3-Chloro-benzohydrazide

3-Chloro-benzohydrazide

In the title compound, C(7)H(7)ClN(2)O, the hydrazide group is inclined at a dihedral angle of 32.30 (11)° with respect to the benzene ring. The amino H atoms form inter-molecular N-H⋯O hydrogen bonds with the O atoms of two adjacent mol-ecules, resulting in 10-membered rings of graph-set motif R(2)...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Acta crystallographica. Section E, Structure reports online Structure reports online, 2010-07, Vol.66 (Pt 8), p.o2169-o2169
Hauptverfasser: Ashiq, Uzma, Jamal, Rifat Ara, Arshad, Muhammad Nadeem, Khan, Islam Ullah
Format: Artikel
Sprache:eng
Schlagworte:
Organic Papers
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page o2169
container_issue Pt 8
container_start_page o2169
container_title Acta crystallographica. Section E, Structure reports online
container_volume 66
creator Ashiq, Uzma
Jamal, Rifat Ara
Arshad, Muhammad Nadeem
Khan, Islam Ullah
description In the title compound, C(7)H(7)ClN(2)O, the hydrazide group is inclined at a dihedral angle of 32.30 (11)° with respect to the benzene ring. The amino H atoms form inter-molecular N-H⋯O hydrogen bonds with the O atoms of two adjacent mol-ecules, resulting in 10-membered rings of graph-set motif R(2) (2)(10). The imino H atom is also involved in an inter-molecular hydrogen bond with an amino N atom of a symmetry-related mol-ecule, resulting in a zigzag chain along the b axis. The structure is further consolidated by an intra-molecular N-H⋯O inter-action, which results in a five-membered ring.
doi_str_mv 10.1107/S1600536810029508
format Article
fullrecord <record><control><sourceid>proquest_pubme</sourceid><recordid>TN_cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_3007237</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>867728954</sourcerecordid><originalsourceid>FETCH-LOGICAL-p1107-ecc5dafeddee0983a00b56a1622401182900c7d0575e993778667c66d2408cf13</originalsourceid><addsrcrecordid>eNpVkE1LxDAURYMgzji6FjduXVVfkuajG0GKo8KAC3Ud0uTVVtpmbKbCzK-3xVF09eDeyznwCDmncEUpqOtnKgEEl5oCsEyAPiDzKUqmbEaOY3wHoFIxekRmjAqtUwFzcsaTvGpCH5ICu12otr63u9rjCTksbRPxdH8X5HV595I_JKun-8f8dpWsJ2uCzglvS_QeETLNLUAhpKWSsRQo1SwDcMqDUAKzjCulpVROSj_W2pWUL8jNN3c9FC16h92mt41Z93Vr-60Jtjb_m66uzFv4NBxAMa5GwOUe0IePAePGtHV02DS2wzBEo6VSTGciHZcXf1W_jp9n8C8Utl4C</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>867728954</pqid></control><display><type>article</type><title>3-Chloro-benzohydrazide</title><source>DOAJ Directory of Open Access Journals</source><source>PubMed Central Open Access</source><source>PubMed Central</source><source>Free Full-Text Journals in Chemistry</source><creator>Ashiq, Uzma ; Jamal, Rifat Ara ; Arshad, Muhammad Nadeem ; Khan, Islam Ullah</creator><creatorcontrib>Ashiq, Uzma ; Jamal, Rifat Ara ; Arshad, Muhammad Nadeem ; Khan, Islam Ullah</creatorcontrib><description>In the title compound, C(7)H(7)ClN(2)O, the hydrazide group is inclined at a dihedral angle of 32.30 (11)° with respect to the benzene ring. The amino H atoms form inter-molecular N-H⋯O hydrogen bonds with the O atoms of two adjacent mol-ecules, resulting in 10-membered rings of graph-set motif R(2) (2)(10). The imino H atom is also involved in an inter-molecular hydrogen bond with an amino N atom of a symmetry-related mol-ecule, resulting in a zigzag chain along the b axis. The structure is further consolidated by an intra-molecular N-H⋯O inter-action, which results in a five-membered ring.</description><identifier>EISSN: 1600-5368</identifier><identifier>DOI: 10.1107/S1600536810029508</identifier><identifier>PMID: 21588450</identifier><language>eng</language><publisher>United States: International Union of Crystallography</publisher><subject>Organic Papers</subject><ispartof>Acta crystallographica. Section E, Structure reports online, 2010-07, Vol.66 (Pt 8), p.o2169-o2169</ispartof><rights>Ashiq et al. 2010 2010</rights><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007237/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC3007237/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,727,780,784,864,885,27924,27925,53791,53793</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/21588450$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Ashiq, Uzma</creatorcontrib><creatorcontrib>Jamal, Rifat Ara</creatorcontrib><creatorcontrib>Arshad, Muhammad Nadeem</creatorcontrib><creatorcontrib>Khan, Islam Ullah</creatorcontrib><title>3-Chloro-benzohydrazide</title><title>Acta crystallographica. Section E, Structure reports online</title><addtitle>Acta Crystallogr Sect E Struct Rep Online</addtitle><description>In the title compound, C(7)H(7)ClN(2)O, the hydrazide group is inclined at a dihedral angle of 32.30 (11)° with respect to the benzene ring. The amino H atoms form inter-molecular N-H⋯O hydrogen bonds with the O atoms of two adjacent mol-ecules, resulting in 10-membered rings of graph-set motif R(2) (2)(10). The imino H atom is also involved in an inter-molecular hydrogen bond with an amino N atom of a symmetry-related mol-ecule, resulting in a zigzag chain along the b axis. The structure is further consolidated by an intra-molecular N-H⋯O inter-action, which results in a five-membered ring.</description><subject>Organic Papers</subject><issn>1600-5368</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><recordid>eNpVkE1LxDAURYMgzji6FjduXVVfkuajG0GKo8KAC3Ud0uTVVtpmbKbCzK-3xVF09eDeyznwCDmncEUpqOtnKgEEl5oCsEyAPiDzKUqmbEaOY3wHoFIxekRmjAqtUwFzcsaTvGpCH5ICu12otr63u9rjCTksbRPxdH8X5HV595I_JKun-8f8dpWsJ2uCzglvS_QeETLNLUAhpKWSsRQo1SwDcMqDUAKzjCulpVROSj_W2pWUL8jNN3c9FC16h92mt41Z93Vr-60Jtjb_m66uzFv4NBxAMa5GwOUe0IePAePGtHV02DS2wzBEo6VSTGciHZcXf1W_jp9n8C8Utl4C</recordid><startdate>20100731</startdate><enddate>20100731</enddate><creator>Ashiq, Uzma</creator><creator>Jamal, Rifat Ara</creator><creator>Arshad, Muhammad Nadeem</creator><creator>Khan, Islam Ullah</creator><general>International Union of Crystallography</general><scope>NPM</scope><scope>7X8</scope><scope>5PM</scope></search><sort><creationdate>20100731</creationdate><title>3-Chloro-benzohydrazide</title><author>Ashiq, Uzma ; Jamal, Rifat Ara ; Arshad, Muhammad Nadeem ; Khan, Islam Ullah</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p1107-ecc5dafeddee0983a00b56a1622401182900c7d0575e993778667c66d2408cf13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Organic Papers</topic><toplevel>online_resources</toplevel><creatorcontrib>Ashiq, Uzma</creatorcontrib><creatorcontrib>Jamal, Rifat Ara</creatorcontrib><creatorcontrib>Arshad, Muhammad Nadeem</creatorcontrib><creatorcontrib>Khan, Islam Ullah</creatorcontrib><collection>PubMed</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Acta crystallographica. Section E, Structure reports online</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ashiq, Uzma</au><au>Jamal, Rifat Ara</au><au>Arshad, Muhammad Nadeem</au><au>Khan, Islam Ullah</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>3-Chloro-benzohydrazide</atitle><jtitle>Acta crystallographica. Section E, Structure reports online</jtitle><addtitle>Acta Crystallogr Sect E Struct Rep Online</addtitle><date>2010-07-31</date><risdate>2010</risdate><volume>66</volume><issue>Pt 8</issue><spage>o2169</spage><epage>o2169</epage><pages>o2169-o2169</pages><eissn>1600-5368</eissn><abstract>In the title compound, C(7)H(7)ClN(2)O, the hydrazide group is inclined at a dihedral angle of 32.30 (11)° with respect to the benzene ring. The amino H atoms form inter-molecular N-H⋯O hydrogen bonds with the O atoms of two adjacent mol-ecules, resulting in 10-membered rings of graph-set motif R(2) (2)(10). The imino H atom is also involved in an inter-molecular hydrogen bond with an amino N atom of a symmetry-related mol-ecule, resulting in a zigzag chain along the b axis. The structure is further consolidated by an intra-molecular N-H⋯O inter-action, which results in a five-membered ring.</abstract><cop>United States</cop><pub>International Union of Crystallography</pub><pmid>21588450</pmid><doi>10.1107/S1600536810029508</doi><oa>free_for_read</oa></addata></record>
fulltext fulltext
identifier EISSN: 1600-5368
ispartof Acta crystallographica. Section E, Structure reports online, 2010-07, Vol.66 (Pt 8), p.o2169-o2169
issn 1600-5368
language eng
recordid cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_3007237
source DOAJ Directory of Open Access Journals; PubMed Central Open Access; PubMed Central; Free Full-Text Journals in Chemistry
subjects Organic Papers
title 3-Chloro-benzohydrazide
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-04T06%3A07%3A16IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_pubme&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=3-Chloro-benzohydrazide&rft.jtitle=Acta%20crystallographica.%20Section%20E,%20Structure%20reports%20online&rft.au=Ashiq,%20Uzma&rft.date=2010-07-31&rft.volume=66&rft.issue=Pt%208&rft.spage=o2169&rft.epage=o2169&rft.pages=o2169-o2169&rft.eissn=1600-5368&rft_id=info:doi/10.1107/S1600536810029508&rft_dat=%3Cproquest_pubme%3E867728954%3C/proquest_pubme%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=867728954&rft_id=info:pmid/21588450&rfr_iscdi=true