Unraveling the Mysterious Role of Palladium in Feigl bis(dimethylglyoximate)nickel(II) Spot Tests by Means of Confocal Raman Microscopy
The acid protection effect promoted by traces of PdCl2 in [Ni(dmgH)2] spot tests was elucidated from confocal Raman microscopy imaging, which revealed the formation of protecting layers of [Pd(dmgH)2] closing the extremities of the [Ni(dmgH)2] filaments.
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| Veröffentlicht in: | Analytical chemistry (Washington) 2012-04, Vol.84 (7), p.3067-3069 |
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| container_end_page | 3069 |
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| container_title | Analytical chemistry (Washington) |
| container_volume | 84 |
| creator | Huila, Manuel F. G Lukin, Nikolas Parussulo, Andre L. A Oliveira, Pedro V Kyohara, Pedro K Araki, Koiti Toma, Henrique E |
| description | The acid protection effect promoted by traces of PdCl2 in [Ni(dmgH)2] spot tests was elucidated from confocal Raman microscopy imaging, which revealed the formation of protecting layers of [Pd(dmgH)2] closing the extremities of the [Ni(dmgH)2] filaments. |
| doi_str_mv | 10.1021/ac3003352 |
| format | Article |
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| source | ACS Publications |
| subjects | Acids Analytical chemistry Chemistry Exact sciences and technology Microscopy Scientific imaging Spectrometric and optical methods |
| title | Unraveling the Mysterious Role of Palladium in Feigl bis(dimethylglyoximate)nickel(II) Spot Tests by Means of Confocal Raman Microscopy |
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