Trehalose matrices for high temperature dynamic nuclear polarization enhanced solid state NMR

Dynamic nuclear polarization (DNP) at cryogenic temperatures has proved to be a valuable technique to enhance the sensitivity of solid-state NMR spectroscopy. Over the years, sample formulations have been optimized for experiments at cryogenic temperatures. At 9.4 T, the best performing polarizing a...

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Veröffentlicht in:	Physical chemistry chemical physics : PCCP 2022-05, Vol.24 (2), p.12167-12175
Hauptverfasser:	Kaushik, Monu, Lingua, Hugo, Stevanato, Gabriele, Elokova, Margarita, Lelli, Moreno, Lesage, Anne, Ouari, Olivier
Format:	Artikel
Sprache:	eng
Schlagworte:	Ambient temperature Chemical Sciences Cryoforming Cryogenic temperature Formulations Glycerol-Water High temperature Molecular structure NMR spectroscopy Polarization Sensitivity enhancement Solid state Spectrum analysis Trehalose
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