Effect of Heat Treatment on the Microstructure and Mechanical Properties of 18Ni-300 Maraging Steel Produced by Additive-Subtractive Hybrid Manufacturing

The present work investigates the effectiveness of two heat treatment cycles-solution treatment + aging (STA) and direct aging (DA)-on optimizing the microstructure and enhancing the mechanical properties of 18Ni-300 maraging steel (300 MS) produced by additive-subtractive hybrid manufacturing (ASHM...

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Veröffentlicht in:Materials 2023-06, Vol.16 (13), p.4749
Hauptverfasser: Osman, Mahmoud, Sarafan, Sheida, Wanjara, Priti, Bernier, Fabrice, Atabay, Sila Ece, Gholipour, Javad, Molavi-Zarandi, Marjan, Soost, Josh, Brochu, Mathieu
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container_title Materials
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creator Osman, Mahmoud
Sarafan, Sheida
Wanjara, Priti
Bernier, Fabrice
Atabay, Sila Ece
Gholipour, Javad
Molavi-Zarandi, Marjan
Soost, Josh
Brochu, Mathieu
description The present work investigates the effectiveness of two heat treatment cycles-solution treatment + aging (STA) and direct aging (DA)-on optimizing the microstructure and enhancing the mechanical properties of 18Ni-300 maraging steel (300 MS) produced by additive-subtractive hybrid manufacturing (ASHM). The STA treatment led to a fully martensitic microstructure with minor remnants of the cellular substructures associated with the solidification conditions in ASHM. DA resulted in some reverted austenite and partial dissolution of the cellular morphologies into shorter fragments. Despite the contrasting microstructures, the tensile strength and the macro- and micro-hardness were comparable between STA and DA conditions. By contrast, the potential for improving the ductility was higher with the DA heat treatment. This is attributed to the higher reverted austenite content in the samples treated by DA, i.e., up to a maximum of 13.4% compared to less than 3.0% in the STA samples. For the DA sample with the highest reverted austenite content of 13.4%, the highest local and global fracture strain values of 30.1 and 5.9 ± 0.6% were measured, while the respective values were 23.4 and 4.4 ± 0.1% for the corresponding STA sample. This work suggests that DA of 300 MS produced by ASHM is sufficient to achieve comparable hardness and tensile strength to STA, whilst maintaining reasonable ductility. Avoiding the solution treatment cycle, with its appreciably higher temperatures, could benefit the dimensional stability and surface quality that are important for ASHM of 300 MS parts.
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The STA treatment led to a fully martensitic microstructure with minor remnants of the cellular substructures associated with the solidification conditions in ASHM. DA resulted in some reverted austenite and partial dissolution of the cellular morphologies into shorter fragments. Despite the contrasting microstructures, the tensile strength and the macro- and micro-hardness were comparable between STA and DA conditions. By contrast, the potential for improving the ductility was higher with the DA heat treatment. This is attributed to the higher reverted austenite content in the samples treated by DA, i.e., up to a maximum of 13.4% compared to less than 3.0% in the STA samples. For the DA sample with the highest reverted austenite content of 13.4%, the highest local and global fracture strain values of 30.1 and 5.9 ± 0.6% were measured, while the respective values were 23.4 and 4.4 ± 0.1% for the corresponding STA sample. This work suggests that DA of 300 MS produced by ASHM is sufficient to achieve comparable hardness and tensile strength to STA, whilst maintaining reasonable ductility. Avoiding the solution treatment cycle, with its appreciably higher temperatures, could benefit the dimensional stability and surface quality that are important for ASHM of 300 MS parts.</description><identifier>ISSN: 1996-1944</identifier><identifier>EISSN: 1996-1944</identifier><identifier>DOI: 10.3390/ma16134749</identifier><identifier>PMID: 37445063</identifier><language>eng</language><publisher>Switzerland: MDPI AG</publisher><subject>Aging ; Alloys ; Austenite ; Dimensional stability ; Ductility ; Grain size ; Hardness ; Heat treating ; Intermetallic compounds ; Lasers ; Manufacturing ; Maraging steels ; Mechanical properties ; Microhardness ; Microstructure ; Particle size ; Solidification ; Solution heat treatment ; Surface properties ; Surface stability ; Tensile strength</subject><ispartof>Materials, 2023-06, Vol.16 (13), p.4749</ispartof><rights>COPYRIGHT 2023 MDPI AG</rights><rights>2023 by the National Research Council Canada. Licensee MDPI, Basel, Switzerland. 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The STA treatment led to a fully martensitic microstructure with minor remnants of the cellular substructures associated with the solidification conditions in ASHM. DA resulted in some reverted austenite and partial dissolution of the cellular morphologies into shorter fragments. Despite the contrasting microstructures, the tensile strength and the macro- and micro-hardness were comparable between STA and DA conditions. By contrast, the potential for improving the ductility was higher with the DA heat treatment. This is attributed to the higher reverted austenite content in the samples treated by DA, i.e., up to a maximum of 13.4% compared to less than 3.0% in the STA samples. For the DA sample with the highest reverted austenite content of 13.4%, the highest local and global fracture strain values of 30.1 and 5.9 ± 0.6% were measured, while the respective values were 23.4 and 4.4 ± 0.1% for the corresponding STA sample. 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The STA treatment led to a fully martensitic microstructure with minor remnants of the cellular substructures associated with the solidification conditions in ASHM. DA resulted in some reverted austenite and partial dissolution of the cellular morphologies into shorter fragments. Despite the contrasting microstructures, the tensile strength and the macro- and micro-hardness were comparable between STA and DA conditions. By contrast, the potential for improving the ductility was higher with the DA heat treatment. This is attributed to the higher reverted austenite content in the samples treated by DA, i.e., up to a maximum of 13.4% compared to less than 3.0% in the STA samples. For the DA sample with the highest reverted austenite content of 13.4%, the highest local and global fracture strain values of 30.1 and 5.9 ± 0.6% were measured, while the respective values were 23.4 and 4.4 ± 0.1% for the corresponding STA sample. This work suggests that DA of 300 MS produced by ASHM is sufficient to achieve comparable hardness and tensile strength to STA, whilst maintaining reasonable ductility. Avoiding the solution treatment cycle, with its appreciably higher temperatures, could benefit the dimensional stability and surface quality that are important for ASHM of 300 MS parts.</abstract><cop>Switzerland</cop><pub>MDPI AG</pub><pmid>37445063</pmid><doi>10.3390/ma16134749</doi><orcidid>https://orcid.org/0000-0003-2900-6249</orcidid><orcidid>https://orcid.org/0000-0001-5017-9596</orcidid><orcidid>https://orcid.org/0000-0001-5729-8045</orcidid><orcidid>https://orcid.org/0000-0001-7662-984X</orcidid><oa>free_for_read</oa></addata></record>
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subjects Aging
Alloys
Austenite
Dimensional stability
Ductility
Grain size
Hardness
Heat treating
Intermetallic compounds
Lasers
Manufacturing
Maraging steels
Mechanical properties
Microhardness
Microstructure
Particle size
Solidification
Solution heat treatment
Surface properties
Surface stability
Tensile strength
title Effect of Heat Treatment on the Microstructure and Mechanical Properties of 18Ni-300 Maraging Steel Produced by Additive-Subtractive Hybrid Manufacturing
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