Crystal structure of hexa-glycinium dodeca-iodo-triplumbate
The crystal structure of hexa-glycinium tetra-μ-iodido-octa-iodido-triplumbate, (C H NO ) [Pb I ] or (GlyH) [Pb I ], is reported. The compound crystallizes in the triclinic space group . The [Pb I ] anion is discrete and located around a special position: the central Pb ion located on the inversion...
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| Veröffentlicht in: | Acta crystallographica. Section E, Crystallographic communications Crystallographic communications, 2024-09, Vol.80 (Pt 9), p.916-920 |
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| container_issue | Pt 9 |
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| container_title | Acta crystallographica. Section E, Crystallographic communications |
| container_volume | 80 |
| creator | Tonoyan, Gayane S Giester, Gerald Ghazaryan, Vahram V Chilingaryan, Ruben Yu Margaryan, Arthur A Mkrtchyan, Artak H Petrosyan, Aram M |
| description | The crystal structure of hexa-glycinium tetra-μ-iodido-octa-iodido-triplumbate, (C
H
NO
)
[Pb
I
] or (GlyH)
[Pb
I
], is reported. The compound crystallizes in the triclinic space group
. The [Pb
I
]
anion is discrete and located around a special position: the central Pb ion located on the inversion center is holodirected, while the other two are hemidirected. The supra-molecular nature is mainly based on C-H⋯I, N-H⋯I, O-H⋯I and N-H⋯O hydrogen bonds. Dimeric cations of type (
⋯
) for the amino acid glycine are observed for the first time. |
| doi_str_mv | 10.1107/S2056989024007606 |
| format | Article |
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H
NO
)
[Pb
I
] or (GlyH)
[Pb
I
], is reported. The compound crystallizes in the triclinic space group
. The [Pb
I
]
anion is discrete and located around a special position: the central Pb ion located on the inversion center is holodirected, while the other two are hemidirected. The supra-molecular nature is mainly based on C-H⋯I, N-H⋯I, O-H⋯I and N-H⋯O hydrogen bonds. Dimeric cations of type (
⋯
) for the amino acid glycine are observed for the first time.</description><identifier>ISSN: 2056-9890</identifier><identifier>EISSN: 2056-9890</identifier><identifier>DOI: 10.1107/S2056989024007606</identifier><identifier>PMID: 39267865</identifier><language>eng</language><publisher>England: International Union of Crystallography</publisher><subject>Research Communications</subject><ispartof>Acta crystallographica. Section E, Crystallographic communications, 2024-09, Vol.80 (Pt 9), p.916-920</ispartof><rights>Tonoyan et al. 2024.</rights><rights>Tonoyan et al. 2024 2024</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><orcidid>0000-0002-9054-0734 ; 0009-0003-2835-349X ; 0000-0002-0449-1308 ; 0009-0000-3334-0835 ; 0000-0002-0457-3696</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC11389678/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC11389678/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,723,776,780,860,881,27901,27902,53766,53768</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/39267865$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Tonoyan, Gayane S</creatorcontrib><creatorcontrib>Giester, Gerald</creatorcontrib><creatorcontrib>Ghazaryan, Vahram V</creatorcontrib><creatorcontrib>Chilingaryan, Ruben Yu</creatorcontrib><creatorcontrib>Margaryan, Arthur A</creatorcontrib><creatorcontrib>Mkrtchyan, Artak H</creatorcontrib><creatorcontrib>Petrosyan, Aram M</creatorcontrib><title>Crystal structure of hexa-glycinium dodeca-iodo-triplumbate</title><title>Acta crystallographica. Section E, Crystallographic communications</title><addtitle>Acta Crystallogr E Crystallogr Commun</addtitle><description>The crystal structure of hexa-glycinium tetra-μ-iodido-octa-iodido-triplumbate, (C
H
NO
)
[Pb
I
] or (GlyH)
[Pb
I
], is reported. The compound crystallizes in the triclinic space group
. The [Pb
I
]
anion is discrete and located around a special position: the central Pb ion located on the inversion center is holodirected, while the other two are hemidirected. The supra-molecular nature is mainly based on C-H⋯I, N-H⋯I, O-H⋯I and N-H⋯O hydrogen bonds. Dimeric cations of type (
⋯
) for the amino acid glycine are observed for the first time.</description><subject>Research Communications</subject><issn>2056-9890</issn><issn>2056-9890</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNpVkEtPwzAQhC0EolXpD-CCcuQSWNvxSxwQqspDqsQBOEeO47RGSRzsBNF_TyoKKqddzay-0SxC5xiuMAZx_UKAcSUVkAxAcOBHaLqT0p12fLBP0DzGdwDAGaOckVM0oYpwITmboptF2MZe10nsw2D6IdjEV8nGful0XW-Na93QJKUvrdGp86VP--C6emgK3dszdFLpOtr5fs7Q2_3ydfGYrp4fnhZ3q7TDmMjUWqmJ4qwkRBDQBTPAxgLGsKykQlSmpKCIFroSnBrIaKYwt6AKLGVWVEBn6PaH2w1FY0tj2z7oOu-Ca3TY5l67_L_Tuk2-9p85xlSqsehIuNwTgv8YbOzzxkVj61q31g8xpxgyRiTDajy9OAz7S_l9Gf0GFPZvMg</recordid><startdate>20240901</startdate><enddate>20240901</enddate><creator>Tonoyan, Gayane S</creator><creator>Giester, Gerald</creator><creator>Ghazaryan, Vahram V</creator><creator>Chilingaryan, Ruben Yu</creator><creator>Margaryan, Arthur A</creator><creator>Mkrtchyan, Artak H</creator><creator>Petrosyan, Aram M</creator><general>International Union of Crystallography</general><scope>NPM</scope><scope>7X8</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0002-9054-0734</orcidid><orcidid>https://orcid.org/0009-0003-2835-349X</orcidid><orcidid>https://orcid.org/0000-0002-0449-1308</orcidid><orcidid>https://orcid.org/0009-0000-3334-0835</orcidid><orcidid>https://orcid.org/0000-0002-0457-3696</orcidid></search><sort><creationdate>20240901</creationdate><title>Crystal structure of hexa-glycinium dodeca-iodo-triplumbate</title><author>Tonoyan, Gayane S ; Giester, Gerald ; Ghazaryan, Vahram V ; Chilingaryan, Ruben Yu ; Margaryan, Arthur A ; Mkrtchyan, Artak H ; Petrosyan, Aram M</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p1128-ee8a2965d22720ab5c05107cc54d377fcd3092a7af763c0434916e09b1884bf03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Research Communications</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Tonoyan, Gayane S</creatorcontrib><creatorcontrib>Giester, Gerald</creatorcontrib><creatorcontrib>Ghazaryan, Vahram V</creatorcontrib><creatorcontrib>Chilingaryan, Ruben Yu</creatorcontrib><creatorcontrib>Margaryan, Arthur A</creatorcontrib><creatorcontrib>Mkrtchyan, Artak H</creatorcontrib><creatorcontrib>Petrosyan, Aram M</creatorcontrib><collection>PubMed</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Acta crystallographica. Section E, Crystallographic communications</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Tonoyan, Gayane S</au><au>Giester, Gerald</au><au>Ghazaryan, Vahram V</au><au>Chilingaryan, Ruben Yu</au><au>Margaryan, Arthur A</au><au>Mkrtchyan, Artak H</au><au>Petrosyan, Aram M</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Crystal structure of hexa-glycinium dodeca-iodo-triplumbate</atitle><jtitle>Acta crystallographica. Section E, Crystallographic communications</jtitle><addtitle>Acta Crystallogr E Crystallogr Commun</addtitle><date>2024-09-01</date><risdate>2024</risdate><volume>80</volume><issue>Pt 9</issue><spage>916</spage><epage>920</epage><pages>916-920</pages><issn>2056-9890</issn><eissn>2056-9890</eissn><abstract>The crystal structure of hexa-glycinium tetra-μ-iodido-octa-iodido-triplumbate, (C
H
NO
)
[Pb
I
] or (GlyH)
[Pb
I
], is reported. The compound crystallizes in the triclinic space group
. The [Pb
I
]
anion is discrete and located around a special position: the central Pb ion located on the inversion center is holodirected, while the other two are hemidirected. The supra-molecular nature is mainly based on C-H⋯I, N-H⋯I, O-H⋯I and N-H⋯O hydrogen bonds. Dimeric cations of type (
⋯
) for the amino acid glycine are observed for the first time.</abstract><cop>England</cop><pub>International Union of Crystallography</pub><pmid>39267865</pmid><doi>10.1107/S2056989024007606</doi><tpages>5</tpages><orcidid>https://orcid.org/0000-0002-9054-0734</orcidid><orcidid>https://orcid.org/0009-0003-2835-349X</orcidid><orcidid>https://orcid.org/0000-0002-0449-1308</orcidid><orcidid>https://orcid.org/0009-0000-3334-0835</orcidid><orcidid>https://orcid.org/0000-0002-0457-3696</orcidid><oa>free_for_read</oa></addata></record> |
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| source | DOAJ Directory of Open Access Journals; PubMed Central; Free Full-Text Journals in Chemistry; PubMed Central Open Access |
| subjects | Research Communications |
| title | Crystal structure of hexa-glycinium dodeca-iodo-triplumbate |
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