Effects of Electron Beam Irradiation on Mechanical and Tribological Properties of PEEK
In this work, the mechanical and tribological characteristics of polyetheretherketone (PEEK) sheets were enhanced by electron beam irradiation. PEEK sheets irradiated at a speed of 0.8 m/min with a total dose of 200 kGy achieved the lowest specific wear rate of 4.57 ± 0.69 (10 mm /N m ), compared to...
Gespeichert in:
| Veröffentlicht in: | Polymers 2023-03, Vol.15 (6), p.1340 |
|---|---|
| Hauptverfasser: | , , , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | |
|---|---|
| container_issue | 6 |
| container_start_page | 1340 |
| container_title | Polymers |
| container_volume | 15 |
| creator | Kurbanova, Bayan Aimaganbetov, Kazybek Ospanov, Kanat Abdrakhmanov, Kairat Zhakiyev, Nurkhat Rakhadilov, Bauyrzhan Sagdoldina, Zhuldyz Almas, Nurlan |
| description | In this work, the mechanical and tribological characteristics of polyetheretherketone (PEEK) sheets were enhanced by electron beam irradiation. PEEK sheets irradiated at a speed of 0.8 m/min with a total dose of 200 kGy achieved the lowest specific wear rate of 4.57 ± 0.69 (10
mm
/N
m
), compared to unirradiated PEEK with a rate of 13.1 ± 0.42 (10
mm
/N
m
). Exposure to an electron beam at 9 m/min for 30 runs, with a dose of 10 kGy per run for a total dose of 300 kGy, resulted in the highest improvement in microhardness, reaching 0.222 GPa. This may be due to the decrease in crystallite size, as indicated by the broadening of the diffraction peaks in the irradiated samples. According to the results of thermogravimetric analysis, the degradation temperature of the irradiated samples remained unchanged at 553 ± 0.5 °C, except a sample irradiated at dose 400 kGy, where the degradation temperature shifted towards a lower position of 544 ± 0.5 °C. Differential scanning calorimetry results revealed that the melting temperature (Tm) of the unirradiated PEEK was about 338 ± 0.5 °C, while a high temperature shift of the Tm was observed for the irradiated samples. |
| doi_str_mv | 10.3390/polym15061340 |
| format | Article |
| fullrecord | <record><control><sourceid>gale_pubme</sourceid><recordid>TN_cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_10051403</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><galeid>A743770526</galeid><sourcerecordid>A743770526</sourcerecordid><originalsourceid>FETCH-LOGICAL-c411t-e334d0752a43b7a3942d3003ffce1ce9214aa2a31abc4f0c8ece0449274c5b3d3</originalsourceid><addsrcrecordid>eNpdkU1v1DAQhi0EolXpkSuKxIVLir8Sr0-oVAEqiuihcLUmznjryrEXO1up_x5vt1QttqUZvX7mtUdDyFtGT4TQ9OMmhbuZdbRnQtIX5JBTJVopevrySX5Ajku5oXXJru-Zek0ORK9XinF2SH4PzqFdSpNcM4Sa5RSbzwhzc54zTB4WX4V6fqC9hugthAbi1FxlP6aQ1vfCZU4bzIvHe5vLYfj-hrxyEAoeP8Qj8uvLcHX2rb34-fX87PSitZKxpUUh5ERVx0GKUYHQkk-CUuGcRWZRcyYBOAgGo5WO2hVapFJqrqTtRjGJI_Jp77vZjjNOFuOSIZhN9jPkO5PAm-c30V-bdbo1jNKOSSqqw4cHh5z-bLEsZvbFYggQMW2L4UpzqRXTvKLv_0Nv0jbH2t-OYr3uVv2OOtlTawhofHSpPmzrnnD2NkV0vuqnSgqlaMf7WtDuC2xOpWR0j99n1OzGbJ6NufLvnvb8SP8bqvgLI96i8Q</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2791695862</pqid></control><display><type>article</type><title>Effects of Electron Beam Irradiation on Mechanical and Tribological Properties of PEEK</title><source>MDPI - Multidisciplinary Digital Publishing Institute</source><source>Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals</source><source>PubMed Central</source><source>PubMed Central Open Access</source><creator>Kurbanova, Bayan ; Aimaganbetov, Kazybek ; Ospanov, Kanat ; Abdrakhmanov, Kairat ; Zhakiyev, Nurkhat ; Rakhadilov, Bauyrzhan ; Sagdoldina, Zhuldyz ; Almas, Nurlan</creator><creatorcontrib>Kurbanova, Bayan ; Aimaganbetov, Kazybek ; Ospanov, Kanat ; Abdrakhmanov, Kairat ; Zhakiyev, Nurkhat ; Rakhadilov, Bauyrzhan ; Sagdoldina, Zhuldyz ; Almas, Nurlan</creatorcontrib><description>In this work, the mechanical and tribological characteristics of polyetheretherketone (PEEK) sheets were enhanced by electron beam irradiation. PEEK sheets irradiated at a speed of 0.8 m/min with a total dose of 200 kGy achieved the lowest specific wear rate of 4.57 ± 0.69 (10
mm
/N
m
), compared to unirradiated PEEK with a rate of 13.1 ± 0.42 (10
mm
/N
m
). Exposure to an electron beam at 9 m/min for 30 runs, with a dose of 10 kGy per run for a total dose of 300 kGy, resulted in the highest improvement in microhardness, reaching 0.222 GPa. This may be due to the decrease in crystallite size, as indicated by the broadening of the diffraction peaks in the irradiated samples. According to the results of thermogravimetric analysis, the degradation temperature of the irradiated samples remained unchanged at 553 ± 0.5 °C, except a sample irradiated at dose 400 kGy, where the degradation temperature shifted towards a lower position of 544 ± 0.5 °C. Differential scanning calorimetry results revealed that the melting temperature (Tm) of the unirradiated PEEK was about 338 ± 0.5 °C, while a high temperature shift of the Tm was observed for the irradiated samples.</description><identifier>ISSN: 2073-4360</identifier><identifier>EISSN: 2073-4360</identifier><identifier>DOI: 10.3390/polym15061340</identifier><identifier>PMID: 36987121</identifier><language>eng</language><publisher>Switzerland: MDPI AG</publisher><subject>Analysis ; Crystallites ; Degradation ; Electric fields ; Electron beams ; Electron irradiation ; Energy ; Friction ; Gamma rays ; High temperature ; Influence ; Irradiation ; Mechanical properties ; Melt temperature ; Microhardness ; Polyether ether ketones ; Polyetheretherketone ; Polymers ; Radiation ; Sheets ; Temperature ; Tensile strength ; Thermogravimetric analysis ; Tribology ; Viscoelasticity ; Wear rate</subject><ispartof>Polymers, 2023-03, Vol.15 (6), p.1340</ispartof><rights>COPYRIGHT 2023 MDPI AG</rights><rights>2023 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><rights>2023 by the authors. 2023</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c411t-e334d0752a43b7a3942d3003ffce1ce9214aa2a31abc4f0c8ece0449274c5b3d3</cites><orcidid>0000-0003-0928-521X ; 0000-0002-4904-2047 ; 0000-0001-6367-9135 ; 0000-0002-4154-1191 ; 0000-0003-2183-3389</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC10051403/pdf/$$EPDF$$P50$$Gpubmedcentral$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.ncbi.nlm.nih.gov/pmc/articles/PMC10051403/$$EHTML$$P50$$Gpubmedcentral$$Hfree_for_read</linktohtml><link.rule.ids>230,314,723,776,780,881,27901,27902,53766,53768</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/36987121$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Kurbanova, Bayan</creatorcontrib><creatorcontrib>Aimaganbetov, Kazybek</creatorcontrib><creatorcontrib>Ospanov, Kanat</creatorcontrib><creatorcontrib>Abdrakhmanov, Kairat</creatorcontrib><creatorcontrib>Zhakiyev, Nurkhat</creatorcontrib><creatorcontrib>Rakhadilov, Bauyrzhan</creatorcontrib><creatorcontrib>Sagdoldina, Zhuldyz</creatorcontrib><creatorcontrib>Almas, Nurlan</creatorcontrib><title>Effects of Electron Beam Irradiation on Mechanical and Tribological Properties of PEEK</title><title>Polymers</title><addtitle>Polymers (Basel)</addtitle><description>In this work, the mechanical and tribological characteristics of polyetheretherketone (PEEK) sheets were enhanced by electron beam irradiation. PEEK sheets irradiated at a speed of 0.8 m/min with a total dose of 200 kGy achieved the lowest specific wear rate of 4.57 ± 0.69 (10
mm
/N
m
), compared to unirradiated PEEK with a rate of 13.1 ± 0.42 (10
mm
/N
m
). Exposure to an electron beam at 9 m/min for 30 runs, with a dose of 10 kGy per run for a total dose of 300 kGy, resulted in the highest improvement in microhardness, reaching 0.222 GPa. This may be due to the decrease in crystallite size, as indicated by the broadening of the diffraction peaks in the irradiated samples. According to the results of thermogravimetric analysis, the degradation temperature of the irradiated samples remained unchanged at 553 ± 0.5 °C, except a sample irradiated at dose 400 kGy, where the degradation temperature shifted towards a lower position of 544 ± 0.5 °C. Differential scanning calorimetry results revealed that the melting temperature (Tm) of the unirradiated PEEK was about 338 ± 0.5 °C, while a high temperature shift of the Tm was observed for the irradiated samples.</description><subject>Analysis</subject><subject>Crystallites</subject><subject>Degradation</subject><subject>Electric fields</subject><subject>Electron beams</subject><subject>Electron irradiation</subject><subject>Energy</subject><subject>Friction</subject><subject>Gamma rays</subject><subject>High temperature</subject><subject>Influence</subject><subject>Irradiation</subject><subject>Mechanical properties</subject><subject>Melt temperature</subject><subject>Microhardness</subject><subject>Polyether ether ketones</subject><subject>Polyetheretherketone</subject><subject>Polymers</subject><subject>Radiation</subject><subject>Sheets</subject><subject>Temperature</subject><subject>Tensile strength</subject><subject>Thermogravimetric analysis</subject><subject>Tribology</subject><subject>Viscoelasticity</subject><subject>Wear rate</subject><issn>2073-4360</issn><issn>2073-4360</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNpdkU1v1DAQhi0EolXpkSuKxIVLir8Sr0-oVAEqiuihcLUmznjryrEXO1up_x5vt1QttqUZvX7mtUdDyFtGT4TQ9OMmhbuZdbRnQtIX5JBTJVopevrySX5Ajku5oXXJru-Zek0ORK9XinF2SH4PzqFdSpNcM4Sa5RSbzwhzc54zTB4WX4V6fqC9hugthAbi1FxlP6aQ1vfCZU4bzIvHe5vLYfj-hrxyEAoeP8Qj8uvLcHX2rb34-fX87PSitZKxpUUh5ERVx0GKUYHQkk-CUuGcRWZRcyYBOAgGo5WO2hVapFJqrqTtRjGJI_Jp77vZjjNOFuOSIZhN9jPkO5PAm-c30V-bdbo1jNKOSSqqw4cHh5z-bLEsZvbFYggQMW2L4UpzqRXTvKLv_0Nv0jbH2t-OYr3uVv2OOtlTawhofHSpPmzrnnD2NkV0vuqnSgqlaMf7WtDuC2xOpWR0j99n1OzGbJ6NufLvnvb8SP8bqvgLI96i8Q</recordid><startdate>20230307</startdate><enddate>20230307</enddate><creator>Kurbanova, Bayan</creator><creator>Aimaganbetov, Kazybek</creator><creator>Ospanov, Kanat</creator><creator>Abdrakhmanov, Kairat</creator><creator>Zhakiyev, Nurkhat</creator><creator>Rakhadilov, Bauyrzhan</creator><creator>Sagdoldina, Zhuldyz</creator><creator>Almas, Nurlan</creator><general>MDPI AG</general><general>MDPI</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>7X8</scope><scope>5PM</scope><orcidid>https://orcid.org/0000-0003-0928-521X</orcidid><orcidid>https://orcid.org/0000-0002-4904-2047</orcidid><orcidid>https://orcid.org/0000-0001-6367-9135</orcidid><orcidid>https://orcid.org/0000-0002-4154-1191</orcidid><orcidid>https://orcid.org/0000-0003-2183-3389</orcidid></search><sort><creationdate>20230307</creationdate><title>Effects of Electron Beam Irradiation on Mechanical and Tribological Properties of PEEK</title><author>Kurbanova, Bayan ; Aimaganbetov, Kazybek ; Ospanov, Kanat ; Abdrakhmanov, Kairat ; Zhakiyev, Nurkhat ; Rakhadilov, Bauyrzhan ; Sagdoldina, Zhuldyz ; Almas, Nurlan</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c411t-e334d0752a43b7a3942d3003ffce1ce9214aa2a31abc4f0c8ece0449274c5b3d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Analysis</topic><topic>Crystallites</topic><topic>Degradation</topic><topic>Electric fields</topic><topic>Electron beams</topic><topic>Electron irradiation</topic><topic>Energy</topic><topic>Friction</topic><topic>Gamma rays</topic><topic>High temperature</topic><topic>Influence</topic><topic>Irradiation</topic><topic>Mechanical properties</topic><topic>Melt temperature</topic><topic>Microhardness</topic><topic>Polyether ether ketones</topic><topic>Polyetheretherketone</topic><topic>Polymers</topic><topic>Radiation</topic><topic>Sheets</topic><topic>Temperature</topic><topic>Tensile strength</topic><topic>Thermogravimetric analysis</topic><topic>Tribology</topic><topic>Viscoelasticity</topic><topic>Wear rate</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kurbanova, Bayan</creatorcontrib><creatorcontrib>Aimaganbetov, Kazybek</creatorcontrib><creatorcontrib>Ospanov, Kanat</creatorcontrib><creatorcontrib>Abdrakhmanov, Kairat</creatorcontrib><creatorcontrib>Zhakiyev, Nurkhat</creatorcontrib><creatorcontrib>Rakhadilov, Bauyrzhan</creatorcontrib><creatorcontrib>Sagdoldina, Zhuldyz</creatorcontrib><creatorcontrib>Almas, Nurlan</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>MEDLINE - Academic</collection><collection>PubMed Central (Full Participant titles)</collection><jtitle>Polymers</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kurbanova, Bayan</au><au>Aimaganbetov, Kazybek</au><au>Ospanov, Kanat</au><au>Abdrakhmanov, Kairat</au><au>Zhakiyev, Nurkhat</au><au>Rakhadilov, Bauyrzhan</au><au>Sagdoldina, Zhuldyz</au><au>Almas, Nurlan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effects of Electron Beam Irradiation on Mechanical and Tribological Properties of PEEK</atitle><jtitle>Polymers</jtitle><addtitle>Polymers (Basel)</addtitle><date>2023-03-07</date><risdate>2023</risdate><volume>15</volume><issue>6</issue><spage>1340</spage><pages>1340-</pages><issn>2073-4360</issn><eissn>2073-4360</eissn><abstract>In this work, the mechanical and tribological characteristics of polyetheretherketone (PEEK) sheets were enhanced by electron beam irradiation. PEEK sheets irradiated at a speed of 0.8 m/min with a total dose of 200 kGy achieved the lowest specific wear rate of 4.57 ± 0.69 (10
mm
/N
m
), compared to unirradiated PEEK with a rate of 13.1 ± 0.42 (10
mm
/N
m
). Exposure to an electron beam at 9 m/min for 30 runs, with a dose of 10 kGy per run for a total dose of 300 kGy, resulted in the highest improvement in microhardness, reaching 0.222 GPa. This may be due to the decrease in crystallite size, as indicated by the broadening of the diffraction peaks in the irradiated samples. According to the results of thermogravimetric analysis, the degradation temperature of the irradiated samples remained unchanged at 553 ± 0.5 °C, except a sample irradiated at dose 400 kGy, where the degradation temperature shifted towards a lower position of 544 ± 0.5 °C. Differential scanning calorimetry results revealed that the melting temperature (Tm) of the unirradiated PEEK was about 338 ± 0.5 °C, while a high temperature shift of the Tm was observed for the irradiated samples.</abstract><cop>Switzerland</cop><pub>MDPI AG</pub><pmid>36987121</pmid><doi>10.3390/polym15061340</doi><orcidid>https://orcid.org/0000-0003-0928-521X</orcidid><orcidid>https://orcid.org/0000-0002-4904-2047</orcidid><orcidid>https://orcid.org/0000-0001-6367-9135</orcidid><orcidid>https://orcid.org/0000-0002-4154-1191</orcidid><orcidid>https://orcid.org/0000-0003-2183-3389</orcidid><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 2073-4360 |
| ispartof | Polymers, 2023-03, Vol.15 (6), p.1340 |
| issn | 2073-4360 2073-4360 |
| language | eng |
| recordid | cdi_pubmedcentral_primary_oai_pubmedcentral_nih_gov_10051403 |
| source | MDPI - Multidisciplinary Digital Publishing Institute; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; PubMed Central; PubMed Central Open Access |
| subjects | Analysis Crystallites Degradation Electric fields Electron beams Electron irradiation Energy Friction Gamma rays High temperature Influence Irradiation Mechanical properties Melt temperature Microhardness Polyether ether ketones Polyetheretherketone Polymers Radiation Sheets Temperature Tensile strength Thermogravimetric analysis Tribology Viscoelasticity Wear rate |
| title | Effects of Electron Beam Irradiation on Mechanical and Tribological Properties of PEEK |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-31T22%3A39%3A00IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-gale_pubme&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Effects%20of%20Electron%20Beam%20Irradiation%20on%20Mechanical%20and%20Tribological%20Properties%20of%20PEEK&rft.jtitle=Polymers&rft.au=Kurbanova,%20Bayan&rft.date=2023-03-07&rft.volume=15&rft.issue=6&rft.spage=1340&rft.pages=1340-&rft.issn=2073-4360&rft.eissn=2073-4360&rft_id=info:doi/10.3390/polym15061340&rft_dat=%3Cgale_pubme%3EA743770526%3C/gale_pubme%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2791695862&rft_id=info:pmid/36987121&rft_galeid=A743770526&rfr_iscdi=true |