Dissolution and Delignification of Bamboo Biomass Using Amino Acid-Based Ionic Liquid
In the present work, the dissolution of bamboo biomass was tested using a number of ionic liquids synthesized in laboratory. It was observed that one of the synthesized amino acid-based ionic liquids, namely 1-ethyl-3-methylimidazolium glycinate, was capable of dissolving the biomass completely. The...
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| Veröffentlicht in: | Applied biochemistry and biotechnology 2011-10, Vol.165 (3-4), p.998-1009 |
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| creator | Muhammad, Nawshad Man, Zakaria Bustam, Mohamad Azmi Mutalib, M. I. Abdul Wilfred, Cecilia D. Rafiq, Sikander |
| description | In the present work, the dissolution of bamboo biomass was tested using a number of ionic liquids synthesized in laboratory. It was observed that one of the synthesized amino acid-based ionic liquids, namely 1-ethyl-3-methylimidazolium glycinate, was capable of dissolving the biomass completely. The dissolved biomass was then regenerated using a reconstitute solvent (acetone/water) and was characterized using Fourier transform infrared spectroscopy, X-ray diffraction, and scanning electron microscopy. The results were compared to preconditioned bamboo biomass. The regenerated biomass was found to have a more homogenous macrostructure, which indicates that the crystalline form and structure of its cellulose has changed from type Ι to type ΙΙ during the dissolution and regeneration process. |
| doi_str_mv | 10.1007/s12010-011-9315-y |
| format | Article |
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I. Abdul ; Wilfred, Cecilia D. ; Rafiq, Sikander</creator><creatorcontrib>Muhammad, Nawshad ; Man, Zakaria ; Bustam, Mohamad Azmi ; Mutalib, M. I. Abdul ; Wilfred, Cecilia D. ; Rafiq, Sikander</creatorcontrib><description>In the present work, the dissolution of bamboo biomass was tested using a number of ionic liquids synthesized in laboratory. It was observed that one of the synthesized amino acid-based ionic liquids, namely 1-ethyl-3-methylimidazolium glycinate, was capable of dissolving the biomass completely. The dissolved biomass was then regenerated using a reconstitute solvent (acetone/water) and was characterized using Fourier transform infrared spectroscopy, X-ray diffraction, and scanning electron microscopy. The results were compared to preconditioned bamboo biomass. The regenerated biomass was found to have a more homogenous macrostructure, which indicates that the crystalline form and structure of its cellulose has changed from type Ι to type ΙΙ during the dissolution and regeneration process.</description><identifier>ISSN: 0273-2289</identifier><identifier>EISSN: 1559-0291</identifier><identifier>DOI: 10.1007/s12010-011-9315-y</identifier><identifier>PMID: 21720837</identifier><identifier>CODEN: ABIBDL</identifier><language>eng</language><publisher>New York: Humana Press Inc</publisher><subject>Amino acids ; Amino Acids - chemistry ; Amino Acids - metabolism ; Bamboo ; Bambusa - metabolism ; Biochemistry ; Biological and medical sciences ; Biomass ; Biotechnology ; Biotechnology - methods ; Cellulose ; Chemistry ; Chemistry and Materials Science ; Crystallization ; Fourier transforms ; Fundamental and applied biological sciences. Psychology ; Imidazoles - chemistry ; Infrared spectroscopy ; Ionic Liquids - chemistry ; Ions ; Lignin - chemistry ; Lignin - metabolism ; Microscopy, Electron, Scanning ; Solubility ; Spectroscopy, Fourier Transform Infrared ; Water ; X-Ray Diffraction</subject><ispartof>Applied biochemistry and biotechnology, 2011-10, Vol.165 (3-4), p.998-1009</ispartof><rights>Springer Science+Business Media, LLC 2011</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c498t-fc720ae6eb823777fdcecb63e10abbeff28dabadb01f4f992654ede66929961a3</citedby><cites>FETCH-LOGICAL-c498t-fc720ae6eb823777fdcecb63e10abbeff28dabadb01f4f992654ede66929961a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s12010-011-9315-y$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s12010-011-9315-y$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27903,27904,41467,42536,51297</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=25293369$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/21720837$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Muhammad, Nawshad</creatorcontrib><creatorcontrib>Man, Zakaria</creatorcontrib><creatorcontrib>Bustam, Mohamad Azmi</creatorcontrib><creatorcontrib>Mutalib, M. I. Abdul</creatorcontrib><creatorcontrib>Wilfred, Cecilia D.</creatorcontrib><creatorcontrib>Rafiq, Sikander</creatorcontrib><title>Dissolution and Delignification of Bamboo Biomass Using Amino Acid-Based Ionic Liquid</title><title>Applied biochemistry and biotechnology</title><addtitle>Appl Biochem Biotechnol</addtitle><addtitle>Appl Biochem Biotechnol</addtitle><description>In the present work, the dissolution of bamboo biomass was tested using a number of ionic liquids synthesized in laboratory. It was observed that one of the synthesized amino acid-based ionic liquids, namely 1-ethyl-3-methylimidazolium glycinate, was capable of dissolving the biomass completely. The dissolved biomass was then regenerated using a reconstitute solvent (acetone/water) and was characterized using Fourier transform infrared spectroscopy, X-ray diffraction, and scanning electron microscopy. The results were compared to preconditioned bamboo biomass. The regenerated biomass was found to have a more homogenous macrostructure, which indicates that the crystalline form and structure of its cellulose has changed from type Ι to type ΙΙ during the dissolution and regeneration process.</description><subject>Amino acids</subject><subject>Amino Acids - chemistry</subject><subject>Amino Acids - metabolism</subject><subject>Bamboo</subject><subject>Bambusa - metabolism</subject><subject>Biochemistry</subject><subject>Biological and medical sciences</subject><subject>Biomass</subject><subject>Biotechnology</subject><subject>Biotechnology - methods</subject><subject>Cellulose</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Crystallization</subject><subject>Fourier transforms</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>Imidazoles - chemistry</subject><subject>Infrared spectroscopy</subject><subject>Ionic Liquids - chemistry</subject><subject>Ions</subject><subject>Lignin - chemistry</subject><subject>Lignin - metabolism</subject><subject>Microscopy, Electron, Scanning</subject><subject>Solubility</subject><subject>Spectroscopy, Fourier Transform Infrared</subject><subject>Water</subject><subject>X-Ray Diffraction</subject><issn>0273-2289</issn><issn>1559-0291</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><sourceid>BENPR</sourceid><recordid>eNqFkc1uEzEUhS0EomnhAdggCwmxGvD1ZPyzTFoKlSKxIWvL45_I1Yzdzs0s8vZ1SKASEmJlyf7O9bn6CHkH7DMwJr8gcAasYQCNbqFrDi_IArpON4xreEkWjMu24VzpC3KJeM8YcNXJ1-SCg-RMtXJBtjcJsQzzPpVMbfb0Jgxpl1NMzv66K5Gu7diXQtepjBaRbjHlHV2NKRe6csk3a4vB07uSk6Ob9Dgn_4a8inbA8PZ8XpHt7def19-bzY9vd9erTeOWWu2b6GoNG0ToFW-llNG74HrRBmC270OMXHnbW98ziMuoNRfdMvgghOZaC7DtFfl0mvswlcc54N6MCV0YBptDmdHUhFJCKP1_knEhOwWqkh_-Iu_LPOW6xhGqFaSCCsEJclNBnEI0D1Ma7XQwwMzRjTm5MdWNOboxh5p5fx4892PwfxK_ZVTg4xmw6OwQJ5tdwmeu47ptxXEXfuKwPuVdmJ4b_vv3J3o-pnY</recordid><startdate>20111001</startdate><enddate>20111001</enddate><creator>Muhammad, Nawshad</creator><creator>Man, Zakaria</creator><creator>Bustam, Mohamad Azmi</creator><creator>Mutalib, M. 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I. Abdul ; Wilfred, Cecilia D. ; Rafiq, Sikander</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c498t-fc720ae6eb823777fdcecb63e10abbeff28dabadb01f4f992654ede66929961a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Amino acids</topic><topic>Amino Acids - chemistry</topic><topic>Amino Acids - metabolism</topic><topic>Bamboo</topic><topic>Bambusa - metabolism</topic><topic>Biochemistry</topic><topic>Biological and medical sciences</topic><topic>Biomass</topic><topic>Biotechnology</topic><topic>Biotechnology - methods</topic><topic>Cellulose</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Crystallization</topic><topic>Fourier transforms</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>Imidazoles - chemistry</topic><topic>Infrared spectroscopy</topic><topic>Ionic Liquids - chemistry</topic><topic>Ions</topic><topic>Lignin - chemistry</topic><topic>Lignin - metabolism</topic><topic>Microscopy, Electron, Scanning</topic><topic>Solubility</topic><topic>Spectroscopy, Fourier Transform Infrared</topic><topic>Water</topic><topic>X-Ray Diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Muhammad, Nawshad</creatorcontrib><creatorcontrib>Man, Zakaria</creatorcontrib><creatorcontrib>Bustam, Mohamad Azmi</creatorcontrib><creatorcontrib>Mutalib, M. I. 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I. Abdul</au><au>Wilfred, Cecilia D.</au><au>Rafiq, Sikander</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Dissolution and Delignification of Bamboo Biomass Using Amino Acid-Based Ionic Liquid</atitle><jtitle>Applied biochemistry and biotechnology</jtitle><stitle>Appl Biochem Biotechnol</stitle><addtitle>Appl Biochem Biotechnol</addtitle><date>2011-10-01</date><risdate>2011</risdate><volume>165</volume><issue>3-4</issue><spage>998</spage><epage>1009</epage><pages>998-1009</pages><issn>0273-2289</issn><eissn>1559-0291</eissn><coden>ABIBDL</coden><abstract>In the present work, the dissolution of bamboo biomass was tested using a number of ionic liquids synthesized in laboratory. It was observed that one of the synthesized amino acid-based ionic liquids, namely 1-ethyl-3-methylimidazolium glycinate, was capable of dissolving the biomass completely. The dissolved biomass was then regenerated using a reconstitute solvent (acetone/water) and was characterized using Fourier transform infrared spectroscopy, X-ray diffraction, and scanning electron microscopy. The results were compared to preconditioned bamboo biomass. The regenerated biomass was found to have a more homogenous macrostructure, which indicates that the crystalline form and structure of its cellulose has changed from type Ι to type ΙΙ during the dissolution and regeneration process.</abstract><cop>New York</cop><pub>Humana Press Inc</pub><pmid>21720837</pmid><doi>10.1007/s12010-011-9315-y</doi><tpages>12</tpages></addata></record> |
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| subjects | Amino acids Amino Acids - chemistry Amino Acids - metabolism Bamboo Bambusa - metabolism Biochemistry Biological and medical sciences Biomass Biotechnology Biotechnology - methods Cellulose Chemistry Chemistry and Materials Science Crystallization Fourier transforms Fundamental and applied biological sciences. Psychology Imidazoles - chemistry Infrared spectroscopy Ionic Liquids - chemistry Ions Lignin - chemistry Lignin - metabolism Microscopy, Electron, Scanning Solubility Spectroscopy, Fourier Transform Infrared Water X-Ray Diffraction |
| title | Dissolution and Delignification of Bamboo Biomass Using Amino Acid-Based Ionic Liquid |
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