Influence of the Second-Phase Resin Structure on the Interfacial Shear Strength of Carbon Fiber/Epoxy Resin
The toughening modification of epoxy resin has received widespread attention. The addition of the second-phase resin has a good toughening effect on epoxy resin. In order to investigate the effect of the second-phase resin on the interphase of composites, in this work the interfacial properties of c...
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description | The toughening modification of epoxy resin has received widespread attention. The addition of the second-phase resin has a good toughening effect on epoxy resin. In order to investigate the effect of the second-phase resin on the interphase of composites, in this work the interfacial properties of carbon fiber (CF)/epoxy resin with the second-phase resin structure were investigated. Methodologies including surface structure observation, chemical characteristics, surface energy of the CF, and micro-phase structure characterization of resin were tested, followed by the micro-interfacial performance of CF/epoxy composites before and after hygrothermal treatment. The results revealed that the sizing process has the positive effect of increasing the interfacial bonding properties of CF/epoxy. From the interfacial shear strength (IFSS) test, the introduction of the second phase in the resin reduced the interfacial bonding performance between the CF and epoxy. After the hygrothermal treatment, water molecules diffused along the interfacial paths between the two resins, which in turn created defects and consequently brought about a reduction in the IFSS. |
doi_str_mv | 10.3390/ma17061323 |
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The addition of the second-phase resin has a good toughening effect on epoxy resin. In order to investigate the effect of the second-phase resin on the interphase of composites, in this work the interfacial properties of carbon fiber (CF)/epoxy resin with the second-phase resin structure were investigated. Methodologies including surface structure observation, chemical characteristics, surface energy of the CF, and micro-phase structure characterization of resin were tested, followed by the micro-interfacial performance of CF/epoxy composites before and after hygrothermal treatment. The results revealed that the sizing process has the positive effect of increasing the interfacial bonding properties of CF/epoxy. From the interfacial shear strength (IFSS) test, the introduction of the second phase in the resin reduced the interfacial bonding performance between the CF and epoxy. After the hygrothermal treatment, water molecules diffused along the interfacial paths between the two resins, which in turn created defects and consequently brought about a reduction in the IFSS.</description><identifier>ISSN: 1996-1944</identifier><identifier>EISSN: 1996-1944</identifier><identifier>DOI: 10.3390/ma17061323</identifier><identifier>PMID: 38541477</identifier><language>eng</language><publisher>Switzerland: MDPI AG</publisher><subject>Bonding strength ; Carbon fiber reinforced plastics ; Composite materials ; Contact angle ; Curing ; Epoxy resins ; Heat resistance ; Interfacial bonding ; Interfacial properties ; Interfacial shear strength ; Manufacturing ; Shear strength ; Solid phases ; Structural analysis ; Surface energy ; Surface structure</subject><ispartof>Materials, 2024-03, Vol.17 (6), p.1323</ispartof><rights>COPYRIGHT 2024 MDPI AG</rights><rights>2024 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>2024 by the authors. 2024</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c446t-bd5d827084ebf518611df7f60fccc7beadddd88b7876f919a5ff7972fce7ee1a3</citedby><cites>FETCH-LOGICAL-c446t-bd5d827084ebf518611df7f60fccc7beadddd88b7876f919a5ff7972fce7ee1a3</cites><orcidid>0000-0003-4358-2576</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC10972230/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC10972230/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,727,780,784,885,27923,27924,53790,53792</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/38541477$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Liu, Hansong</creatorcontrib><creatorcontrib>Sun, Jinsong</creatorcontrib><creatorcontrib>Zhang, Lianwang</creatorcontrib><creatorcontrib>Liu, Zhaobo</creatorcontrib><creatorcontrib>Huang, Chengyu</creatorcontrib><creatorcontrib>Sun, Mingchen</creatorcontrib><creatorcontrib>Duan, Ziqi</creatorcontrib><creatorcontrib>Wang, Wenge</creatorcontrib><creatorcontrib>Zhong, Xiangyu</creatorcontrib><creatorcontrib>Bao, Jianwen</creatorcontrib><title>Influence of the Second-Phase Resin Structure on the Interfacial Shear Strength of Carbon Fiber/Epoxy Resin</title><title>Materials</title><addtitle>Materials (Basel)</addtitle><description>The toughening modification of epoxy resin has received widespread attention. The addition of the second-phase resin has a good toughening effect on epoxy resin. In order to investigate the effect of the second-phase resin on the interphase of composites, in this work the interfacial properties of carbon fiber (CF)/epoxy resin with the second-phase resin structure were investigated. Methodologies including surface structure observation, chemical characteristics, surface energy of the CF, and micro-phase structure characterization of resin were tested, followed by the micro-interfacial performance of CF/epoxy composites before and after hygrothermal treatment. The results revealed that the sizing process has the positive effect of increasing the interfacial bonding properties of CF/epoxy. From the interfacial shear strength (IFSS) test, the introduction of the second phase in the resin reduced the interfacial bonding performance between the CF and epoxy. After the hygrothermal treatment, water molecules diffused along the interfacial paths between the two resins, which in turn created defects and consequently brought about a reduction in the IFSS.</description><subject>Bonding strength</subject><subject>Carbon fiber reinforced plastics</subject><subject>Composite materials</subject><subject>Contact angle</subject><subject>Curing</subject><subject>Epoxy resins</subject><subject>Heat resistance</subject><subject>Interfacial bonding</subject><subject>Interfacial properties</subject><subject>Interfacial shear strength</subject><subject>Manufacturing</subject><subject>Shear strength</subject><subject>Solid phases</subject><subject>Structural analysis</subject><subject>Surface energy</subject><subject>Surface structure</subject><issn>1996-1944</issn><issn>1996-1944</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNpdkcFu1DAQhi0EolXphQdAkbggpLSe2ImdE6pWbVmpEoiFs-U4441LYi92gujb4-2WUhgfPLK_-e2Zn5DXQM8Ya-n5pEHQBljFnpFjaNumhJbz50_yI3Ka0i3NwRjIqn1JjpisOXAhjsn3tbfjgt5gEWwxD1hs0ATfl58HnbD4gsn5YjPHxcxLzIy_Z9Z-xmi1cXosNgPquEfQb-dhr7LSscvgleswnl_uwq-7g84r8sLqMeHpw35Cvl1dfl19LG8-Xa9XFzel4byZy66ve1kJKjl2tgbZAPRW2IZaY4zoUPc5pOyEFI1todW1taIVlTUoEEGzE_LhoLtbugl7g36OelS76CYd71TQTv17492gtuGnApplKkazwrsHhRh-LJhmNblkcBy1x7AkxShwCiBFndG3_6G3YYk-95epPHEmJW8zdXagtnpE5bwN-WGTV4-Ty_NG6_L5hZCyqimrIBe8PxSYGFKKaB-_D1TtjVd_jc_wm6cNP6J_bGa_AZiuqVA</recordid><startdate>20240313</startdate><enddate>20240313</enddate><creator>Liu, Hansong</creator><creator>Sun, Jinsong</creator><creator>Zhang, Lianwang</creator><creator>Liu, Zhaobo</creator><creator>Huang, Chengyu</creator><creator>Sun, Mingchen</creator><creator>Duan, Ziqi</creator><creator>Wang, Wenge</creator><creator>Zhong, Xiangyu</creator><creator>Bao, Jianwen</creator><general>MDPI AG</general><general>MDPI</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>7X8</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0003-4358-2576</orcidid></search><sort><creationdate>20240313</creationdate><title>Influence of the Second-Phase Resin Structure on the Interfacial Shear Strength of Carbon Fiber/Epoxy Resin</title><author>Liu, Hansong ; Sun, Jinsong ; Zhang, Lianwang ; Liu, Zhaobo ; Huang, Chengyu ; Sun, Mingchen ; Duan, Ziqi ; Wang, Wenge ; Zhong, Xiangyu ; Bao, Jianwen</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c446t-bd5d827084ebf518611df7f60fccc7beadddd88b7876f919a5ff7972fce7ee1a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Bonding strength</topic><topic>Carbon fiber reinforced plastics</topic><topic>Composite materials</topic><topic>Contact angle</topic><topic>Curing</topic><topic>Epoxy resins</topic><topic>Heat resistance</topic><topic>Interfacial bonding</topic><topic>Interfacial properties</topic><topic>Interfacial shear strength</topic><topic>Manufacturing</topic><topic>Shear strength</topic><topic>Solid phases</topic><topic>Structural analysis</topic><topic>Surface energy</topic><topic>Surface structure</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Liu, Hansong</creatorcontrib><creatorcontrib>Sun, Jinsong</creatorcontrib><creatorcontrib>Zhang, Lianwang</creatorcontrib><creatorcontrib>Liu, Zhaobo</creatorcontrib><creatorcontrib>Huang, Chengyu</creatorcontrib><creatorcontrib>Sun, Mingchen</creatorcontrib><creatorcontrib>Duan, Ziqi</creatorcontrib><creatorcontrib>Wang, Wenge</creatorcontrib><creatorcontrib>Zhong, Xiangyu</creatorcontrib><creatorcontrib>Bao, Jianwen</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Liu, Hansong</au><au>Sun, Jinsong</au><au>Zhang, Lianwang</au><au>Liu, Zhaobo</au><au>Huang, Chengyu</au><au>Sun, Mingchen</au><au>Duan, Ziqi</au><au>Wang, Wenge</au><au>Zhong, Xiangyu</au><au>Bao, Jianwen</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Influence of the Second-Phase Resin Structure on the Interfacial Shear Strength of Carbon Fiber/Epoxy Resin</atitle><jtitle>Materials</jtitle><addtitle>Materials (Basel)</addtitle><date>2024-03-13</date><risdate>2024</risdate><volume>17</volume><issue>6</issue><spage>1323</spage><pages>1323-</pages><issn>1996-1944</issn><eissn>1996-1944</eissn><abstract>The toughening modification of epoxy resin has received widespread attention. The addition of the second-phase resin has a good toughening effect on epoxy resin. In order to investigate the effect of the second-phase resin on the interphase of composites, in this work the interfacial properties of carbon fiber (CF)/epoxy resin with the second-phase resin structure were investigated. Methodologies including surface structure observation, chemical characteristics, surface energy of the CF, and micro-phase structure characterization of resin were tested, followed by the micro-interfacial performance of CF/epoxy composites before and after hygrothermal treatment. The results revealed that the sizing process has the positive effect of increasing the interfacial bonding properties of CF/epoxy. From the interfacial shear strength (IFSS) test, the introduction of the second phase in the resin reduced the interfacial bonding performance between the CF and epoxy. After the hygrothermal treatment, water molecules diffused along the interfacial paths between the two resins, which in turn created defects and consequently brought about a reduction in the IFSS.</abstract><cop>Switzerland</cop><pub>MDPI AG</pub><pmid>38541477</pmid><doi>10.3390/ma17061323</doi><orcidid>https://orcid.org/0000-0003-4358-2576</orcidid><oa>free_for_read</oa></addata></record> |
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source | Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; PubMed Central Open Access; MDPI - Multidisciplinary Digital Publishing Institute; PubMed Central; Free Full-Text Journals in Chemistry |
subjects | Bonding strength Carbon fiber reinforced plastics Composite materials Contact angle Curing Epoxy resins Heat resistance Interfacial bonding Interfacial properties Interfacial shear strength Manufacturing Shear strength Solid phases Structural analysis Surface energy Surface structure |
title | Influence of the Second-Phase Resin Structure on the Interfacial Shear Strength of Carbon Fiber/Epoxy Resin |
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