Rapid detection of fumonisin B 1 and B 2 in ground corn samples using smartphone-controlled portable near-infrared spectrometry and chemometrics

A portable near-infrared (NIR) spectrometer coupled with chemometrics for the detection of fumonisin B and B (FBs) in ground corn samples was proposed in the present work. A total of 173 corn samples were collected, and their FB contents were determined by HPLC-MS/MS. Partial least squares (PLS), su...

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Veröffentlicht in:Food chemistry 2022-08, Vol.384, p.132487
Hauptverfasser: Shen, Guanghui, Kang, Xiaocun, Su, Jianshuo, Qiu, Jianbo, Liu, Xin, Xu, Jianhong, Shi, Jianrong, Mohamed, Sherif Ramzy
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Sprache:eng
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Zusammenfassung:A portable near-infrared (NIR) spectrometer coupled with chemometrics for the detection of fumonisin B and B (FBs) in ground corn samples was proposed in the present work. A total of 173 corn samples were collected, and their FB contents were determined by HPLC-MS/MS. Partial least squares (PLS), support vector machine (SVM) and local PLS based on global PLS score (LPLS-S) algorithms were employed to construct quantitative models. The performance of the SVM and LPLS-S was better than that of PLS, and the LPLS-S presented the lowest RMSEP (12.08 mg/kg) and the highest RPD (3.44). Partial least squares-discriminant analysis (PLS-DA) and support vector machine-discriminant analysis (SVM-DA) were used to classify corn samples according to the maximum residue limit (MRL) of FBs, and the discriminant accuracy of both the PLS-DA and SVM-DA algorithms was above 86.0%. Thus, the present study provided a rapid method for monitoring FB contamination in corn samples.
ISSN:1873-7072