Glow discharge optical emission spectroscopy for accurate and well resolved analysis of coatings and thin films

In the last years, glow discharge optical emission spectrometry (GDOES) gained more and more acceptance in the analysis of functional coatings. GDOES thereby represents an interesting alternative to common depth profiling techniques like AES and SIMS, based on its unique combination of high erosion...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Thin solid films 2011-12, Vol.520 (5), p.1660-1667
Hauptverfasser: Wilke, Marcus, Teichert, Gerd, Gemma, Ryota, Pundt, Astrid, Kirchheim, Reiner, Romanus, Henry, Schaaf, Peter
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page 1667
container_issue 5
container_start_page 1660
container_title Thin solid films
container_volume 520
creator Wilke, Marcus
Teichert, Gerd
Gemma, Ryota
Pundt, Astrid
Kirchheim, Reiner
Romanus, Henry
Schaaf, Peter
description In the last years, glow discharge optical emission spectrometry (GDOES) gained more and more acceptance in the analysis of functional coatings. GDOES thereby represents an interesting alternative to common depth profiling techniques like AES and SIMS, based on its unique combination of high erosion rates and erosion depths, sensitivity, analysis of nonconductive layers and easy quantification even for light elements such as C, N, O and H. Starting with the fundamentals of GDOES, a short overview on new developments in instrument design for accurate and well resolved thin film analyses is presented. The article focuses on the analytical capabilities of glow discharge optical emission spectrometry in the analysis of metallic coatings and thin films. Results illustrating the high depth resolution, confirmation of stoichiometry, the detection of light elements in coatings as well as contamination on the surface or interfaces will be demonstrated by measurements of: a multilayer system Cr/Ti on silicon, interface contamination on silicon during deposition of aluminum, Al 2O 3-nanoparticle containing conversion coatings on zinc for corrosion resistance, Ti 3SiC 2 MAX-phase coatings by pulsed laser deposition and hydrogen detection in a V/Fe multilayer system. The selected examples illustrate that GDOES can be successfully adopted as an analytical tool in the development of new materials and coatings. A discussion of the results as well as of the limitations of GDOES is presented.
doi_str_mv 10.1016/j.tsf.2011.07.058
format Article
fullrecord <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_968175376</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S0040609011014453</els_id><sourcerecordid>1671308350</sourcerecordid><originalsourceid>FETCH-LOGICAL-c458t-d2359fa698463caa69a331d033912aed31ac3a875b8be5a926a2327ac2a5304b3</originalsourceid><addsrcrecordid>eNp9kU1r3DAQhkVpoNu0P6A3XUp6sTuSVh8mpxLyUQj00pzFrCwnWryWq_Em7L-vkg055qRBPDMjvQ9j3wS0AoT5uW0XGloJQrRgW9DuA1sJZ7tGWiU-shXAGhoDHXxin4m2ACCkVCuWr8f8xPtE4QHLfeR5XlLAkcddIkp54jTHsJRMIc8HPuTCMYR9wSVynHr-FMeRl0h5fIx9vcHxQIl4HnjIuKTpnl6w5SFNfEjjjr6wkwFHil9fz1N2d3X59-Kmuf1z_fvi120T1totTS-V7gY0nVsbFbAWqJToQalOSIy9EhgUOqs3bhM1dtKgVNJikKgVrDfqlJ0d584l_9tHWnz9UKivxSnmPfnOOGG1sqaSP94lhbFCgVMaKiqOaKiBUImDn0vaYTl4Af5Zg9_6qsE_a_BgfdVQe76_jkeqwQ4Fp5DorVFqp41QsnLnRy7WVB5TLJ5CilOIfSrVgO9zemfLf8RLnj0</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1671308350</pqid></control><display><type>article</type><title>Glow discharge optical emission spectroscopy for accurate and well resolved analysis of coatings and thin films</title><source>Access via ScienceDirect (Elsevier)</source><creator>Wilke, Marcus ; Teichert, Gerd ; Gemma, Ryota ; Pundt, Astrid ; Kirchheim, Reiner ; Romanus, Henry ; Schaaf, Peter</creator><creatorcontrib>Wilke, Marcus ; Teichert, Gerd ; Gemma, Ryota ; Pundt, Astrid ; Kirchheim, Reiner ; Romanus, Henry ; Schaaf, Peter</creatorcontrib><description>In the last years, glow discharge optical emission spectrometry (GDOES) gained more and more acceptance in the analysis of functional coatings. GDOES thereby represents an interesting alternative to common depth profiling techniques like AES and SIMS, based on its unique combination of high erosion rates and erosion depths, sensitivity, analysis of nonconductive layers and easy quantification even for light elements such as C, N, O and H. Starting with the fundamentals of GDOES, a short overview on new developments in instrument design for accurate and well resolved thin film analyses is presented. The article focuses on the analytical capabilities of glow discharge optical emission spectrometry in the analysis of metallic coatings and thin films. Results illustrating the high depth resolution, confirmation of stoichiometry, the detection of light elements in coatings as well as contamination on the surface or interfaces will be demonstrated by measurements of: a multilayer system Cr/Ti on silicon, interface contamination on silicon during deposition of aluminum, Al 2O 3-nanoparticle containing conversion coatings on zinc for corrosion resistance, Ti 3SiC 2 MAX-phase coatings by pulsed laser deposition and hydrogen detection in a V/Fe multilayer system. The selected examples illustrate that GDOES can be successfully adopted as an analytical tool in the development of new materials and coatings. A discussion of the results as well as of the limitations of GDOES is presented.</description><identifier>ISSN: 0040-6090</identifier><identifier>EISSN: 1879-2731</identifier><identifier>DOI: 10.1016/j.tsf.2011.07.058</identifier><identifier>CODEN: THSFAP</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Coatings ; Condensed matter: structure, mechanical and thermal properties ; Cross-disciplinary physics: materials science; rheology ; Defects and impurities: doping, implantation, distribution, concentration, etc ; Electric discharges ; Electrodeposition, electroplating ; Elemental depth profiles ; Emission analysis ; Exact sciences and technology ; GDOES ; Glow discharge optical emission spectroscopy ; Glow discharges ; Glow; corona ; Light elements ; Materials science ; Mathematical analysis ; MAX phase ; Methods of deposition of films and coatings; film growth and epitaxy ; Multilayers ; Nanoscale materials and structures: fabrication and characterization ; Other topics in nanoscale materials and structures ; Physics ; Physics of gases, plasmas and electric discharges ; Physics of plasmas and electric discharges ; Spectroscopy ; Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties) ; Thick coatings ; Thin film analysis ; Thin film structure and morphology ; Thin films ; Thin films and coatings</subject><ispartof>Thin solid films, 2011-12, Vol.520 (5), p.1660-1667</ispartof><rights>2011 Elsevier B.V.</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c458t-d2359fa698463caa69a331d033912aed31ac3a875b8be5a926a2327ac2a5304b3</citedby><cites>FETCH-LOGICAL-c458t-d2359fa698463caa69a331d033912aed31ac3a875b8be5a926a2327ac2a5304b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.tsf.2011.07.058$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>309,310,314,780,784,789,790,3550,23930,23931,25140,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&amp;idt=25856132$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Wilke, Marcus</creatorcontrib><creatorcontrib>Teichert, Gerd</creatorcontrib><creatorcontrib>Gemma, Ryota</creatorcontrib><creatorcontrib>Pundt, Astrid</creatorcontrib><creatorcontrib>Kirchheim, Reiner</creatorcontrib><creatorcontrib>Romanus, Henry</creatorcontrib><creatorcontrib>Schaaf, Peter</creatorcontrib><title>Glow discharge optical emission spectroscopy for accurate and well resolved analysis of coatings and thin films</title><title>Thin solid films</title><description>In the last years, glow discharge optical emission spectrometry (GDOES) gained more and more acceptance in the analysis of functional coatings. GDOES thereby represents an interesting alternative to common depth profiling techniques like AES and SIMS, based on its unique combination of high erosion rates and erosion depths, sensitivity, analysis of nonconductive layers and easy quantification even for light elements such as C, N, O and H. Starting with the fundamentals of GDOES, a short overview on new developments in instrument design for accurate and well resolved thin film analyses is presented. The article focuses on the analytical capabilities of glow discharge optical emission spectrometry in the analysis of metallic coatings and thin films. Results illustrating the high depth resolution, confirmation of stoichiometry, the detection of light elements in coatings as well as contamination on the surface or interfaces will be demonstrated by measurements of: a multilayer system Cr/Ti on silicon, interface contamination on silicon during deposition of aluminum, Al 2O 3-nanoparticle containing conversion coatings on zinc for corrosion resistance, Ti 3SiC 2 MAX-phase coatings by pulsed laser deposition and hydrogen detection in a V/Fe multilayer system. The selected examples illustrate that GDOES can be successfully adopted as an analytical tool in the development of new materials and coatings. A discussion of the results as well as of the limitations of GDOES is presented.</description><subject>Coatings</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Defects and impurities: doping, implantation, distribution, concentration, etc</subject><subject>Electric discharges</subject><subject>Electrodeposition, electroplating</subject><subject>Elemental depth profiles</subject><subject>Emission analysis</subject><subject>Exact sciences and technology</subject><subject>GDOES</subject><subject>Glow discharge optical emission spectroscopy</subject><subject>Glow discharges</subject><subject>Glow; corona</subject><subject>Light elements</subject><subject>Materials science</subject><subject>Mathematical analysis</subject><subject>MAX phase</subject><subject>Methods of deposition of films and coatings; film growth and epitaxy</subject><subject>Multilayers</subject><subject>Nanoscale materials and structures: fabrication and characterization</subject><subject>Other topics in nanoscale materials and structures</subject><subject>Physics</subject><subject>Physics of gases, plasmas and electric discharges</subject><subject>Physics of plasmas and electric discharges</subject><subject>Spectroscopy</subject><subject>Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties)</subject><subject>Thick coatings</subject><subject>Thin film analysis</subject><subject>Thin film structure and morphology</subject><subject>Thin films</subject><subject>Thin films and coatings</subject><issn>0040-6090</issn><issn>1879-2731</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNp9kU1r3DAQhkVpoNu0P6A3XUp6sTuSVh8mpxLyUQj00pzFrCwnWryWq_Em7L-vkg055qRBPDMjvQ9j3wS0AoT5uW0XGloJQrRgW9DuA1sJZ7tGWiU-shXAGhoDHXxin4m2ACCkVCuWr8f8xPtE4QHLfeR5XlLAkcddIkp54jTHsJRMIc8HPuTCMYR9wSVynHr-FMeRl0h5fIx9vcHxQIl4HnjIuKTpnl6w5SFNfEjjjr6wkwFHil9fz1N2d3X59-Kmuf1z_fvi120T1totTS-V7gY0nVsbFbAWqJToQalOSIy9EhgUOqs3bhM1dtKgVNJikKgVrDfqlJ0d584l_9tHWnz9UKivxSnmPfnOOGG1sqaSP94lhbFCgVMaKiqOaKiBUImDn0vaYTl4Af5Zg9_6qsE_a_BgfdVQe76_jkeqwQ4Fp5DorVFqp41QsnLnRy7WVB5TLJ5CilOIfSrVgO9zemfLf8RLnj0</recordid><startdate>20111230</startdate><enddate>20111230</enddate><creator>Wilke, Marcus</creator><creator>Teichert, Gerd</creator><creator>Gemma, Ryota</creator><creator>Pundt, Astrid</creator><creator>Kirchheim, Reiner</creator><creator>Romanus, Henry</creator><creator>Schaaf, Peter</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QF</scope><scope>7SE</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope><scope>7TV</scope><scope>C1K</scope></search><sort><creationdate>20111230</creationdate><title>Glow discharge optical emission spectroscopy for accurate and well resolved analysis of coatings and thin films</title><author>Wilke, Marcus ; Teichert, Gerd ; Gemma, Ryota ; Pundt, Astrid ; Kirchheim, Reiner ; Romanus, Henry ; Schaaf, Peter</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c458t-d2359fa698463caa69a331d033912aed31ac3a875b8be5a926a2327ac2a5304b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Coatings</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Defects and impurities: doping, implantation, distribution, concentration, etc</topic><topic>Electric discharges</topic><topic>Electrodeposition, electroplating</topic><topic>Elemental depth profiles</topic><topic>Emission analysis</topic><topic>Exact sciences and technology</topic><topic>GDOES</topic><topic>Glow discharge optical emission spectroscopy</topic><topic>Glow discharges</topic><topic>Glow; corona</topic><topic>Light elements</topic><topic>Materials science</topic><topic>Mathematical analysis</topic><topic>MAX phase</topic><topic>Methods of deposition of films and coatings; film growth and epitaxy</topic><topic>Multilayers</topic><topic>Nanoscale materials and structures: fabrication and characterization</topic><topic>Other topics in nanoscale materials and structures</topic><topic>Physics</topic><topic>Physics of gases, plasmas and electric discharges</topic><topic>Physics of plasmas and electric discharges</topic><topic>Spectroscopy</topic><topic>Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties)</topic><topic>Thick coatings</topic><topic>Thin film analysis</topic><topic>Thin film structure and morphology</topic><topic>Thin films</topic><topic>Thin films and coatings</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wilke, Marcus</creatorcontrib><creatorcontrib>Teichert, Gerd</creatorcontrib><creatorcontrib>Gemma, Ryota</creatorcontrib><creatorcontrib>Pundt, Astrid</creatorcontrib><creatorcontrib>Kirchheim, Reiner</creatorcontrib><creatorcontrib>Romanus, Henry</creatorcontrib><creatorcontrib>Schaaf, Peter</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Aluminium Industry Abstracts</collection><collection>Corrosion Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Pollution Abstracts</collection><collection>Environmental Sciences and Pollution Management</collection><jtitle>Thin solid films</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wilke, Marcus</au><au>Teichert, Gerd</au><au>Gemma, Ryota</au><au>Pundt, Astrid</au><au>Kirchheim, Reiner</au><au>Romanus, Henry</au><au>Schaaf, Peter</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Glow discharge optical emission spectroscopy for accurate and well resolved analysis of coatings and thin films</atitle><jtitle>Thin solid films</jtitle><date>2011-12-30</date><risdate>2011</risdate><volume>520</volume><issue>5</issue><spage>1660</spage><epage>1667</epage><pages>1660-1667</pages><issn>0040-6090</issn><eissn>1879-2731</eissn><coden>THSFAP</coden><abstract>In the last years, glow discharge optical emission spectrometry (GDOES) gained more and more acceptance in the analysis of functional coatings. GDOES thereby represents an interesting alternative to common depth profiling techniques like AES and SIMS, based on its unique combination of high erosion rates and erosion depths, sensitivity, analysis of nonconductive layers and easy quantification even for light elements such as C, N, O and H. Starting with the fundamentals of GDOES, a short overview on new developments in instrument design for accurate and well resolved thin film analyses is presented. The article focuses on the analytical capabilities of glow discharge optical emission spectrometry in the analysis of metallic coatings and thin films. Results illustrating the high depth resolution, confirmation of stoichiometry, the detection of light elements in coatings as well as contamination on the surface or interfaces will be demonstrated by measurements of: a multilayer system Cr/Ti on silicon, interface contamination on silicon during deposition of aluminum, Al 2O 3-nanoparticle containing conversion coatings on zinc for corrosion resistance, Ti 3SiC 2 MAX-phase coatings by pulsed laser deposition and hydrogen detection in a V/Fe multilayer system. The selected examples illustrate that GDOES can be successfully adopted as an analytical tool in the development of new materials and coatings. A discussion of the results as well as of the limitations of GDOES is presented.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.tsf.2011.07.058</doi><tpages>8</tpages></addata></record>
fulltext fulltext
identifier ISSN: 0040-6090
ispartof Thin solid films, 2011-12, Vol.520 (5), p.1660-1667
issn 0040-6090
1879-2731
language eng
recordid cdi_proquest_miscellaneous_968175376
source Access via ScienceDirect (Elsevier)
subjects Coatings
Condensed matter: structure, mechanical and thermal properties
Cross-disciplinary physics: materials science
rheology
Defects and impurities: doping, implantation, distribution, concentration, etc
Electric discharges
Electrodeposition, electroplating
Elemental depth profiles
Emission analysis
Exact sciences and technology
GDOES
Glow discharge optical emission spectroscopy
Glow discharges
Glow
corona
Light elements
Materials science
Mathematical analysis
MAX phase
Methods of deposition of films and coatings
film growth and epitaxy
Multilayers
Nanoscale materials and structures: fabrication and characterization
Other topics in nanoscale materials and structures
Physics
Physics of gases, plasmas and electric discharges
Physics of plasmas and electric discharges
Spectroscopy
Surfaces and interfaces
thin films and whiskers (structure and nonelectronic properties)
Thick coatings
Thin film analysis
Thin film structure and morphology
Thin films
Thin films and coatings
title Glow discharge optical emission spectroscopy for accurate and well resolved analysis of coatings and thin films
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-02T18%3A04%3A16IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Glow%20discharge%20optical%20emission%20spectroscopy%20for%20accurate%20and%20well%20resolved%20analysis%20of%20coatings%20and%20thin%20films&rft.jtitle=Thin%20solid%20films&rft.au=Wilke,%20Marcus&rft.date=2011-12-30&rft.volume=520&rft.issue=5&rft.spage=1660&rft.epage=1667&rft.pages=1660-1667&rft.issn=0040-6090&rft.eissn=1879-2731&rft.coden=THSFAP&rft_id=info:doi/10.1016/j.tsf.2011.07.058&rft_dat=%3Cproquest_cross%3E1671308350%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1671308350&rft_id=info:pmid/&rft_els_id=S0040609011014453&rfr_iscdi=true