An efficient route for the synthesis of phosphorus-selenium macro-heterocycles
Four-membered ring [PhP(Se)(μ-Se)] 2 (Woollins' reagent, WR) reacts with disodium alkenyl-diols followed by in situ ring-closure reaction with appropriate dibromoalkanes affording a series of unusual nine- to fifteen-membered organoselenophosphorus macrocycles bearing the O-P-Se-C n -Se-P-O or...
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| Veröffentlicht in: | Chemical communications (Cambridge, England) England), 2013-03, Vol.49 (26), p.2619-2621 |
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| container_title | Chemical communications (Cambridge, England) |
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| creator | Hua, Guoxiong Slawin, Alexandra M. Z Randall, Rebecca A. M Cordes, David B Crawford, L. Ellis Bühl, Michael Woollins, J. Derek |
| description | Four-membered ring [PhP(Se)(μ-Se)]
2
(Woollins' reagent, WR) reacts with disodium alkenyl-diols followed by
in situ
ring-closure reaction with appropriate dibromoalkanes affording a series of unusual nine- to fifteen-membered organoselenophosphorus macrocycles bearing the O-P-Se-C
n
-Se-P-O or O-P-Se-C
n
-O-P-Se linkage.
[PhP(Se)(μ-Se)]2 (Woollins' reagent,
WR
) with disodium alkenyl-diols and dibromoalkanes are able to construct a series of unusual nine- to fifteen-membered organoselenophosphorus macrocycles bearing the O-P-Se-C
n
-Se-P-O linkage or the O-P-Se-C
n
-O-P-Se linkage. |
| doi_str_mv | 10.1039/c3cc40515j |
| format | Article |
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2
(Woollins' reagent, WR) reacts with disodium alkenyl-diols followed by
in situ
ring-closure reaction with appropriate dibromoalkanes affording a series of unusual nine- to fifteen-membered organoselenophosphorus macrocycles bearing the O-P-Se-C
n
-Se-P-O or O-P-Se-C
n
-O-P-Se linkage.
[PhP(Se)(μ-Se)]2 (Woollins' reagent,
WR
) with disodium alkenyl-diols and dibromoalkanes are able to construct a series of unusual nine- to fifteen-membered organoselenophosphorus macrocycles bearing the O-P-Se-C
n
-Se-P-O linkage or the O-P-Se-C
n
-O-P-Se linkage.</description><identifier>ISSN: 1359-7345</identifier><identifier>EISSN: 1364-548X</identifier><identifier>DOI: 10.1039/c3cc40515j</identifier><identifier>PMID: 23436007</identifier><language>eng</language><publisher>England</publisher><subject>Bearing ; Heterocyclic Compounds - chemical synthesis ; Heterocyclic Compounds - chemistry ; Linkages ; Macromolecular Substances - chemical synthesis ; Macromolecular Substances - chemistry ; Models, Molecular ; Molecular Structure ; Organoselenium Compounds - chemical synthesis ; Organoselenium Compounds - chemistry ; Phosphorus - chemistry ; Selenium - chemistry ; Synthesis</subject><ispartof>Chemical communications (Cambridge, England), 2013-03, Vol.49 (26), p.2619-2621</ispartof><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c404t-762d93f22032886cd4d791266ee2795c4408c031d9a1cab1ddd9200277a8f9263</citedby><cites>FETCH-LOGICAL-c404t-762d93f22032886cd4d791266ee2795c4408c031d9a1cab1ddd9200277a8f9263</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27922,27923</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/23436007$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Hua, Guoxiong</creatorcontrib><creatorcontrib>Slawin, Alexandra M. Z</creatorcontrib><creatorcontrib>Randall, Rebecca A. M</creatorcontrib><creatorcontrib>Cordes, David B</creatorcontrib><creatorcontrib>Crawford, L. Ellis</creatorcontrib><creatorcontrib>Bühl, Michael</creatorcontrib><creatorcontrib>Woollins, J. Derek</creatorcontrib><title>An efficient route for the synthesis of phosphorus-selenium macro-heterocycles</title><title>Chemical communications (Cambridge, England)</title><addtitle>Chem Commun (Camb)</addtitle><description>Four-membered ring [PhP(Se)(μ-Se)]
2
(Woollins' reagent, WR) reacts with disodium alkenyl-diols followed by
in situ
ring-closure reaction with appropriate dibromoalkanes affording a series of unusual nine- to fifteen-membered organoselenophosphorus macrocycles bearing the O-P-Se-C
n
-Se-P-O or O-P-Se-C
n
-O-P-Se linkage.
[PhP(Se)(μ-Se)]2 (Woollins' reagent,
WR
) with disodium alkenyl-diols and dibromoalkanes are able to construct a series of unusual nine- to fifteen-membered organoselenophosphorus macrocycles bearing the O-P-Se-C
n
-Se-P-O linkage or the O-P-Se-C
n
-O-P-Se linkage.</description><subject>Bearing</subject><subject>Heterocyclic Compounds - chemical synthesis</subject><subject>Heterocyclic Compounds - chemistry</subject><subject>Linkages</subject><subject>Macromolecular Substances - chemical synthesis</subject><subject>Macromolecular Substances - chemistry</subject><subject>Models, Molecular</subject><subject>Molecular Structure</subject><subject>Organoselenium Compounds - chemical synthesis</subject><subject>Organoselenium Compounds - chemistry</subject><subject>Phosphorus - chemistry</subject><subject>Selenium - chemistry</subject><subject>Synthesis</subject><issn>1359-7345</issn><issn>1364-548X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqNkctLAzEQxoMotj4u3pV4E2E1790cy-KTohcFb8s2mdAt-6jJ7qH_vamt9SYODDPw_RhmvkHojJIbSri-NdwYQSSViz00plyJRIrsY3_dS52kXMgROgphQWJQmR2iEeOCK0LSMXqZtBicq0wFbY99N_SAXedxPwccVm0soQq4c3g570JMP4QkQA1tNTS4KY3vkjn04DuzMjWEE3TgyjrA6bYeo_f7u7f8MZm-Pjzlk2kSFxV9kipmNXeMEc6yTBkrbKopUwqApVoaIUhmCKdWl9SUM2qt1YwQlqZl5jRT_BhdbeYuffc5QOiLpgoG6rpsoRtCQbnQglOq5D9QKjKtBGMRvd6g8awQPLhi6aum9KuCkmJtdZHzPP-2-jnCF9u5w6wBu0N_vI3A-QbwwezU319F_fIvvVhax78AXFKNeg</recordid><startdate>20130305</startdate><enddate>20130305</enddate><creator>Hua, Guoxiong</creator><creator>Slawin, Alexandra M. Z</creator><creator>Randall, Rebecca A. M</creator><creator>Cordes, David B</creator><creator>Crawford, L. Ellis</creator><creator>Bühl, Michael</creator><creator>Woollins, J. Derek</creator><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>7SP</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>20130305</creationdate><title>An efficient route for the synthesis of phosphorus-selenium macro-heterocycles</title><author>Hua, Guoxiong ; Slawin, Alexandra M. Z ; Randall, Rebecca A. M ; Cordes, David B ; Crawford, L. Ellis ; Bühl, Michael ; Woollins, J. Derek</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c404t-762d93f22032886cd4d791266ee2795c4408c031d9a1cab1ddd9200277a8f9263</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Bearing</topic><topic>Heterocyclic Compounds - chemical synthesis</topic><topic>Heterocyclic Compounds - chemistry</topic><topic>Linkages</topic><topic>Macromolecular Substances - chemical synthesis</topic><topic>Macromolecular Substances - chemistry</topic><topic>Models, Molecular</topic><topic>Molecular Structure</topic><topic>Organoselenium Compounds - chemical synthesis</topic><topic>Organoselenium Compounds - chemistry</topic><topic>Phosphorus - chemistry</topic><topic>Selenium - chemistry</topic><topic>Synthesis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hua, Guoxiong</creatorcontrib><creatorcontrib>Slawin, Alexandra M. Z</creatorcontrib><creatorcontrib>Randall, Rebecca A. M</creatorcontrib><creatorcontrib>Cordes, David B</creatorcontrib><creatorcontrib>Crawford, L. Ellis</creatorcontrib><creatorcontrib>Bühl, Michael</creatorcontrib><creatorcontrib>Woollins, J. Derek</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Electronics & Communications Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Chemical communications (Cambridge, England)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Hua, Guoxiong</au><au>Slawin, Alexandra M. Z</au><au>Randall, Rebecca A. M</au><au>Cordes, David B</au><au>Crawford, L. Ellis</au><au>Bühl, Michael</au><au>Woollins, J. Derek</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>An efficient route for the synthesis of phosphorus-selenium macro-heterocycles</atitle><jtitle>Chemical communications (Cambridge, England)</jtitle><addtitle>Chem Commun (Camb)</addtitle><date>2013-03-05</date><risdate>2013</risdate><volume>49</volume><issue>26</issue><spage>2619</spage><epage>2621</epage><pages>2619-2621</pages><issn>1359-7345</issn><eissn>1364-548X</eissn><abstract>Four-membered ring [PhP(Se)(μ-Se)]
2
(Woollins' reagent, WR) reacts with disodium alkenyl-diols followed by
in situ
ring-closure reaction with appropriate dibromoalkanes affording a series of unusual nine- to fifteen-membered organoselenophosphorus macrocycles bearing the O-P-Se-C
n
-Se-P-O or O-P-Se-C
n
-O-P-Se linkage.
[PhP(Se)(μ-Se)]2 (Woollins' reagent,
WR
) with disodium alkenyl-diols and dibromoalkanes are able to construct a series of unusual nine- to fifteen-membered organoselenophosphorus macrocycles bearing the O-P-Se-C
n
-Se-P-O linkage or the O-P-Se-C
n
-O-P-Se linkage.</abstract><cop>England</cop><pmid>23436007</pmid><doi>10.1039/c3cc40515j</doi><tpages>3</tpages><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1359-7345 |
| ispartof | Chemical communications (Cambridge, England), 2013-03, Vol.49 (26), p.2619-2621 |
| issn | 1359-7345 1364-548X |
| language | eng |
| recordid | cdi_pubmed_primary_23436007 |
| source | MEDLINE; Royal Society Of Chemistry Journals 2008-; Alma/SFX Local Collection |
| subjects | Bearing Heterocyclic Compounds - chemical synthesis Heterocyclic Compounds - chemistry Linkages Macromolecular Substances - chemical synthesis Macromolecular Substances - chemistry Models, Molecular Molecular Structure Organoselenium Compounds - chemical synthesis Organoselenium Compounds - chemistry Phosphorus - chemistry Selenium - chemistry Synthesis |
| title | An efficient route for the synthesis of phosphorus-selenium macro-heterocycles |
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