Quantitative research on effects of Nb on hot deformation behaviors of high-Nb microalloyed steels

► The amount of Nb in solution and/or in precipitates was determined. ► The Nb cannot be completely dissolved during the reheating process. ► The precipitates cannot effect on dynamic recrystallization. ► The Q def presents a perfect linear correlation with the amount of Nb in solution. ► Each addit...

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Veröffentlicht in:Materials science & engineering. A, Structural materials : properties, microstructure and processing Structural materials : properties, microstructure and processing, 2011-12, Vol.530, p.277-284
Hauptverfasser: Cao, Ya-bin, Xiao, Fu-ren, Qiao, Gui-ying, Zhang, Xiao-bing, Liao, Bo
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container_title Materials science & engineering. A, Structural materials : properties, microstructure and processing
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creator Cao, Ya-bin
Xiao, Fu-ren
Qiao, Gui-ying
Zhang, Xiao-bing
Liao, Bo
description ► The amount of Nb in solution and/or in precipitates was determined. ► The Nb cannot be completely dissolved during the reheating process. ► The precipitates cannot effect on dynamic recrystallization. ► The Q def presents a perfect linear correlation with the amount of Nb in solution. ► Each addition of 1 wt% Nb in solution adds 1599.9 ± 137.7 kJ/mol to Q def. The hot deformation behaviors of six high-Nb steels were investigated by hot compression methods on a Gleeble-3500 thermo-mechanical simulator. The amount of Nb in solution and/or in precipitates of the specimens deformed at different conditions was determined by inductively coupled plasma–atomic emission spectrometry (ICP–AES). The effects of dissolved Nb and precipitates on hot deformation behavior were discussed. The results show that Nb cannot be completely dissolved in the high-Nb steels during the reheating process, and the undissolved precipitates do not influence the dynamic recrystallization due to their larger size. Moreover, the undissolved precipitates more effectively influence the peak stress instead of peak strain. Strain induced precipitation occurs during the hot deformation process. However, the precipitates cannot delay the dynamic recrystallization because of the longer induction period. The deformation activation energy presents a perfect linear correlation as a function of the amount of Nb in solutions, and each addition of Nb by 1 wt% would lead to an increase of the deformation activation energy by 1599.9 ± 137.7 kJ/mol.
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The hot deformation behaviors of six high-Nb steels were investigated by hot compression methods on a Gleeble-3500 thermo-mechanical simulator. The amount of Nb in solution and/or in precipitates of the specimens deformed at different conditions was determined by inductively coupled plasma–atomic emission spectrometry (ICP–AES). The effects of dissolved Nb and precipitates on hot deformation behavior were discussed. The results show that Nb cannot be completely dissolved in the high-Nb steels during the reheating process, and the undissolved precipitates do not influence the dynamic recrystallization due to their larger size. Moreover, the undissolved precipitates more effectively influence the peak stress instead of peak strain. Strain induced precipitation occurs during the hot deformation process. However, the precipitates cannot delay the dynamic recrystallization because of the longer induction period. 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A, Structural materials : properties, microstructure and processing</title><description>► The amount of Nb in solution and/or in precipitates was determined. ► The Nb cannot be completely dissolved during the reheating process. ► The precipitates cannot effect on dynamic recrystallization. ► The Q def presents a perfect linear correlation with the amount of Nb in solution. ► Each addition of 1 wt% Nb in solution adds 1599.9 ± 137.7 kJ/mol to Q def. The hot deformation behaviors of six high-Nb steels were investigated by hot compression methods on a Gleeble-3500 thermo-mechanical simulator. The amount of Nb in solution and/or in precipitates of the specimens deformed at different conditions was determined by inductively coupled plasma–atomic emission spectrometry (ICP–AES). The effects of dissolved Nb and precipitates on hot deformation behavior were discussed. 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subjects Applied sciences
Cold working, work hardening
annealing, quenching, tempering, recovery, and recrystallization
textures
Cross-disciplinary physics: materials science
rheology
Deformation
Deformation activation energy
Dissolution
Dissolved Nb
Dynamic recrystallization
Elasticity. Plasticity
Emission analysis
Exact sciences and technology
Inductively coupled plasma
Materials science
Mechanical properties and methods of testing. Rheology. Fracture mechanics. Tribology
Metals. Metallurgy
Niobium
Physics
Precipitates
Precipitation
Spectroscopy
Strain induced precipitation
Treatment of materials and its effects on microstructure and properties
title Quantitative research on effects of Nb on hot deformation behaviors of high-Nb microalloyed steels
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