Surface modification of several dental substrates by non-thermal, atmospheric plasma brush
Abstract Objective The purpose of this study was to reveal the effectiveness of non-thermal atmospheric plasma brush in surface wettability and modification of four dental substrates. Methods Specimens of dental substrates including dentin, enamel, and two composites Filtek Z250, Filtek LS Silorane...
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| Veröffentlicht in: | Dental materials 2013-08, Vol.29 (8), p.871-880 |
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| creator | Chen, Mingsheng Zhang, Ying Sky Driver, M Caruso, Anthony N Yu, Qingsong Wang, Yong |
| description | Abstract Objective The purpose of this study was to reveal the effectiveness of non-thermal atmospheric plasma brush in surface wettability and modification of four dental substrates. Methods Specimens of dental substrates including dentin, enamel, and two composites Filtek Z250, Filtek LS Silorane were prepared (∼2 mm thick, ∼10 mm diameter). The prepared surfaces were treated for 5–45 s with a non-thermal atmospheric plasma brush working at temperatures from 36 to 38 °C. The plasma-treatment effects on these surfaces were studied with contact-angle measurement, X-ray photoemission spectroscopy (XPS) and scanning electron microscopy (SEM). Results The non-thermal atmospheric argon plasma brush was very efficient in improving the surface hydrophilicity of four substrates studied. The results indicated that water contact angle values decreased considerably after only 5 s plasma treatment of all these substrates. After 30 s treatment, the values were further reduced to |
| doi_str_mv | 10.1016/j.dental.2013.05.002 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_pubme</sourceid><recordid>TN_cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_3730850</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S010956411300119X</els_id><sourcerecordid>1412526209</sourcerecordid><originalsourceid>FETCH-LOGICAL-c584t-14d67c8b4091409410111084eda3d3130c8337682768d3c5663adc0cabfea9be3</originalsourceid><addsrcrecordid>eNqFUk2LFDEQDaK44-o_EMnRg91Wkv68CLL4BQseVkG8FOmk2snY3RmT9MD8ezPMun5cPBQhVNV7Ve8VY08FlAJE83JXWlqSnkoJQpVQlwDyHtuIru0LgL69zzYgoC_qphIX7FGMOwCoZC8esgup2rrupNqwrzdrGLUhPnvrRmd0cn7hfuSRDhT0xM8kPK5DTEEninw48sUvRdpSmPX0gus0-7jPP2f4ftJx1nwIa9w-Zg9GPUV6cvtess9v33y6el9cf3z34er1dWHqrkqFqGzTmm6ooBc5qrycENBVZLWySigwnVJt08kcVpm6aZS2BoweRtL9QOqSvTrj7tdhJmvywHlw3Ac363BErx3-nVncFr_5A6pWQVdDBnh-CxD8j5ViwtlFQ9OkF_JrRFEJWctGQp9Lq3OpCT7GQOMdjQA82YI7PCuGJ1sQasy25LZnf4541_TLh987UBbq4ChgNI4WQ9YFMgmtd_9j-BfATG7Jfk7f6Uhx59ewZBNQYJQIeHM6jdNlZH2z3v0X9ROugLa9</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1412526209</pqid></control><display><type>article</type><title>Surface modification of several dental substrates by non-thermal, atmospheric plasma brush</title><source>MEDLINE</source><source>Elsevier ScienceDirect Journals</source><creator>Chen, Mingsheng ; Zhang, Ying ; Sky Driver, M ; Caruso, Anthony N ; Yu, Qingsong ; Wang, Yong</creator><creatorcontrib>Chen, Mingsheng ; Zhang, Ying ; Sky Driver, M ; Caruso, Anthony N ; Yu, Qingsong ; Wang, Yong</creatorcontrib><description>Abstract Objective The purpose of this study was to reveal the effectiveness of non-thermal atmospheric plasma brush in surface wettability and modification of four dental substrates. Methods Specimens of dental substrates including dentin, enamel, and two composites Filtek Z250, Filtek LS Silorane were prepared (∼2 mm thick, ∼10 mm diameter). The prepared surfaces were treated for 5–45 s with a non-thermal atmospheric plasma brush working at temperatures from 36 to 38 °C. The plasma-treatment effects on these surfaces were studied with contact-angle measurement, X-ray photoemission spectroscopy (XPS) and scanning electron microscopy (SEM). Results The non-thermal atmospheric argon plasma brush was very efficient in improving the surface hydrophilicity of four substrates studied. The results indicated that water contact angle values decreased considerably after only 5 s plasma treatment of all these substrates. After 30 s treatment, the values were further reduced to <5°, which was close to a value for super hydrophilic surfaces. XPS analysis indicated that the percent of elements associated with mineral in dentin/enamel or fillers in the composites increased. In addition, the percent of carbon (%C) decreased while %O increased for all four substrates. As a result, the O/C ratio increased dramatically, suggesting that new oxygen-containing polar moieties were formed on the surfaces after plasma treatment. SEM surface images indicated that no significant morphology change was induced on these dental substrates after exposure to plasmas. Significance Without affecting the bulk properties, a super-hydrophilic surface could be easily achieved by the plasma brush treatment regardless of original hydrophilicity/hydrophobicity of dental substrates tested.</description><identifier>ISSN: 0109-5641</identifier><identifier>EISSN: 1879-0097</identifier><identifier>DOI: 10.1016/j.dental.2013.05.002</identifier><identifier>PMID: 23755823</identifier><language>eng</language><publisher>England: Elsevier Ltd</publisher><subject>Advanced Basic Science ; Argon - chemistry ; Carbon - analysis ; Composite Resins - chemistry ; Composites ; Contact angle ; Curing Lights, Dental - classification ; Dental Enamel - ultrastructure ; Dental surfaces ; Dentin - ultrastructure ; Dentistry ; Humans ; Hydrophobic and Hydrophilic Interactions ; Materials Testing ; Microscopy, Electron, Scanning ; Non-thermal plasmas ; Oxygen - analysis ; Photoelectron Spectroscopy ; Plasma Gases - chemistry ; Polymerization ; Silorane Resins - chemistry ; Surface Properties ; Time Factors ; Wettability</subject><ispartof>Dental materials, 2013-08, Vol.29 (8), p.871-880</ispartof><rights>Academy of Dental Materials</rights><rights>2013 Academy of Dental Materials</rights><rights>Copyright © 2013 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.</rights><rights>2004 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved 2004</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c584t-14d67c8b4091409410111084eda3d3130c8337682768d3c5663adc0cabfea9be3</citedby><cites>FETCH-LOGICAL-c584t-14d67c8b4091409410111084eda3d3130c8337682768d3c5663adc0cabfea9be3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S010956411300119X$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>230,314,776,780,881,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/23755823$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Chen, Mingsheng</creatorcontrib><creatorcontrib>Zhang, Ying</creatorcontrib><creatorcontrib>Sky Driver, M</creatorcontrib><creatorcontrib>Caruso, Anthony N</creatorcontrib><creatorcontrib>Yu, Qingsong</creatorcontrib><creatorcontrib>Wang, Yong</creatorcontrib><title>Surface modification of several dental substrates by non-thermal, atmospheric plasma brush</title><title>Dental materials</title><addtitle>Dent Mater</addtitle><description>Abstract Objective The purpose of this study was to reveal the effectiveness of non-thermal atmospheric plasma brush in surface wettability and modification of four dental substrates. Methods Specimens of dental substrates including dentin, enamel, and two composites Filtek Z250, Filtek LS Silorane were prepared (∼2 mm thick, ∼10 mm diameter). The prepared surfaces were treated for 5–45 s with a non-thermal atmospheric plasma brush working at temperatures from 36 to 38 °C. The plasma-treatment effects on these surfaces were studied with contact-angle measurement, X-ray photoemission spectroscopy (XPS) and scanning electron microscopy (SEM). Results The non-thermal atmospheric argon plasma brush was very efficient in improving the surface hydrophilicity of four substrates studied. The results indicated that water contact angle values decreased considerably after only 5 s plasma treatment of all these substrates. After 30 s treatment, the values were further reduced to <5°, which was close to a value for super hydrophilic surfaces. XPS analysis indicated that the percent of elements associated with mineral in dentin/enamel or fillers in the composites increased. In addition, the percent of carbon (%C) decreased while %O increased for all four substrates. As a result, the O/C ratio increased dramatically, suggesting that new oxygen-containing polar moieties were formed on the surfaces after plasma treatment. SEM surface images indicated that no significant morphology change was induced on these dental substrates after exposure to plasmas. Significance Without affecting the bulk properties, a super-hydrophilic surface could be easily achieved by the plasma brush treatment regardless of original hydrophilicity/hydrophobicity of dental substrates tested.</description><subject>Advanced Basic Science</subject><subject>Argon - chemistry</subject><subject>Carbon - analysis</subject><subject>Composite Resins - chemistry</subject><subject>Composites</subject><subject>Contact angle</subject><subject>Curing Lights, Dental - classification</subject><subject>Dental Enamel - ultrastructure</subject><subject>Dental surfaces</subject><subject>Dentin - ultrastructure</subject><subject>Dentistry</subject><subject>Humans</subject><subject>Hydrophobic and Hydrophilic Interactions</subject><subject>Materials Testing</subject><subject>Microscopy, Electron, Scanning</subject><subject>Non-thermal plasmas</subject><subject>Oxygen - analysis</subject><subject>Photoelectron Spectroscopy</subject><subject>Plasma Gases - chemistry</subject><subject>Polymerization</subject><subject>Silorane Resins - chemistry</subject><subject>Surface Properties</subject><subject>Time Factors</subject><subject>Wettability</subject><issn>0109-5641</issn><issn>1879-0097</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFUk2LFDEQDaK44-o_EMnRg91Wkv68CLL4BQseVkG8FOmk2snY3RmT9MD8ezPMun5cPBQhVNV7Ve8VY08FlAJE83JXWlqSnkoJQpVQlwDyHtuIru0LgL69zzYgoC_qphIX7FGMOwCoZC8esgup2rrupNqwrzdrGLUhPnvrRmd0cn7hfuSRDhT0xM8kPK5DTEEninw48sUvRdpSmPX0gus0-7jPP2f4ftJx1nwIa9w-Zg9GPUV6cvtess9v33y6el9cf3z34er1dWHqrkqFqGzTmm6ooBc5qrycENBVZLWySigwnVJt08kcVpm6aZS2BoweRtL9QOqSvTrj7tdhJmvywHlw3Ac363BErx3-nVncFr_5A6pWQVdDBnh-CxD8j5ViwtlFQ9OkF_JrRFEJWctGQp9Lq3OpCT7GQOMdjQA82YI7PCuGJ1sQasy25LZnf4541_TLh987UBbq4ChgNI4WQ9YFMgmtd_9j-BfATG7Jfk7f6Uhx59ewZBNQYJQIeHM6jdNlZH2z3v0X9ROugLa9</recordid><startdate>20130801</startdate><enddate>20130801</enddate><creator>Chen, Mingsheng</creator><creator>Zhang, Ying</creator><creator>Sky Driver, M</creator><creator>Caruso, Anthony N</creator><creator>Yu, Qingsong</creator><creator>Wang, Yong</creator><general>Elsevier Ltd</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>5PM</scope></search><sort><creationdate>20130801</creationdate><title>Surface modification of several dental substrates by non-thermal, atmospheric plasma brush</title><author>Chen, Mingsheng ; Zhang, Ying ; Sky Driver, M ; Caruso, Anthony N ; Yu, Qingsong ; Wang, Yong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c584t-14d67c8b4091409410111084eda3d3130c8337682768d3c5663adc0cabfea9be3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Advanced Basic Science</topic><topic>Argon - chemistry</topic><topic>Carbon - analysis</topic><topic>Composite Resins - chemistry</topic><topic>Composites</topic><topic>Contact angle</topic><topic>Curing Lights, Dental - classification</topic><topic>Dental Enamel - ultrastructure</topic><topic>Dental surfaces</topic><topic>Dentin - ultrastructure</topic><topic>Dentistry</topic><topic>Humans</topic><topic>Hydrophobic and Hydrophilic Interactions</topic><topic>Materials Testing</topic><topic>Microscopy, Electron, Scanning</topic><topic>Non-thermal plasmas</topic><topic>Oxygen - analysis</topic><topic>Photoelectron Spectroscopy</topic><topic>Plasma Gases - chemistry</topic><topic>Polymerization</topic><topic>Silorane Resins - chemistry</topic><topic>Surface Properties</topic><topic>Time Factors</topic><topic>Wettability</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Chen, Mingsheng</creatorcontrib><creatorcontrib>Zhang, Ying</creatorcontrib><creatorcontrib>Sky Driver, M</creatorcontrib><creatorcontrib>Caruso, Anthony N</creatorcontrib><creatorcontrib>Yu, Qingsong</creatorcontrib><creatorcontrib>Wang, Yong</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Dental materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Chen, Mingsheng</au><au>Zhang, Ying</au><au>Sky Driver, M</au><au>Caruso, Anthony N</au><au>Yu, Qingsong</au><au>Wang, Yong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Surface modification of several dental substrates by non-thermal, atmospheric plasma brush</atitle><jtitle>Dental materials</jtitle><addtitle>Dent Mater</addtitle><date>2013-08-01</date><risdate>2013</risdate><volume>29</volume><issue>8</issue><spage>871</spage><epage>880</epage><pages>871-880</pages><issn>0109-5641</issn><eissn>1879-0097</eissn><abstract>Abstract Objective The purpose of this study was to reveal the effectiveness of non-thermal atmospheric plasma brush in surface wettability and modification of four dental substrates. Methods Specimens of dental substrates including dentin, enamel, and two composites Filtek Z250, Filtek LS Silorane were prepared (∼2 mm thick, ∼10 mm diameter). The prepared surfaces were treated for 5–45 s with a non-thermal atmospheric plasma brush working at temperatures from 36 to 38 °C. The plasma-treatment effects on these surfaces were studied with contact-angle measurement, X-ray photoemission spectroscopy (XPS) and scanning electron microscopy (SEM). Results The non-thermal atmospheric argon plasma brush was very efficient in improving the surface hydrophilicity of four substrates studied. The results indicated that water contact angle values decreased considerably after only 5 s plasma treatment of all these substrates. After 30 s treatment, the values were further reduced to <5°, which was close to a value for super hydrophilic surfaces. XPS analysis indicated that the percent of elements associated with mineral in dentin/enamel or fillers in the composites increased. In addition, the percent of carbon (%C) decreased while %O increased for all four substrates. As a result, the O/C ratio increased dramatically, suggesting that new oxygen-containing polar moieties were formed on the surfaces after plasma treatment. SEM surface images indicated that no significant morphology change was induced on these dental substrates after exposure to plasmas. Significance Without affecting the bulk properties, a super-hydrophilic surface could be easily achieved by the plasma brush treatment regardless of original hydrophilicity/hydrophobicity of dental substrates tested.</abstract><cop>England</cop><pub>Elsevier Ltd</pub><pmid>23755823</pmid><doi>10.1016/j.dental.2013.05.002</doi><tpages>10</tpages><oa>free_for_read</oa></addata></record> |
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| subjects | Advanced Basic Science Argon - chemistry Carbon - analysis Composite Resins - chemistry Composites Contact angle Curing Lights, Dental - classification Dental Enamel - ultrastructure Dental surfaces Dentin - ultrastructure Dentistry Humans Hydrophobic and Hydrophilic Interactions Materials Testing Microscopy, Electron, Scanning Non-thermal plasmas Oxygen - analysis Photoelectron Spectroscopy Plasma Gases - chemistry Polymerization Silorane Resins - chemistry Surface Properties Time Factors Wettability |
| title | Surface modification of several dental substrates by non-thermal, atmospheric plasma brush |
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