The MYTHEN detector for X-ray powder diffraction experiments at the Swiss Light Source
The MYTHEN single‐photon‐counting silicon microstrip detector has been developed at the Swiss Light Source for time‐resolved powder diffraction experiments. An upgraded version of the detector has been installed at the SLS powder diffraction station allowing the acquisition of diffraction patterns o...
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| Veröffentlicht in: | Journal of synchrotron radiation 2010-09, Vol.17 (5), p.653-668 |
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| container_title | Journal of synchrotron radiation |
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| creator | Bergamaschi, Anna Cervellino, Antonio Dinapoli, Roberto Gozzo, Fabia Henrich, Beat Johnson, Ian Kraft, Philipp Mozzanica, Aldo Schmitt, Bernd Shi, Xintian |
| description | The MYTHEN single‐photon‐counting silicon microstrip detector has been developed at the Swiss Light Source for time‐resolved powder diffraction experiments. An upgraded version of the detector has been installed at the SLS powder diffraction station allowing the acquisition of diffraction patterns over 120° in 2θ in fractions of seconds. Thanks to the outstanding performance of the detector and to the calibration procedures developed, the quality of the data obtained is now comparable with that of traditional high‐resolution point detectors in terms of FWHM resolution and peak profile shape, with the additional advantage of fast and simultaneous acquisition of the full diffraction pattern. MYTHEN is therefore optimal for time‐resolved or dose‐critical measurements. The characteristics of the MYTHEN detector together with the calibration procedures implemented for the optimization of the data are described in detail. The refinements of two known standard powders are discussed together with a remarkable application of MYTHEN to organic compounds in relation to the problem of radiation damage. |
| doi_str_mv | 10.1107/S0909049510026051 |
| format | Article |
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An upgraded version of the detector has been installed at the SLS powder diffraction station allowing the acquisition of diffraction patterns over 120° in 2θ in fractions of seconds. Thanks to the outstanding performance of the detector and to the calibration procedures developed, the quality of the data obtained is now comparable with that of traditional high‐resolution point detectors in terms of FWHM resolution and peak profile shape, with the additional advantage of fast and simultaneous acquisition of the full diffraction pattern. MYTHEN is therefore optimal for time‐resolved or dose‐critical measurements. The characteristics of the MYTHEN detector together with the calibration procedures implemented for the optimization of the data are described in detail. The refinements of two known standard powders are discussed together with a remarkable application of MYTHEN to organic compounds in relation to the problem of radiation damage.</description><identifier>ISSN: 1600-5775</identifier><identifier>ISSN: 0909-0495</identifier><identifier>EISSN: 1600-5775</identifier><identifier>DOI: 10.1107/S0909049510026051</identifier><identifier>PMID: 20724787</identifier><language>eng</language><publisher>5 Abbey Square, Chester, Cheshire CH1 2HU, England: International Union of Crystallography</publisher><subject>Bupivacaine - chemistry ; Calibration ; Detectors ; Diffraction ; Diffraction patterns ; Light sources ; Optimization ; powder diffraction ; Powder Diffraction - instrumentation ; Powder Diffraction - methods ; Research Papers ; Stations ; Synchrotron radiation ; Synchrotrons - instrumentation ; X-Ray Diffraction - instrumentation ; X-Ray Diffraction - methods</subject><ispartof>Journal of synchrotron radiation, 2010-09, Vol.17 (5), p.653-668</ispartof><rights>Anna Bergamaschi et al. 2010</rights><rights>Anna Bergamaschi et al. 2010 2010</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c5838-32b194c7f730b0134ce01dcd1ab9d54cf40be639ead29fb636fe0ca5219132693</citedby><cites>FETCH-LOGICAL-c5838-32b194c7f730b0134ce01dcd1ab9d54cf40be639ead29fb636fe0ca5219132693</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC2924792/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC2924792/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,315,728,781,785,886,1418,11567,27929,27930,45579,45580,46057,46481,53796,53798</link.rule.ids><linktorsrc>$$Uhttps://onlinelibrary.wiley.com/doi/abs/10.1107%2FS0909049510026051$$EView_record_in_Wiley-Blackwell$$FView_record_in_$$GWiley-Blackwell</linktorsrc><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/20724787$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Bergamaschi, Anna</creatorcontrib><creatorcontrib>Cervellino, Antonio</creatorcontrib><creatorcontrib>Dinapoli, Roberto</creatorcontrib><creatorcontrib>Gozzo, Fabia</creatorcontrib><creatorcontrib>Henrich, Beat</creatorcontrib><creatorcontrib>Johnson, Ian</creatorcontrib><creatorcontrib>Kraft, Philipp</creatorcontrib><creatorcontrib>Mozzanica, Aldo</creatorcontrib><creatorcontrib>Schmitt, Bernd</creatorcontrib><creatorcontrib>Shi, Xintian</creatorcontrib><title>The MYTHEN detector for X-ray powder diffraction experiments at the Swiss Light Source</title><title>Journal of synchrotron radiation</title><addtitle>J. Synchrotron Rad</addtitle><description>The MYTHEN single‐photon‐counting silicon microstrip detector has been developed at the Swiss Light Source for time‐resolved powder diffraction experiments. An upgraded version of the detector has been installed at the SLS powder diffraction station allowing the acquisition of diffraction patterns over 120° in 2θ in fractions of seconds. Thanks to the outstanding performance of the detector and to the calibration procedures developed, the quality of the data obtained is now comparable with that of traditional high‐resolution point detectors in terms of FWHM resolution and peak profile shape, with the additional advantage of fast and simultaneous acquisition of the full diffraction pattern. MYTHEN is therefore optimal for time‐resolved or dose‐critical measurements. The characteristics of the MYTHEN detector together with the calibration procedures implemented for the optimization of the data are described in detail. The refinements of two known standard powders are discussed together with a remarkable application of MYTHEN to organic compounds in relation to the problem of radiation damage.</description><subject>Bupivacaine - chemistry</subject><subject>Calibration</subject><subject>Detectors</subject><subject>Diffraction</subject><subject>Diffraction patterns</subject><subject>Light sources</subject><subject>Optimization</subject><subject>powder diffraction</subject><subject>Powder Diffraction - instrumentation</subject><subject>Powder Diffraction - methods</subject><subject>Research Papers</subject><subject>Stations</subject><subject>Synchrotron radiation</subject><subject>Synchrotrons - instrumentation</subject><subject>X-Ray Diffraction - instrumentation</subject><subject>X-Ray Diffraction - methods</subject><issn>1600-5775</issn><issn>0909-0495</issn><issn>1600-5775</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkc1uEzEUhUcIRH_gAdgg71gNvbbH9niDhKomKUrbxQRoV5bHc6cxTDKpPSHN2-MqJWrForIsW_L5jo7vybIPFD5TCuqkAp1WoQUFYBIEfZUdUgmQC6XE6yf3g-woxl8AVCrG32YHDBQrVKkOsx-zOZKLm9nk7JI0OKAb-kDatK_zYLdk1W8aDKTxbRusG3y_JHi_wuAXuBwisQMZEl9tfIxk6m_nA6n6dXD4LnvT2i7i-8fzOPs-OpudTvLp1fj89Os0d6LkZc5ZTXXhVKs41EB54RBo4xpqa92IwrUF1Ci5Rtsw3daSyxbBWcGoppxJzY-zLzvf1bpeYONSqmA7s0oBbdia3nrz_GXp5-a2_2OYTgPQLBl8ejQI_d0a42AWPjrsOrvEfh1NySkVabr8RaUqSi3LgkJS0p3ShT7GgO0-DwXzUJz5r7jEfHz6kT3xr6kkKHeCje9w-7Kj-VbdjEcCWJnQfIf6OOD9HrXht5GKK2F-Xo7N9YWq-GgkzYT_BSsJsoU</recordid><startdate>201009</startdate><enddate>201009</enddate><creator>Bergamaschi, Anna</creator><creator>Cervellino, Antonio</creator><creator>Dinapoli, Roberto</creator><creator>Gozzo, Fabia</creator><creator>Henrich, Beat</creator><creator>Johnson, Ian</creator><creator>Kraft, Philipp</creator><creator>Mozzanica, Aldo</creator><creator>Schmitt, Bernd</creator><creator>Shi, Xintian</creator><general>International Union of Crystallography</general><scope>BSCLL</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope><scope>5PM</scope></search><sort><creationdate>201009</creationdate><title>The MYTHEN detector for X-ray powder diffraction experiments at the Swiss Light Source</title><author>Bergamaschi, Anna ; Cervellino, Antonio ; Dinapoli, Roberto ; Gozzo, Fabia ; Henrich, Beat ; Johnson, Ian ; Kraft, Philipp ; Mozzanica, Aldo ; Schmitt, Bernd ; Shi, Xintian</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c5838-32b194c7f730b0134ce01dcd1ab9d54cf40be639ead29fb636fe0ca5219132693</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Bupivacaine - chemistry</topic><topic>Calibration</topic><topic>Detectors</topic><topic>Diffraction</topic><topic>Diffraction patterns</topic><topic>Light sources</topic><topic>Optimization</topic><topic>powder diffraction</topic><topic>Powder Diffraction - instrumentation</topic><topic>Powder Diffraction - methods</topic><topic>Research Papers</topic><topic>Stations</topic><topic>Synchrotron radiation</topic><topic>Synchrotrons - instrumentation</topic><topic>X-Ray Diffraction - instrumentation</topic><topic>X-Ray Diffraction - methods</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bergamaschi, Anna</creatorcontrib><creatorcontrib>Cervellino, Antonio</creatorcontrib><creatorcontrib>Dinapoli, Roberto</creatorcontrib><creatorcontrib>Gozzo, Fabia</creatorcontrib><creatorcontrib>Henrich, Beat</creatorcontrib><creatorcontrib>Johnson, Ian</creatorcontrib><creatorcontrib>Kraft, Philipp</creatorcontrib><creatorcontrib>Mozzanica, Aldo</creatorcontrib><creatorcontrib>Schmitt, Bernd</creatorcontrib><creatorcontrib>Shi, Xintian</creatorcontrib><collection>Istex</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Journal of synchrotron radiation</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>Bergamaschi, Anna</au><au>Cervellino, Antonio</au><au>Dinapoli, Roberto</au><au>Gozzo, Fabia</au><au>Henrich, Beat</au><au>Johnson, Ian</au><au>Kraft, Philipp</au><au>Mozzanica, Aldo</au><au>Schmitt, Bernd</au><au>Shi, Xintian</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The MYTHEN detector for X-ray powder diffraction experiments at the Swiss Light Source</atitle><jtitle>Journal of synchrotron radiation</jtitle><addtitle>J. Synchrotron Rad</addtitle><date>2010-09</date><risdate>2010</risdate><volume>17</volume><issue>5</issue><spage>653</spage><epage>668</epage><pages>653-668</pages><issn>1600-5775</issn><issn>0909-0495</issn><eissn>1600-5775</eissn><abstract>The MYTHEN single‐photon‐counting silicon microstrip detector has been developed at the Swiss Light Source for time‐resolved powder diffraction experiments. An upgraded version of the detector has been installed at the SLS powder diffraction station allowing the acquisition of diffraction patterns over 120° in 2θ in fractions of seconds. Thanks to the outstanding performance of the detector and to the calibration procedures developed, the quality of the data obtained is now comparable with that of traditional high‐resolution point detectors in terms of FWHM resolution and peak profile shape, with the additional advantage of fast and simultaneous acquisition of the full diffraction pattern. MYTHEN is therefore optimal for time‐resolved or dose‐critical measurements. The characteristics of the MYTHEN detector together with the calibration procedures implemented for the optimization of the data are described in detail. The refinements of two known standard powders are discussed together with a remarkable application of MYTHEN to organic compounds in relation to the problem of radiation damage.</abstract><cop>5 Abbey Square, Chester, Cheshire CH1 2HU, England</cop><pub>International Union of Crystallography</pub><pmid>20724787</pmid><doi>10.1107/S0909049510026051</doi><tpages>16</tpages><oa>free_for_read</oa></addata></record> |
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| source | Wiley Online Library (Open Access Collection) |
| subjects | Bupivacaine - chemistry Calibration Detectors Diffraction Diffraction patterns Light sources Optimization powder diffraction Powder Diffraction - instrumentation Powder Diffraction - methods Research Papers Stations Synchrotron radiation Synchrotrons - instrumentation X-Ray Diffraction - instrumentation X-Ray Diffraction - methods |
| title | The MYTHEN detector for X-ray powder diffraction experiments at the Swiss Light Source |
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