High-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector
Coherent (X‐ray) diffractive imaging (CDI) is an increasingly popular form of X‐ray microscopy, mainly due to its potential to produce high‐resolution images and the lack of an objective lens between the sample and its corresponding imaging detector. One challenge, however, is that very high dynamic...
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Veröffentlicht in: | Journal of synchrotron radiation 2014-09, Vol.21 (5), p.1167-1174 |
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creator | Giewekemeyer, Klaus Philipp, Hugh T. Wilke, Robin N. Aquila, Andrew Osterhoff, Markus Tate, Mark W. Shanks, Katherine S. Zozulya, Alexey V. Salditt, Tim Gruner, Sol M. Mancuso, Adrian P. |
description | Coherent (X‐ray) diffractive imaging (CDI) is an increasingly popular form of X‐ray microscopy, mainly due to its potential to produce high‐resolution images and the lack of an objective lens between the sample and its corresponding imaging detector. One challenge, however, is that very high dynamic range diffraction data must be collected to produce both quantitative and high‐resolution images. In this work, hard X‐ray ptychographic coherent diffractive imaging has been performed at the P10 beamline of the PETRA III synchrotron to demonstrate the potential of a very wide dynamic range imaging X‐ray detector (the Mixed‐Mode Pixel Array Detector, or MM‐PAD). The detector is capable of single photon detection, detecting fluxes exceeding 1 × 108 8‐keV photons pixel−1 s−1, and framing at 1 kHz. A ptychographic reconstruction was performed using a peak focal intensity on the order of 1 × 1010 photons µm−2 s−1 within an area of approximately 325 nm × 603 nm. This was done without need of a beam stop and with a very modest attenuation, while `still' images of the empty beam far‐field intensity were recorded without any attenuation. The treatment of the detector frames and CDI methodology for reconstruction of non‐sensitive detector regions, partially also extending the active detector area, are described. |
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One challenge, however, is that very high dynamic range diffraction data must be collected to produce both quantitative and high‐resolution images. In this work, hard X‐ray ptychographic coherent diffractive imaging has been performed at the P10 beamline of the PETRA III synchrotron to demonstrate the potential of a very wide dynamic range imaging X‐ray detector (the Mixed‐Mode Pixel Array Detector, or MM‐PAD). The detector is capable of single photon detection, detecting fluxes exceeding 1 × 108 8‐keV photons pixel−1 s−1, and framing at 1 kHz. A ptychographic reconstruction was performed using a peak focal intensity on the order of 1 × 1010 photons µm−2 s−1 within an area of approximately 325 nm × 603 nm. This was done without need of a beam stop and with a very modest attenuation, while `still' images of the empty beam far‐field intensity were recorded without any attenuation. The treatment of the detector frames and CDI methodology for reconstruction of non‐sensitive detector regions, partially also extending the active detector area, are described.</description><identifier>ISSN: 1600-5775</identifier><identifier>ISSN: 0909-0495</identifier><identifier>EISSN: 1600-5775</identifier><identifier>DOI: 10.1107/S1600577514013411</identifier><identifier>PMID: 25178008</identifier><language>eng</language><publisher>5 Abbey Square, Chester, Cheshire CH1 2HU, England: International Union of Crystallography</publisher><subject>Arrays ; Beams (radiation) ; CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS ; coherent X-ray diffractive imaging ; Diffraction ; Image Enhancement - instrumentation ; Image Enhancement - methods ; Imaging ; Instruments & Instrumentation ; Optical Imaging - instrumentation ; Optical Imaging - methods ; Optics ; Photons ; Physics ; pixel array detectors ; ptychography ; Reconstruction ; Research Papers ; Synchrotrons ; X-Ray Diffraction - instrumentation ; X-Ray Diffraction - methods ; X-rays</subject><ispartof>Journal of synchrotron radiation, 2014-09, Vol.21 (5), p.1167-1174</ispartof><rights>Klaus Giewekemeyer et al. 2014</rights><rights>Klaus Giewekemeyer et al. 2014</rights><rights>Klaus Giewekemeyer et al. 2014 2014</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c6416-81a9b1ba1adee3726c1d561b8ad51fd187e0107c2d90ddf1e290cb7aa8e02b513</citedby><cites>FETCH-LOGICAL-c6416-81a9b1ba1adee3726c1d561b8ad51fd187e0107c2d90ddf1e290cb7aa8e02b513</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC4151683/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC4151683/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,315,729,782,786,887,1419,11571,27933,27934,45583,45584,46061,46485,53800,53802</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/25178008$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink><backlink>$$Uhttps://www.osti.gov/servlets/purl/1625777$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Giewekemeyer, Klaus</creatorcontrib><creatorcontrib>Philipp, Hugh T.</creatorcontrib><creatorcontrib>Wilke, Robin N.</creatorcontrib><creatorcontrib>Aquila, Andrew</creatorcontrib><creatorcontrib>Osterhoff, Markus</creatorcontrib><creatorcontrib>Tate, Mark W.</creatorcontrib><creatorcontrib>Shanks, Katherine S.</creatorcontrib><creatorcontrib>Zozulya, Alexey V.</creatorcontrib><creatorcontrib>Salditt, Tim</creatorcontrib><creatorcontrib>Gruner, Sol M.</creatorcontrib><creatorcontrib>Mancuso, Adrian P.</creatorcontrib><creatorcontrib>Cornell Univ., Ithaca, NY (United States)</creatorcontrib><title>High-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector</title><title>Journal of synchrotron radiation</title><addtitle>Jnl of Synchrotron Radiation</addtitle><description>Coherent (X‐ray) diffractive imaging (CDI) is an increasingly popular form of X‐ray microscopy, mainly due to its potential to produce high‐resolution images and the lack of an objective lens between the sample and its corresponding imaging detector. One challenge, however, is that very high dynamic range diffraction data must be collected to produce both quantitative and high‐resolution images. In this work, hard X‐ray ptychographic coherent diffractive imaging has been performed at the P10 beamline of the PETRA III synchrotron to demonstrate the potential of a very wide dynamic range imaging X‐ray detector (the Mixed‐Mode Pixel Array Detector, or MM‐PAD). The detector is capable of single photon detection, detecting fluxes exceeding 1 × 108 8‐keV photons pixel−1 s−1, and framing at 1 kHz. A ptychographic reconstruction was performed using a peak focal intensity on the order of 1 × 1010 photons µm−2 s−1 within an area of approximately 325 nm × 603 nm. This was done without need of a beam stop and with a very modest attenuation, while `still' images of the empty beam far‐field intensity were recorded without any attenuation. The treatment of the detector frames and CDI methodology for reconstruction of non‐sensitive detector regions, partially also extending the active detector area, are described.</description><subject>Arrays</subject><subject>Beams (radiation)</subject><subject>CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS</subject><subject>coherent X-ray diffractive imaging</subject><subject>Diffraction</subject><subject>Image Enhancement - instrumentation</subject><subject>Image Enhancement - methods</subject><subject>Imaging</subject><subject>Instruments & Instrumentation</subject><subject>Optical Imaging - instrumentation</subject><subject>Optical Imaging - methods</subject><subject>Optics</subject><subject>Photons</subject><subject>Physics</subject><subject>pixel array detectors</subject><subject>ptychography</subject><subject>Reconstruction</subject><subject>Research Papers</subject><subject>Synchrotrons</subject><subject>X-Ray Diffraction - instrumentation</subject><subject>X-Ray Diffraction - methods</subject><subject>X-rays</subject><issn>1600-5775</issn><issn>0909-0495</issn><issn>1600-5775</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><sourceid>24P</sourceid><sourceid>WIN</sourceid><sourceid>EIF</sourceid><recordid>eNqNksFu1TAQRSMEoqXwAWxQBBs2AU8S2wmLSqhAH1WhSC1CrCzHniQuSRzspDR_j59SngosYOXR-Nyx79VE0WMgLwAIf3kOjBDKOYWcQJYD3In2t61k27t7q96LHnh_SQgwnmb3o72UAi8IKfajZmOaNtHLIHujEieHBmNlW3Q4TLE2de2kmswVxqaXjRmaV_E4Laq1jZNju8SzD714ajHuzTXqpLca4zGUXSydk0uscUI1WfcwulfLzuOjm_Mg-vzu7cXRJjk9O35_9Po0USwHlhQgywoqCVIjZjxlCjRlUBVSU6g1FBxJcK5SXRKta8C0JKriUhZI0opCdhAdrnPHuepRq2DDyU6MLvzfLcJKI36_GUwrGnslcqDAiiwMeLoOsH4ywisT_t8qOwzBhgCWhjh5gJ7fvOLs9xn9JHrjFXadHNDOfsuFdHmZ_wdKWXBEeJoG9Nkf6KWd3RDiChQtysCVeaBgpZSz3jusd-aAiO1aiL_WImie3E5lp_i1BwEoV-CH6XD590Rxcv41_XBGScGCNlm1xk94vdNK900wnnEqvnw8FicXnygv6RuxyX4CnQ3Sow</recordid><startdate>201409</startdate><enddate>201409</enddate><creator>Giewekemeyer, Klaus</creator><creator>Philipp, Hugh T.</creator><creator>Wilke, Robin N.</creator><creator>Aquila, Andrew</creator><creator>Osterhoff, Markus</creator><creator>Tate, Mark W.</creator><creator>Shanks, Katherine S.</creator><creator>Zozulya, Alexey V.</creator><creator>Salditt, Tim</creator><creator>Gruner, Sol M.</creator><creator>Mancuso, Adrian P.</creator><general>International Union of Crystallography</general><general>John Wiley & Sons, Inc</general><scope>BSCLL</scope><scope>24P</scope><scope>WIN</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>JQ2</scope><scope>L7M</scope><scope>7X8</scope><scope>7SC</scope><scope>L~C</scope><scope>L~D</scope><scope>OIOZB</scope><scope>OTOTI</scope><scope>5PM</scope></search><sort><creationdate>201409</creationdate><title>High-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector</title><author>Giewekemeyer, Klaus ; 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One challenge, however, is that very high dynamic range diffraction data must be collected to produce both quantitative and high‐resolution images. In this work, hard X‐ray ptychographic coherent diffractive imaging has been performed at the P10 beamline of the PETRA III synchrotron to demonstrate the potential of a very wide dynamic range imaging X‐ray detector (the Mixed‐Mode Pixel Array Detector, or MM‐PAD). The detector is capable of single photon detection, detecting fluxes exceeding 1 × 108 8‐keV photons pixel−1 s−1, and framing at 1 kHz. A ptychographic reconstruction was performed using a peak focal intensity on the order of 1 × 1010 photons µm−2 s−1 within an area of approximately 325 nm × 603 nm. This was done without need of a beam stop and with a very modest attenuation, while `still' images of the empty beam far‐field intensity were recorded without any attenuation. The treatment of the detector frames and CDI methodology for reconstruction of non‐sensitive detector regions, partially also extending the active detector area, are described.</abstract><cop>5 Abbey Square, Chester, Cheshire CH1 2HU, England</cop><pub>International Union of Crystallography</pub><pmid>25178008</pmid><doi>10.1107/S1600577514013411</doi><tpages>8</tpages><oa>free_for_read</oa></addata></record> |
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subjects | Arrays Beams (radiation) CLASSICAL AND QUANTUM MECHANICS, GENERAL PHYSICS coherent X-ray diffractive imaging Diffraction Image Enhancement - instrumentation Image Enhancement - methods Imaging Instruments & Instrumentation Optical Imaging - instrumentation Optical Imaging - methods Optics Photons Physics pixel array detectors ptychography Reconstruction Research Papers Synchrotrons X-Ray Diffraction - instrumentation X-Ray Diffraction - methods X-rays |
title | High-dynamic-range coherent diffractive imaging: ptychography using the mixed-mode pixel array detector |
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