S. ; Stoupin, S. ; Terentyev, S. ; Williams, G. J. ; Zhu, D. ; Robert, A. ; Boutet, S.</creator><creatorcontrib>Feng, Y. ; Alonso-Mori, R. ; Barends, T. R. M. ; Blank, V. D. ; Botha, S. ; Chollet, M. ; Damiani, D. S. ; Doak, R. B. ; Glownia, J. M. ; Koglin, J. M. ; Lemke, H. T. ; Messerschmidt, M. ; Nass, K. ; Nelson, S. ; Schlichting, I. ; Shoeman, R. L. ; Shvyd'ko, Yu. V. ; Sikorski, M. ; Song, S. ; Stoupin, S. ; Terentyev, S. ; Williams, G. J. ; Zhu, D. ; Robert, A. ; Boutet, S. ; SLAC National Accelerator Lab., Menlo Park, CA (United States) ; Argonne National Lab. (ANL), Argonne, IL (United States)</creatorcontrib><description>Multiplexing of the Linac Coherent Light Source beam was demonstrated for hard X‐rays by spectral division using a near‐perfect diamond thin‐crystal monochromator operating in the Bragg geometry. The wavefront and coherence properties of both the reflected and transmitted beams were well preserved, thus allowing simultaneous measurements at two separate instruments. In this report, the structure determination of a prototypical protein was performed using serial femtosecond crystallography simultaneously with a femtosecond time‐resolved XANES studies of photoexcited spin transition dynamics in an iron spin‐crossover system. The results of both experiments using the multiplexed beams are similar to those obtained separately, using a dedicated beam, with no significant differences in quality.</description><identifier>ISSN: 1600-5775</identifier><identifier>ISSN: 0909-0495</identifier><identifier>EISSN: 1600-5775</identifier><identifier>DOI: 10.1107/S1600577515003999</identifier><identifier>PMID: 25931078</identifier><language>eng</language><publisher>5 Abbey Square, Chester, Cheshire CH1 2HU, England: International Union of Crystallography</publisher><subject>CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS ; diamond ; FEL ; Free-Electron Lasers ; multiplexing ; multiplexing diamond ; PARTICLE ACCELERATORS ; thin-crystal ; X-ray</subject><ispartof>Journal of synchrotron radiation, 2015-05, Vol.22 (3), p.626-633</ispartof><rights>Y. Feng et al . 2015</rights><rights>Y. Feng et al . 2015</rights><rights>Y. Feng et al. 2015 2015</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c5422-6da32cabb98b33acdc614f6583704c6bad7ec7894c6f1baa4756079494109f043</citedby><cites>FETCH-LOGICAL-c5422-6da32cabb98b33acdc614f6583704c6bad7ec7894c6f1baa4756079494109f043</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC4416679/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC4416679/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,723,776,780,881,1411,11541,27901,27902,45550,45551,46027,46451,53766,53768</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/25931078$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink><backlink>$$Uhttps://www.osti.gov/servlets/purl/1189942$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Feng, Y.</creatorcontrib><creatorcontrib>Alonso-Mori, R.</creatorcontrib><creatorcontrib>Barends, T. R. M.</creatorcontrib><creatorcontrib>Blank, V. D.</creatorcontrib><creatorcontrib>Botha, S.</creatorcontrib><creatorcontrib>Chollet, M.</creatorcontrib><creatorcontrib>Damiani, D. S.</creatorcontrib><creatorcontrib>Doak, R. B.</creatorcontrib><creatorcontrib>Glownia, J. M.</creatorcontrib><creatorcontrib>Koglin, J. M.</creatorcontrib><creatorcontrib>Lemke, H. T.</creatorcontrib><creatorcontrib>Messerschmidt, M.</creatorcontrib><creatorcontrib>Nass, K.</creatorcontrib><creatorcontrib>Nelson, S.</creatorcontrib><creatorcontrib>Schlichting, I.</creatorcontrib><creatorcontrib>Shoeman, R. L.</creatorcontrib><creatorcontrib>Shvyd'ko, Yu. V.</creatorcontrib><creatorcontrib>Sikorski, M.</creatorcontrib><creatorcontrib>Song, S.</creatorcontrib><creatorcontrib>Stoupin, S.</creatorcontrib><creatorcontrib>Terentyev, S.</creatorcontrib><creatorcontrib>Williams, G. J.</creatorcontrib><creatorcontrib>Zhu, D.</creatorcontrib><creatorcontrib>Robert, A.</creatorcontrib><creatorcontrib>Boutet, S.</creatorcontrib><creatorcontrib>SLAC National Accelerator Lab., Menlo Park, CA (United States)</creatorcontrib><creatorcontrib>Argonne National Lab. (ANL), Argonne, IL (United States)</creatorcontrib><title>Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source</title><title>Journal of synchrotron radiation</title><addtitle>Jnl of Synchrotron Radiation</addtitle><description>Multiplexing of the Linac Coherent Light Source beam was demonstrated for hard X‐rays by spectral division using a near‐perfect diamond thin‐crystal monochromator operating in the Bragg geometry. The wavefront and coherence properties of both the reflected and transmitted beams were well preserved, thus allowing simultaneous measurements at two separate instruments. In this report, the structure determination of a prototypical protein was performed using serial femtosecond crystallography simultaneously with a femtosecond time‐resolved XANES studies of photoexcited spin transition dynamics in an iron spin‐crossover system. The results of both experiments using the multiplexed beams are similar to those obtained separately, using a dedicated beam, with no significant differences in quality.</description><subject>CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS</subject><subject>diamond</subject><subject>FEL</subject><subject>Free-Electron Lasers</subject><subject>multiplexing</subject><subject>multiplexing diamond</subject><subject>PARTICLE ACCELERATORS</subject><subject>thin-crystal</subject><subject>X-ray</subject><issn>1600-5775</issn><issn>0909-0495</issn><issn>1600-5775</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><sourceid>24P</sourceid><recordid>eNqFkUFvFCEYhidGY9vVH-DFEL30sgoDA8PFpFl122ajh9GYeiEMy-xQZ2AFRnf_TX9Lf5lMpm6qHjwBH8_78vF-WfYMwVcIQfa6QhTCgrECFRBizvmD7Hgszcfaw3v7o-wkhGsIEWU5fpwd5QXHyaA8zuxb3TsbopfROAtcA4Lphy5Kq90QgN5ttTe9tjGAIRi7ub2JrbFA-X2IsgMjarad3qUrICOIrQYrY6UCC9dqn3S3NyuzaSOo3OCVfpI9amQX9NO7dZZ9fv_u0-J8vvq4vFicreaqIHk-p2uJcyXrmpc1xlKtFUWkoUWJGSSK1nLNtGIlT_sG1VISVlDIOOEEQd5AgmfZm8l3O9S9XqvUiJed2Ka_SL8XThrx5401rdi4H4IQRCnjyeDFZOBCNCIoE7VqlbNWqygQKjkneYJO717x7vugQxS9CUp33ZSeSHGXjNAx9Fn28i_0OgViUwYjxUpIGB4pNFHKuxC8bg4dIyjGkYt_Rp40z-9_9aD4PeME8An4aTq9_7-juKyu8quLdBobmk9aE6LeHbTSfxOUYVaILx-Wolri1fklq8RX_Avl8Mm-</recordid><startdate>201505</startdate><enddate>201505</enddate><creator>Feng, Y.</creator><creator>Alonso-Mori, R.</creator><creator>Barends, T. 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J.</creator><creator>Zhu, D.</creator><creator>Robert, A.</creator><creator>Boutet, S.</creator><general>International Union of Crystallography</general><general>John Wiley & Sons, Inc</general><scope>BSCLL</scope><scope>24P</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>JQ2</scope><scope>L7M</scope><scope>7X8</scope><scope>OIOZB</scope><scope>OTOTI</scope><scope>5PM</scope></search><sort><creationdate>201505</creationdate><title>Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source</title><author>Feng, Y. ; Alonso-Mori, R. ; Barends, T. R. M. ; Blank, V. D. ; Botha, S. ; Chollet, M. ; Damiani, D. S. ; Doak, R. B. ; Glownia, J. M. ; Koglin, J. M. ; Lemke, H. T. ; Messerschmidt, M. ; Nass, K. ; Nelson, S. ; Schlichting, I. ; Shoeman, R. L. ; Shvyd'ko, Yu. V. ; Sikorski, M. ; Song, S. ; Stoupin, S. ; Terentyev, S. ; Williams, G. 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(ANL), Argonne, IL (United States)</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source</atitle><jtitle>Journal of synchrotron radiation</jtitle><addtitle>Jnl of Synchrotron Radiation</addtitle><date>2015-05</date><risdate>2015</risdate><volume>22</volume><issue>3</issue><spage>626</spage><epage>633</epage><pages>626-633</pages><issn>1600-5775</issn><issn>0909-0495</issn><eissn>1600-5775</eissn><abstract>Multiplexing of the Linac Coherent Light Source beam was demonstrated for hard X‐rays by spectral division using a near‐perfect diamond thin‐crystal monochromator operating in the Bragg geometry. The wavefront and coherence properties of both the reflected and transmitted beams were well preserved, thus allowing simultaneous measurements at two separate instruments. 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| subjects | CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS diamond FEL Free-Electron Lasers multiplexing multiplexing diamond PARTICLE ACCELERATORS thin-crystal X-ray |
| title | Demonstration of simultaneous experiments using thin crystal multiplexing at the Linac Coherent Light Source |
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