Effect of Heat Treatment on the Microstructure and Mechanical Properties of 18Ni-300 Maraging Steel Produced by Additive-Subtractive Hybrid Manufacturing
The present work investigates the effectiveness of two heat treatment cycles-solution treatment + aging (STA) and direct aging (DA)-on optimizing the microstructure and enhancing the mechanical properties of 18Ni-300 maraging steel (300 MS) produced by additive-subtractive hybrid manufacturing (ASHM...
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description | The present work investigates the effectiveness of two heat treatment cycles-solution treatment + aging (STA) and direct aging (DA)-on optimizing the microstructure and enhancing the mechanical properties of 18Ni-300 maraging steel (300 MS) produced by additive-subtractive hybrid manufacturing (ASHM). The STA treatment led to a fully martensitic microstructure with minor remnants of the cellular substructures associated with the solidification conditions in ASHM. DA resulted in some reverted austenite and partial dissolution of the cellular morphologies into shorter fragments. Despite the contrasting microstructures, the tensile strength and the macro- and micro-hardness were comparable between STA and DA conditions. By contrast, the potential for improving the ductility was higher with the DA heat treatment. This is attributed to the higher reverted austenite content in the samples treated by DA, i.e., up to a maximum of 13.4% compared to less than 3.0% in the STA samples. For the DA sample with the highest reverted austenite content of 13.4%, the highest local and global fracture strain values of 30.1 and 5.9 ± 0.6% were measured, while the respective values were 23.4 and 4.4 ± 0.1% for the corresponding STA sample. This work suggests that DA of 300 MS produced by ASHM is sufficient to achieve comparable hardness and tensile strength to STA, whilst maintaining reasonable ductility. Avoiding the solution treatment cycle, with its appreciably higher temperatures, could benefit the dimensional stability and surface quality that are important for ASHM of 300 MS parts. |
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The STA treatment led to a fully martensitic microstructure with minor remnants of the cellular substructures associated with the solidification conditions in ASHM. DA resulted in some reverted austenite and partial dissolution of the cellular morphologies into shorter fragments. Despite the contrasting microstructures, the tensile strength and the macro- and micro-hardness were comparable between STA and DA conditions. By contrast, the potential for improving the ductility was higher with the DA heat treatment. This is attributed to the higher reverted austenite content in the samples treated by DA, i.e., up to a maximum of 13.4% compared to less than 3.0% in the STA samples. For the DA sample with the highest reverted austenite content of 13.4%, the highest local and global fracture strain values of 30.1 and 5.9 ± 0.6% were measured, while the respective values were 23.4 and 4.4 ± 0.1% for the corresponding STA sample. This work suggests that DA of 300 MS produced by ASHM is sufficient to achieve comparable hardness and tensile strength to STA, whilst maintaining reasonable ductility. Avoiding the solution treatment cycle, with its appreciably higher temperatures, could benefit the dimensional stability and surface quality that are important for ASHM of 300 MS parts.</description><identifier>ISSN: 1996-1944</identifier><identifier>EISSN: 1996-1944</identifier><identifier>DOI: 10.3390/ma16134749</identifier><identifier>PMID: 37445063</identifier><language>eng</language><publisher>Switzerland: MDPI AG</publisher><subject>Aging ; Alloys ; Austenite ; Dimensional stability ; Ductility ; Grain size ; Hardness ; Heat treating ; Intermetallic compounds ; Lasers ; Manufacturing ; Maraging steels ; Mechanical properties ; Microhardness ; Microstructure ; Particle size ; Solidification ; Solution heat treatment ; Surface properties ; Surface stability ; Tensile strength</subject><ispartof>Materials, 2023-06, Vol.16 (13), p.4749</ispartof><rights>COPYRIGHT 2023 MDPI AG</rights><rights>2023 by the National Research Council Canada. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>2023 by the National Research Council Canada. 2023</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c446t-cd2a848dd7212b42e94040ae378579917bd69a63a72aac87129bdd11d78697383</citedby><cites>FETCH-LOGICAL-c446t-cd2a848dd7212b42e94040ae378579917bd69a63a72aac87129bdd11d78697383</cites><orcidid>0000-0003-2900-6249 ; 0000-0001-5017-9596 ; 0000-0001-5729-8045 ; 0000-0001-7662-984X</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC10342934/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC10342934/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,727,780,784,885,27924,27925,53791,53793</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/37445063$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Osman, Mahmoud</creatorcontrib><creatorcontrib>Sarafan, Sheida</creatorcontrib><creatorcontrib>Wanjara, Priti</creatorcontrib><creatorcontrib>Bernier, Fabrice</creatorcontrib><creatorcontrib>Atabay, Sila Ece</creatorcontrib><creatorcontrib>Gholipour, Javad</creatorcontrib><creatorcontrib>Molavi-Zarandi, Marjan</creatorcontrib><creatorcontrib>Soost, Josh</creatorcontrib><creatorcontrib>Brochu, Mathieu</creatorcontrib><title>Effect of Heat Treatment on the Microstructure and Mechanical Properties of 18Ni-300 Maraging Steel Produced by Additive-Subtractive Hybrid Manufacturing</title><title>Materials</title><addtitle>Materials (Basel)</addtitle><description>The present work investigates the effectiveness of two heat treatment cycles-solution treatment + aging (STA) and direct aging (DA)-on optimizing the microstructure and enhancing the mechanical properties of 18Ni-300 maraging steel (300 MS) produced by additive-subtractive hybrid manufacturing (ASHM). The STA treatment led to a fully martensitic microstructure with minor remnants of the cellular substructures associated with the solidification conditions in ASHM. DA resulted in some reverted austenite and partial dissolution of the cellular morphologies into shorter fragments. Despite the contrasting microstructures, the tensile strength and the macro- and micro-hardness were comparable between STA and DA conditions. By contrast, the potential for improving the ductility was higher with the DA heat treatment. This is attributed to the higher reverted austenite content in the samples treated by DA, i.e., up to a maximum of 13.4% compared to less than 3.0% in the STA samples. For the DA sample with the highest reverted austenite content of 13.4%, the highest local and global fracture strain values of 30.1 and 5.9 ± 0.6% were measured, while the respective values were 23.4 and 4.4 ± 0.1% for the corresponding STA sample. This work suggests that DA of 300 MS produced by ASHM is sufficient to achieve comparable hardness and tensile strength to STA, whilst maintaining reasonable ductility. Avoiding the solution treatment cycle, with its appreciably higher temperatures, could benefit the dimensional stability and surface quality that are important for ASHM of 300 MS parts.</description><subject>Aging</subject><subject>Alloys</subject><subject>Austenite</subject><subject>Dimensional stability</subject><subject>Ductility</subject><subject>Grain size</subject><subject>Hardness</subject><subject>Heat treating</subject><subject>Intermetallic compounds</subject><subject>Lasers</subject><subject>Manufacturing</subject><subject>Maraging steels</subject><subject>Mechanical properties</subject><subject>Microhardness</subject><subject>Microstructure</subject><subject>Particle size</subject><subject>Solidification</subject><subject>Solution heat treatment</subject><subject>Surface properties</subject><subject>Surface stability</subject><subject>Tensile strength</subject><issn>1996-1944</issn><issn>1996-1944</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNpdkm1rFDEQxxdRbKl94weQgG-ksDVPt0leyVGqJ_RUaH29zCazdym72TObLdxH8dua9fqkCWSGyW_-ySRTFG8ZPRfC0I89sIoJqaR5URwzY6qSGSlfPvOPitNxvKV5CME0N6-LI6GkXNBKHBe_L9sWbSJDS1YIidzEvPYYciSQtEWy9jYOY4qTTVNEAsGRNdotBG-hIz_isMOYPI6zAtPffCkoJWuIsPFhQ64T4l_KTRYdafZk6ZxP_g7L66lJEezsk9W-iT4LQ5hamA_KuW-KVy10I57e25Pi5-fLm4tVefX9y9eL5VVppaxSaR0HLbVzijPeSI5GUkkBhdILZQxTjasMVAIUB7BaMW4a5xhzSldGCS1Oik8H3d3U9Ohsrj1CV--i7yHu6wF8_e9O8Nt6M9zVjArJjZBZ4cO9Qhx-TTimuvejxa6DgMM01lwLzaXhSmT0_X_o7TDFkOubqUpWFZU8U-cHagMd1j60w_xSeTrsvR0Ctj7Hl2qhhVnQBcsJZ4eE-a_GiO3j9Rmt5zapn9okw--eF_yIPjSF-APB8bgR</recordid><startdate>20230630</startdate><enddate>20230630</enddate><creator>Osman, Mahmoud</creator><creator>Sarafan, Sheida</creator><creator>Wanjara, Priti</creator><creator>Bernier, Fabrice</creator><creator>Atabay, Sila Ece</creator><creator>Gholipour, Javad</creator><creator>Molavi-Zarandi, Marjan</creator><creator>Soost, Josh</creator><creator>Brochu, Mathieu</creator><general>MDPI AG</general><general>MDPI</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>7X8</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0003-2900-6249</orcidid><orcidid>https://orcid.org/0000-0001-5017-9596</orcidid><orcidid>https://orcid.org/0000-0001-5729-8045</orcidid><orcidid>https://orcid.org/0000-0001-7662-984X</orcidid></search><sort><creationdate>20230630</creationdate><title>Effect of Heat Treatment on the Microstructure and Mechanical Properties of 18Ni-300 Maraging Steel Produced by Additive-Subtractive Hybrid Manufacturing</title><author>Osman, Mahmoud ; 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The STA treatment led to a fully martensitic microstructure with minor remnants of the cellular substructures associated with the solidification conditions in ASHM. DA resulted in some reverted austenite and partial dissolution of the cellular morphologies into shorter fragments. Despite the contrasting microstructures, the tensile strength and the macro- and micro-hardness were comparable between STA and DA conditions. By contrast, the potential for improving the ductility was higher with the DA heat treatment. This is attributed to the higher reverted austenite content in the samples treated by DA, i.e., up to a maximum of 13.4% compared to less than 3.0% in the STA samples. For the DA sample with the highest reverted austenite content of 13.4%, the highest local and global fracture strain values of 30.1 and 5.9 ± 0.6% were measured, while the respective values were 23.4 and 4.4 ± 0.1% for the corresponding STA sample. This work suggests that DA of 300 MS produced by ASHM is sufficient to achieve comparable hardness and tensile strength to STA, whilst maintaining reasonable ductility. Avoiding the solution treatment cycle, with its appreciably higher temperatures, could benefit the dimensional stability and surface quality that are important for ASHM of 300 MS parts.</abstract><cop>Switzerland</cop><pub>MDPI AG</pub><pmid>37445063</pmid><doi>10.3390/ma16134749</doi><orcidid>https://orcid.org/0000-0003-2900-6249</orcidid><orcidid>https://orcid.org/0000-0001-5017-9596</orcidid><orcidid>https://orcid.org/0000-0001-5729-8045</orcidid><orcidid>https://orcid.org/0000-0001-7662-984X</orcidid><oa>free_for_read</oa></addata></record> |
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subjects | Aging Alloys Austenite Dimensional stability Ductility Grain size Hardness Heat treating Intermetallic compounds Lasers Manufacturing Maraging steels Mechanical properties Microhardness Microstructure Particle size Solidification Solution heat treatment Surface properties Surface stability Tensile strength |
title | Effect of Heat Treatment on the Microstructure and Mechanical Properties of 18Ni-300 Maraging Steel Produced by Additive-Subtractive Hybrid Manufacturing |
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