Selected advances in small‐angle scattering and applications they serve in manufacturing, energy and climate change
Innovations in small‐angle X‐ray and neutron scattering (SAXS and SANS) at major X‐ray and neutron facilities offer new characterization tools for researching materials phenomena relevant to advanced applications. For SAXS, the new generation of diffraction‐limited storage rings, incorporating multi...
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| Veröffentlicht in: | Journal of applied crystallography 2023-06, Vol.56 (3), p.787-800 |
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| description | Innovations in small‐angle X‐ray and neutron scattering (SAXS and SANS) at major X‐ray and neutron facilities offer new characterization tools for researching materials phenomena relevant to advanced applications. For SAXS, the new generation of diffraction‐limited storage rings, incorporating multi‐bend achromat concepts, dramatically decrease electron beam emittance and significantly increase X‐ray brilliance over previous third‐generation sources. This results in intense X‐ray incident beams that are more compact in the horizontal plane, allowing significantly improved spatial resolution, better time resolution, and a new era for coherent‐beam SAXS methods such as X‐ray photon correlation spectroscopy. Elsewhere, X‐ray free‐electron laser sources provide extremely bright, fully coherent, X‐ray pulses of |
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Selected recent advances in small‐angle X‐ray and neutron scattering are highlighted, together with some of the hard material applications they serve in the areas of manufacturing, energy and climate change. This paper is associated with work presented at the 18th International Conference on Small‐Angle Scattering, Campinas, Brazil, September 2022 (SAS 2022).</description><identifier>ISSN: 1600-5767</identifier><identifier>ISSN: 0021-8898</identifier><identifier>EISSN: 1600-5767</identifier><identifier>DOI: 10.1107/S1600576723003898</identifier><identifier>PMID: 37284276</identifier><language>eng</language><publisher>5 Abbey Square, Chester, Cheshire CH1 2HU, England: International Union of Crystallography</publisher><subject>advanced manufacturing ; carbon dioxide reduction ; Carriages ; Climate change ; Data collection ; Electron beams ; Emittance ; energy applications ; Manufacturing ; MATERIALS SCIENCE ; microstructure characterization ; Neutron diffraction ; Neutron scattering ; Neutron sources ; Neutrons ; Optics ; Photon correlation spectroscopy ; Research Papers ; Small angle X ray scattering ; small-angle neutron scattering ; Spallation ; Spatial discrimination ; Spatial resolution ; Spectroscopy ; Storage rings (particle accelerators) ; Structural analysis</subject><ispartof>Journal of applied crystallography, 2023-06, Vol.56 (3), p.787-800</ispartof><rights>2023 Andrew J. Allen. published by IUCr Journals.</rights><rights>Andrew J. Allen 2023.</rights><rights>2023. This article is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>Andrew J. Allen 2023 2023</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a5282-bf5d3ebbcb85d19b4e03b8fed30ab869177a7f14689398e26288b2a3b7e2761e3</citedby><cites>FETCH-LOGICAL-a5282-bf5d3ebbcb85d19b4e03b8fed30ab869177a7f14689398e26288b2a3b7e2761e3</cites><orcidid>0000-0002-6496-8411 ; 0000000264968411</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1107%2FS1600576723003898$$EPDF$$P50$$Gwiley$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1107%2FS1600576723003898$$EHTML$$P50$$Gwiley$$Hfree_for_read</linktohtml><link.rule.ids>230,314,776,780,881,1411,27901,27902,45550,45551</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/37284276$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink><backlink>$$Uhttps://www.osti.gov/biblio/1975564$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Allen, Andrew J.</creatorcontrib><creatorcontrib>Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)</creatorcontrib><title>Selected advances in small‐angle scattering and applications they serve in manufacturing, energy and climate change</title><title>Journal of applied crystallography</title><addtitle>J Appl Crystallogr</addtitle><description>Innovations in small‐angle X‐ray and neutron scattering (SAXS and SANS) at major X‐ray and neutron facilities offer new characterization tools for researching materials phenomena relevant to advanced applications. For SAXS, the new generation of diffraction‐limited storage rings, incorporating multi‐bend achromat concepts, dramatically decrease electron beam emittance and significantly increase X‐ray brilliance over previous third‐generation sources. This results in intense X‐ray incident beams that are more compact in the horizontal plane, allowing significantly improved spatial resolution, better time resolution, and a new era for coherent‐beam SAXS methods such as X‐ray photon correlation spectroscopy. Elsewhere, X‐ray free‐electron laser sources provide extremely bright, fully coherent, X‐ray pulses of <100 fs and can support SAXS studies of material processes where entire SAXS data sets are collected in a single pulse train. Meanwhile, SANS at both steady‐state reactor and pulsed spallation neutron sources has significantly evolved. Developments in neutron optics and multiple detector carriages now enable data collection in a few minutes for materials characterization over nanometre‐to‐micrometre scale ranges, opening up real‐time studies of multi‐scale materials phenomena. SANS at pulsed neutron sources is becoming more integrated with neutron diffraction methods for simultaneous structure characterization of complex materials. In this paper, selected developments are highlighted and some recent state‐of‐the‐art studies discussed, relevant to hard matter applications in advanced manufacturing, energy and climate change.
Selected recent advances in small‐angle X‐ray and neutron scattering are highlighted, together with some of the hard material applications they serve in the areas of manufacturing, energy and climate change. This paper is associated with work presented at the 18th International Conference on Small‐Angle Scattering, Campinas, Brazil, September 2022 (SAS 2022).</description><subject>advanced manufacturing</subject><subject>carbon dioxide reduction</subject><subject>Carriages</subject><subject>Climate change</subject><subject>Data collection</subject><subject>Electron beams</subject><subject>Emittance</subject><subject>energy applications</subject><subject>Manufacturing</subject><subject>MATERIALS SCIENCE</subject><subject>microstructure characterization</subject><subject>Neutron diffraction</subject><subject>Neutron scattering</subject><subject>Neutron sources</subject><subject>Neutrons</subject><subject>Optics</subject><subject>Photon correlation spectroscopy</subject><subject>Research Papers</subject><subject>Small angle X ray scattering</subject><subject>small-angle neutron scattering</subject><subject>Spallation</subject><subject>Spatial discrimination</subject><subject>Spatial resolution</subject><subject>Spectroscopy</subject><subject>Storage rings (particle accelerators)</subject><subject>Structural analysis</subject><issn>1600-5767</issn><issn>0021-8898</issn><issn>1600-5767</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>24P</sourceid><recordid>eNqFkc1u1DAUhS1ERUvhAdggCzYsGPBPEjsrhEZAiyohUWZt2c7NjCvHGWxn0Ox4BJ6RJ8HplKrAgpWt6-8c33MvQk8oeUUpEa8vaUNILRrBOCFctvIeOplLi7l2_879GD1M6YoQWlD2AB1zwWTFRHOCpkvwYDN0WHc7HSwk7AJOg_b-5_cfOqw94GR1zhBdWGMdCrjdeldKbgwJ5w3scYK4g1k36DD12uZphl9iCBDX-2uR9W7QGbDdFE94hI567RM8vjlP0er9uy_Ls8XFpw_ny7cXC10zyRamrzsOxlgj6462pgLCjeyh40Qb2bRUCC16WjWy5a0E1jApDdPcCCjhKPBT9Obgu53MAJ2FkKP2ahtLM3GvRu3Uny_BbdR63ClKWEXLaIvDs4PDmLJTyboMdmPHEMrQFG1FXTdVgV7cfBPHrxOkrAaXLHivA4xTUiULr9qWkdnv-V_o1TjFUIYwU4wJJkRdKHqgbBxTitDftkyJmlev_ll90Ty9m_VW8XvXBWgPwDfnYf9_R_Vx-ZmtVjUhjP8CeRG76A</recordid><startdate>202306</startdate><enddate>202306</enddate><creator>Allen, Andrew J.</creator><general>International Union of Crystallography</general><general>Blackwell Publishing Ltd</general><scope>24P</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><scope>7X8</scope><scope>OTOTI</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0002-6496-8411</orcidid><orcidid>https://orcid.org/0000000264968411</orcidid></search><sort><creationdate>202306</creationdate><title>Selected advances in small‐angle scattering and applications they serve in manufacturing, energy and climate change</title><author>Allen, Andrew J.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a5282-bf5d3ebbcb85d19b4e03b8fed30ab869177a7f14689398e26288b2a3b7e2761e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>advanced manufacturing</topic><topic>carbon dioxide reduction</topic><topic>Carriages</topic><topic>Climate change</topic><topic>Data collection</topic><topic>Electron beams</topic><topic>Emittance</topic><topic>energy applications</topic><topic>Manufacturing</topic><topic>MATERIALS SCIENCE</topic><topic>microstructure characterization</topic><topic>Neutron diffraction</topic><topic>Neutron scattering</topic><topic>Neutron sources</topic><topic>Neutrons</topic><topic>Optics</topic><topic>Photon correlation spectroscopy</topic><topic>Research Papers</topic><topic>Small angle X ray scattering</topic><topic>small-angle neutron scattering</topic><topic>Spallation</topic><topic>Spatial discrimination</topic><topic>Spatial resolution</topic><topic>Spectroscopy</topic><topic>Storage rings (particle accelerators)</topic><topic>Structural analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Allen, Andrew J.</creatorcontrib><creatorcontrib>Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)</creatorcontrib><collection>Wiley Online Library Open Access</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><collection>OSTI.GOV</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Journal of applied crystallography</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Allen, Andrew J.</au><aucorp>Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Selected advances in small‐angle scattering and applications they serve in manufacturing, energy and climate change</atitle><jtitle>Journal of applied crystallography</jtitle><addtitle>J Appl Crystallogr</addtitle><date>2023-06</date><risdate>2023</risdate><volume>56</volume><issue>3</issue><spage>787</spage><epage>800</epage><pages>787-800</pages><issn>1600-5767</issn><issn>0021-8898</issn><eissn>1600-5767</eissn><abstract>Innovations in small‐angle X‐ray and neutron scattering (SAXS and SANS) at major X‐ray and neutron facilities offer new characterization tools for researching materials phenomena relevant to advanced applications. For SAXS, the new generation of diffraction‐limited storage rings, incorporating multi‐bend achromat concepts, dramatically decrease electron beam emittance and significantly increase X‐ray brilliance over previous third‐generation sources. This results in intense X‐ray incident beams that are more compact in the horizontal plane, allowing significantly improved spatial resolution, better time resolution, and a new era for coherent‐beam SAXS methods such as X‐ray photon correlation spectroscopy. Elsewhere, X‐ray free‐electron laser sources provide extremely bright, fully coherent, X‐ray pulses of <100 fs and can support SAXS studies of material processes where entire SAXS data sets are collected in a single pulse train. Meanwhile, SANS at both steady‐state reactor and pulsed spallation neutron sources has significantly evolved. Developments in neutron optics and multiple detector carriages now enable data collection in a few minutes for materials characterization over nanometre‐to‐micrometre scale ranges, opening up real‐time studies of multi‐scale materials phenomena. SANS at pulsed neutron sources is becoming more integrated with neutron diffraction methods for simultaneous structure characterization of complex materials. In this paper, selected developments are highlighted and some recent state‐of‐the‐art studies discussed, relevant to hard matter applications in advanced manufacturing, energy and climate change.
Selected recent advances in small‐angle X‐ray and neutron scattering are highlighted, together with some of the hard material applications they serve in the areas of manufacturing, energy and climate change. This paper is associated with work presented at the 18th International Conference on Small‐Angle Scattering, Campinas, Brazil, September 2022 (SAS 2022).</abstract><cop>5 Abbey Square, Chester, Cheshire CH1 2HU, England</cop><pub>International Union of Crystallography</pub><pmid>37284276</pmid><doi>10.1107/S1600576723003898</doi><tpages>14</tpages><orcidid>https://orcid.org/0000-0002-6496-8411</orcidid><orcidid>https://orcid.org/0000000264968411</orcidid><oa>free_for_read</oa></addata></record> |
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| ispartof | Journal of applied crystallography, 2023-06, Vol.56 (3), p.787-800 |
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| source | Wiley Online Library Journals Frontfile Complete; Alma/SFX Local Collection |
| subjects | advanced manufacturing carbon dioxide reduction Carriages Climate change Data collection Electron beams Emittance energy applications Manufacturing MATERIALS SCIENCE microstructure characterization Neutron diffraction Neutron scattering Neutron sources Neutrons Optics Photon correlation spectroscopy Research Papers Small angle X ray scattering small-angle neutron scattering Spallation Spatial discrimination Spatial resolution Spectroscopy Storage rings (particle accelerators) Structural analysis |
| title | Selected advances in small‐angle scattering and applications they serve in manufacturing, energy and climate change |
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