Development and application of a polar coating for stir bar sorptive extraction of emerging pollutants from environmental water samples
[Display omitted] ► We prepare a new polar monolithic coating for stir bar sorptive extraction (SBSE). ► The new coating is successfully apply for SBSE polar compounds. ► We develop an effective method to determine polar pollutants in water samples. In the present study, a stir bar coated with hydro...
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| Veröffentlicht in: | Analytica chimica acta 2011-11, Vol.706 (1), p.135-142 |
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| container_title | Analytica chimica acta |
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| creator | Bratkowska, D. Marcé, R.M. Cormack, P.A.G. Borrull, F. Fontanals, N. |
| description | [Display omitted]
► We prepare a new polar monolithic coating for stir bar sorptive extraction (SBSE). ► The new coating is successfully apply for SBSE polar compounds. ► We develop an effective method to determine polar pollutants in water samples.
In the present study, a stir bar coated with hydrophilic polymer based on poly(N-vinylpyrrolidone-co-divinylbenzene) was prepared for the sorptive extraction of polar compounds. The main parameters affecting the polymerisation of the coating were investigated.
The new stir bar was applied successfully in stir bar sorptive extraction with liquid desorption followed by liquid chromatography–mass spectrometry in tandem with a triple quadrupole for the determination of a group of polar pharmaceuticals and personal care products (PPCPs) in environmental water matrices. Different variables affecting extraction and desorption such as agitation speed, temperature, ionic strength and extraction time were optimised. The results showed that the stir bar is able to enrich the selected analytes effectively.
The developed method was applied to determine a group of PPCPs in different complex environmental samples, including river, effluent and influent waste water. |
| doi_str_mv | 10.1016/j.aca.2011.08.028 |
| format | Article |
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► We prepare a new polar monolithic coating for stir bar sorptive extraction (SBSE). ► The new coating is successfully apply for SBSE polar compounds. ► We develop an effective method to determine polar pollutants in water samples.
In the present study, a stir bar coated with hydrophilic polymer based on poly(N-vinylpyrrolidone-co-divinylbenzene) was prepared for the sorptive extraction of polar compounds. The main parameters affecting the polymerisation of the coating were investigated.
The new stir bar was applied successfully in stir bar sorptive extraction with liquid desorption followed by liquid chromatography–mass spectrometry in tandem with a triple quadrupole for the determination of a group of polar pharmaceuticals and personal care products (PPCPs) in environmental water matrices. Different variables affecting extraction and desorption such as agitation speed, temperature, ionic strength and extraction time were optimised. The results showed that the stir bar is able to enrich the selected analytes effectively.
The developed method was applied to determine a group of PPCPs in different complex environmental samples, including river, effluent and influent waste water.</description><identifier>ISSN: 0003-2670</identifier><identifier>EISSN: 1873-4324</identifier><identifier>DOI: 10.1016/j.aca.2011.08.028</identifier><identifier>PMID: 21995920</identifier><identifier>CODEN: ACACAM</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Analysis methods ; Analytical chemistry ; Applied sciences ; Chemistry ; Chromatographic methods and physical methods associated with chromatography ; Coating ; Desorption ; Enrichment ; Environmental water samples ; Exact sciences and technology ; Extraction ; Global environmental pollution ; Liquids ; Mathematical analysis ; Matrices ; Monolithic polar material ; Natural water pollution ; Other chromatographic methods ; Pharmaceuticals and personal care products (PPCPs) ; Pollution ; Polymerization ; Spectrometric and optical methods ; Stir bar sorptive extraction (SBSE) ; Water treatment and pollution</subject><ispartof>Analytica chimica acta, 2011-11, Vol.706 (1), p.135-142</ispartof><rights>2011 Elsevier B.V.</rights><rights>2015 INIST-CNRS</rights><rights>Copyright © 2011 Elsevier B.V. All rights reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c447t-93e297df58c376f5e2664c266b2fcd897a09b241a90fc41cb6a062e781805f693</citedby><cites>FETCH-LOGICAL-c447t-93e297df58c376f5e2664c266b2fcd897a09b241a90fc41cb6a062e781805f693</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.aca.2011.08.028$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=24615399$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/21995920$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Bratkowska, D.</creatorcontrib><creatorcontrib>Marcé, R.M.</creatorcontrib><creatorcontrib>Cormack, P.A.G.</creatorcontrib><creatorcontrib>Borrull, F.</creatorcontrib><creatorcontrib>Fontanals, N.</creatorcontrib><title>Development and application of a polar coating for stir bar sorptive extraction of emerging pollutants from environmental water samples</title><title>Analytica chimica acta</title><addtitle>Anal Chim Acta</addtitle><description>[Display omitted]
► We prepare a new polar monolithic coating for stir bar sorptive extraction (SBSE). ► The new coating is successfully apply for SBSE polar compounds. ► We develop an effective method to determine polar pollutants in water samples.
In the present study, a stir bar coated with hydrophilic polymer based on poly(N-vinylpyrrolidone-co-divinylbenzene) was prepared for the sorptive extraction of polar compounds. The main parameters affecting the polymerisation of the coating were investigated.
The new stir bar was applied successfully in stir bar sorptive extraction with liquid desorption followed by liquid chromatography–mass spectrometry in tandem with a triple quadrupole for the determination of a group of polar pharmaceuticals and personal care products (PPCPs) in environmental water matrices. Different variables affecting extraction and desorption such as agitation speed, temperature, ionic strength and extraction time were optimised. The results showed that the stir bar is able to enrich the selected analytes effectively.
The developed method was applied to determine a group of PPCPs in different complex environmental samples, including river, effluent and influent waste water.</description><subject>Analysis methods</subject><subject>Analytical chemistry</subject><subject>Applied sciences</subject><subject>Chemistry</subject><subject>Chromatographic methods and physical methods associated with chromatography</subject><subject>Coating</subject><subject>Desorption</subject><subject>Enrichment</subject><subject>Environmental water samples</subject><subject>Exact sciences and technology</subject><subject>Extraction</subject><subject>Global environmental pollution</subject><subject>Liquids</subject><subject>Mathematical analysis</subject><subject>Matrices</subject><subject>Monolithic polar material</subject><subject>Natural water pollution</subject><subject>Other chromatographic methods</subject><subject>Pharmaceuticals and personal care products (PPCPs)</subject><subject>Pollution</subject><subject>Polymerization</subject><subject>Spectrometric and optical methods</subject><subject>Stir bar sorptive extraction (SBSE)</subject><subject>Water treatment and pollution</subject><issn>0003-2670</issn><issn>1873-4324</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqFkcuO1DAQRSMEYpqBD2CDvEGwSbCdxA-xQsNTGokNrK2KUx65lcTBdjfwBfw2Dt0Du2Hjkkvn3irVraqnjDaMMvFq34CFhlPGGqoaytW9aseUbOuu5d39akcpbWsuJL2oHqW0L1_OaPewuuBM615zuqt-vcUjTmGdcckElpHAuk7eQvZhIcERIGuYIBIbSmu5IS5EkrKPZCjNFOKa_REJ_sgR7K0GZ4w3G1yk0yHDkhNxMcwEl6OPYdlmwUS-Q8biAfM6YXpcPXAwJXxyrpfV1_fvvlx9rK8_f_h09ea6tl0nc61b5FqOrle2lcL1yIXobHkG7uyotASqB94x0NTZjtlBABUcpWKK9k7o9rJ6cfJdY_h2wJTN7JPFaYIFwyEZLVrVUSX6_5JKq55KKTfPl3eSTEhWPNs_KDuhNoaUIjqzRj9D_GkYNVumZm9KpmbL1FBlSqZF8-xsfxhmHP8qbkMswPMzAMnC5CIs1qd_XCdY3-pt-OsTh-XAR4_RJOtxsTj6iDabMfg71vgNNhDATw</recordid><startdate>20111107</startdate><enddate>20111107</enddate><creator>Bratkowska, D.</creator><creator>Marcé, R.M.</creator><creator>Cormack, P.A.G.</creator><creator>Borrull, F.</creator><creator>Fontanals, N.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope><scope>7X8</scope><scope>7TV</scope><scope>C1K</scope></search><sort><creationdate>20111107</creationdate><title>Development and application of a polar coating for stir bar sorptive extraction of emerging pollutants from environmental water samples</title><author>Bratkowska, D. ; Marcé, R.M. ; Cormack, P.A.G. ; Borrull, F. ; Fontanals, N.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c447t-93e297df58c376f5e2664c266b2fcd897a09b241a90fc41cb6a062e781805f693</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Analysis methods</topic><topic>Analytical chemistry</topic><topic>Applied sciences</topic><topic>Chemistry</topic><topic>Chromatographic methods and physical methods associated with chromatography</topic><topic>Coating</topic><topic>Desorption</topic><topic>Enrichment</topic><topic>Environmental water samples</topic><topic>Exact sciences and technology</topic><topic>Extraction</topic><topic>Global environmental pollution</topic><topic>Liquids</topic><topic>Mathematical analysis</topic><topic>Matrices</topic><topic>Monolithic polar material</topic><topic>Natural water pollution</topic><topic>Other chromatographic methods</topic><topic>Pharmaceuticals and personal care products (PPCPs)</topic><topic>Pollution</topic><topic>Polymerization</topic><topic>Spectrometric and optical methods</topic><topic>Stir bar sorptive extraction (SBSE)</topic><topic>Water treatment and pollution</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bratkowska, D.</creatorcontrib><creatorcontrib>Marcé, R.M.</creatorcontrib><creatorcontrib>Cormack, P.A.G.</creatorcontrib><creatorcontrib>Borrull, F.</creatorcontrib><creatorcontrib>Fontanals, N.</creatorcontrib><collection>Pascal-Francis</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><collection>Pollution Abstracts</collection><collection>Environmental Sciences and Pollution Management</collection><jtitle>Analytica chimica acta</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bratkowska, D.</au><au>Marcé, R.M.</au><au>Cormack, P.A.G.</au><au>Borrull, F.</au><au>Fontanals, N.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Development and application of a polar coating for stir bar sorptive extraction of emerging pollutants from environmental water samples</atitle><jtitle>Analytica chimica acta</jtitle><addtitle>Anal Chim Acta</addtitle><date>2011-11-07</date><risdate>2011</risdate><volume>706</volume><issue>1</issue><spage>135</spage><epage>142</epage><pages>135-142</pages><issn>0003-2670</issn><eissn>1873-4324</eissn><coden>ACACAM</coden><abstract>[Display omitted]
► We prepare a new polar monolithic coating for stir bar sorptive extraction (SBSE). ► The new coating is successfully apply for SBSE polar compounds. ► We develop an effective method to determine polar pollutants in water samples.
In the present study, a stir bar coated with hydrophilic polymer based on poly(N-vinylpyrrolidone-co-divinylbenzene) was prepared for the sorptive extraction of polar compounds. The main parameters affecting the polymerisation of the coating were investigated.
The new stir bar was applied successfully in stir bar sorptive extraction with liquid desorption followed by liquid chromatography–mass spectrometry in tandem with a triple quadrupole for the determination of a group of polar pharmaceuticals and personal care products (PPCPs) in environmental water matrices. Different variables affecting extraction and desorption such as agitation speed, temperature, ionic strength and extraction time were optimised. The results showed that the stir bar is able to enrich the selected analytes effectively.
The developed method was applied to determine a group of PPCPs in different complex environmental samples, including river, effluent and influent waste water.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><pmid>21995920</pmid><doi>10.1016/j.aca.2011.08.028</doi><tpages>8</tpages></addata></record> |
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| source | ScienceDirect Journals (5 years ago - present) |
| subjects | Analysis methods Analytical chemistry Applied sciences Chemistry Chromatographic methods and physical methods associated with chromatography Coating Desorption Enrichment Environmental water samples Exact sciences and technology Extraction Global environmental pollution Liquids Mathematical analysis Matrices Monolithic polar material Natural water pollution Other chromatographic methods Pharmaceuticals and personal care products (PPCPs) Pollution Polymerization Spectrometric and optical methods Stir bar sorptive extraction (SBSE) Water treatment and pollution |
| title | Development and application of a polar coating for stir bar sorptive extraction of emerging pollutants from environmental water samples |
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