Surface morphology and mechanical properties of new-generation flowable resin composites for dental restoration
Abstract Objectives The purpose of this study was to characterize the surface morphology and the elastic properties of four dental restorative flowable composites currently on the market (Venus Diamond Flow, Vertise Flow, Filtex Supreme XT Flow, Surefil SDR Flow). Additionally, one adhesive system (...
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Veröffentlicht in: | Dental materials 2011-12, Vol.27 (12), p.1221-1228 |
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description | Abstract Objectives The purpose of this study was to characterize the surface morphology and the elastic properties of four dental restorative flowable composites currently on the market (Venus Diamond Flow, Vertise Flow, Filtex Supreme XT Flow, Surefil SDR Flow). Additionally, one adhesive system (Adhese One F) and one non-flowable composite (Venus Diamond) have also been characterized as the control materials. Methods Surface morphology was studied by both scanning electron and atomic force microscopy, and the elastic modulus and the hardness measured by instrumented indentation. Grain analysis was performed on the microscopic images, and statistical analysis was carried out on the results of the nanoindentation measurements. Results It was observed that Vertise, Filtek XT and Surefil SDR exhibit stiffness similar to the non-flowable Venus Diamond, whereas Venus Diamond Flow presents itself as the more compliant flowable composite, with Adhese showing intermediate stiffness. Grain analysis of the images confirmed the general rule that the mechanical properties improve with increasing filler loading, with the notable exception of Vertise Flow that shows modulus and hardness as high as 9.1 ± 0.6 and 0.43 ± 0.03 GPa, respectively, for an estimated loading of only ∼40% by volume. Significance Whereas generally flowable composites are confirmed not to possess sufficiently strong mechanical properties for bulk restorations, exceptions can eventually be found upon appropriate laboratory screening, as presently seems to be the case for Vertise Flow. However, real practice in actual restorations and respective clinical evaluation are required for final assessment of the suggested results. |
doi_str_mv | 10.1016/j.dental.2011.08.596 |
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Additionally, one adhesive system (Adhese One F) and one non-flowable composite (Venus Diamond) have also been characterized as the control materials. Methods Surface morphology was studied by both scanning electron and atomic force microscopy, and the elastic modulus and the hardness measured by instrumented indentation. Grain analysis was performed on the microscopic images, and statistical analysis was carried out on the results of the nanoindentation measurements. Results It was observed that Vertise, Filtek XT and Surefil SDR exhibit stiffness similar to the non-flowable Venus Diamond, whereas Venus Diamond Flow presents itself as the more compliant flowable composite, with Adhese showing intermediate stiffness. Grain analysis of the images confirmed the general rule that the mechanical properties improve with increasing filler loading, with the notable exception of Vertise Flow that shows modulus and hardness as high as 9.1 ± 0.6 and 0.43 ± 0.03 GPa, respectively, for an estimated loading of only ∼40% by volume. Significance Whereas generally flowable composites are confirmed not to possess sufficiently strong mechanical properties for bulk restorations, exceptions can eventually be found upon appropriate laboratory screening, as presently seems to be the case for Vertise Flow. However, real practice in actual restorations and respective clinical evaluation are required for final assessment of the suggested results.</description><identifier>ISSN: 0109-5641</identifier><identifier>EISSN: 1879-0097</identifier><identifier>DOI: 10.1016/j.dental.2011.08.596</identifier><identifier>PMID: 22000067</identifier><language>eng</language><publisher>England: Elsevier Ltd</publisher><subject>Acrylic Resins - chemistry ; Advanced Basic Science ; Atomic force microscopy ; Composite Resins - chemistry ; Compressive Strength ; Dental materials ; Dental Materials - chemistry ; Dental Restoration, Permanent ; Dentistry ; Elastic Modulus ; Hardness ; Humans ; Materials Testing ; Mechanical Phenomena ; Mechanical properties ; Microscopy, Atomic Force ; Microscopy, Electron, Scanning ; Morphology ; Nanocomposites - chemistry ; Nanoindentation ; Particle Size ; Pliability ; Resin Cements - chemistry ; Restoration ; Restorative resin composites ; Scanning electron microscopy ; Surface Properties ; Tensile Strength ; Venus ; Viscosity</subject><ispartof>Dental materials, 2011-12, Vol.27 (12), p.1221-1228</ispartof><rights>Academy of Dental Materials</rights><rights>2011 Academy of Dental Materials</rights><rights>Copyright © 2011 Academy of Dental Materials. Published by Elsevier Ltd. All rights reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c514t-2d26854afadd5ff14ee0d0eb7eaa8d3b1244ad6deaf14449ce97a315132cec83</citedby><cites>FETCH-LOGICAL-c514t-2d26854afadd5ff14ee0d0eb7eaa8d3b1244ad6deaf14449ce97a315132cec83</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0109564111008578$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/22000067$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Salerno, Marco</creatorcontrib><creatorcontrib>Derchi, Giacomo</creatorcontrib><creatorcontrib>Thorat, Sanjay</creatorcontrib><creatorcontrib>Ceseracciu, Luca</creatorcontrib><creatorcontrib>Ruffilli, Roberta</creatorcontrib><creatorcontrib>Barone, Alberto C</creatorcontrib><title>Surface morphology and mechanical properties of new-generation flowable resin composites for dental restoration</title><title>Dental materials</title><addtitle>Dent Mater</addtitle><description>Abstract Objectives The purpose of this study was to characterize the surface morphology and the elastic properties of four dental restorative flowable composites currently on the market (Venus Diamond Flow, Vertise Flow, Filtex Supreme XT Flow, Surefil SDR Flow). Additionally, one adhesive system (Adhese One F) and one non-flowable composite (Venus Diamond) have also been characterized as the control materials. Methods Surface morphology was studied by both scanning electron and atomic force microscopy, and the elastic modulus and the hardness measured by instrumented indentation. Grain analysis was performed on the microscopic images, and statistical analysis was carried out on the results of the nanoindentation measurements. Results It was observed that Vertise, Filtek XT and Surefil SDR exhibit stiffness similar to the non-flowable Venus Diamond, whereas Venus Diamond Flow presents itself as the more compliant flowable composite, with Adhese showing intermediate stiffness. Grain analysis of the images confirmed the general rule that the mechanical properties improve with increasing filler loading, with the notable exception of Vertise Flow that shows modulus and hardness as high as 9.1 ± 0.6 and 0.43 ± 0.03 GPa, respectively, for an estimated loading of only ∼40% by volume. Significance Whereas generally flowable composites are confirmed not to possess sufficiently strong mechanical properties for bulk restorations, exceptions can eventually be found upon appropriate laboratory screening, as presently seems to be the case for Vertise Flow. 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Derchi, Giacomo ; Thorat, Sanjay ; Ceseracciu, Luca ; Ruffilli, Roberta ; Barone, Alberto C</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c514t-2d26854afadd5ff14ee0d0eb7eaa8d3b1244ad6deaf14449ce97a315132cec83</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Acrylic Resins - chemistry</topic><topic>Advanced Basic Science</topic><topic>Atomic force microscopy</topic><topic>Composite Resins - chemistry</topic><topic>Compressive Strength</topic><topic>Dental materials</topic><topic>Dental Materials - chemistry</topic><topic>Dental Restoration, Permanent</topic><topic>Dentistry</topic><topic>Elastic Modulus</topic><topic>Hardness</topic><topic>Humans</topic><topic>Materials Testing</topic><topic>Mechanical Phenomena</topic><topic>Mechanical properties</topic><topic>Microscopy, Atomic Force</topic><topic>Microscopy, Electron, Scanning</topic><topic>Morphology</topic><topic>Nanocomposites - chemistry</topic><topic>Nanoindentation</topic><topic>Particle Size</topic><topic>Pliability</topic><topic>Resin Cements - chemistry</topic><topic>Restoration</topic><topic>Restorative resin composites</topic><topic>Scanning electron microscopy</topic><topic>Surface Properties</topic><topic>Tensile Strength</topic><topic>Venus</topic><topic>Viscosity</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Salerno, Marco</creatorcontrib><creatorcontrib>Derchi, Giacomo</creatorcontrib><creatorcontrib>Thorat, Sanjay</creatorcontrib><creatorcontrib>Ceseracciu, Luca</creatorcontrib><creatorcontrib>Ruffilli, Roberta</creatorcontrib><creatorcontrib>Barone, Alberto C</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Engineered Materials Abstracts</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Dental materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Salerno, Marco</au><au>Derchi, Giacomo</au><au>Thorat, Sanjay</au><au>Ceseracciu, Luca</au><au>Ruffilli, Roberta</au><au>Barone, Alberto C</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Surface morphology and mechanical properties of new-generation flowable resin composites for dental restoration</atitle><jtitle>Dental materials</jtitle><addtitle>Dent Mater</addtitle><date>2011-12-01</date><risdate>2011</risdate><volume>27</volume><issue>12</issue><spage>1221</spage><epage>1228</epage><pages>1221-1228</pages><issn>0109-5641</issn><eissn>1879-0097</eissn><abstract>Abstract Objectives The purpose of this study was to characterize the surface morphology and the elastic properties of four dental restorative flowable composites currently on the market (Venus Diamond Flow, Vertise Flow, Filtex Supreme XT Flow, Surefil SDR Flow). Additionally, one adhesive system (Adhese One F) and one non-flowable composite (Venus Diamond) have also been characterized as the control materials. Methods Surface morphology was studied by both scanning electron and atomic force microscopy, and the elastic modulus and the hardness measured by instrumented indentation. Grain analysis was performed on the microscopic images, and statistical analysis was carried out on the results of the nanoindentation measurements. Results It was observed that Vertise, Filtek XT and Surefil SDR exhibit stiffness similar to the non-flowable Venus Diamond, whereas Venus Diamond Flow presents itself as the more compliant flowable composite, with Adhese showing intermediate stiffness. Grain analysis of the images confirmed the general rule that the mechanical properties improve with increasing filler loading, with the notable exception of Vertise Flow that shows modulus and hardness as high as 9.1 ± 0.6 and 0.43 ± 0.03 GPa, respectively, for an estimated loading of only ∼40% by volume. Significance Whereas generally flowable composites are confirmed not to possess sufficiently strong mechanical properties for bulk restorations, exceptions can eventually be found upon appropriate laboratory screening, as presently seems to be the case for Vertise Flow. However, real practice in actual restorations and respective clinical evaluation are required for final assessment of the suggested results.</abstract><cop>England</cop><pub>Elsevier Ltd</pub><pmid>22000067</pmid><doi>10.1016/j.dental.2011.08.596</doi><tpages>8</tpages></addata></record> |
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subjects | Acrylic Resins - chemistry Advanced Basic Science Atomic force microscopy Composite Resins - chemistry Compressive Strength Dental materials Dental Materials - chemistry Dental Restoration, Permanent Dentistry Elastic Modulus Hardness Humans Materials Testing Mechanical Phenomena Mechanical properties Microscopy, Atomic Force Microscopy, Electron, Scanning Morphology Nanocomposites - chemistry Nanoindentation Particle Size Pliability Resin Cements - chemistry Restoration Restorative resin composites Scanning electron microscopy Surface Properties Tensile Strength Venus Viscosity |
title | Surface morphology and mechanical properties of new-generation flowable resin composites for dental restoration |
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