Atmospheric pressure aminocarbonylation of aryl iodides using palladium nanoparticles supported on MOF-5

An efficient amide synthesis by atmospheric pressure aminocarbonylation using palladium nanoparticles supported on MOF-5 is reported. Interestingly, only 0.5 wt% palladium loading was required to achieve high yields. The catalyst is recyclable and offers negligible palladium leaching.

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Bibliographische Detailangaben
Veröffentlicht in:	Chemical communications (Cambridge, England) England), 2012-01, Vol.48 (12), p.1805-1807
Hauptverfasser:	Dang, Tuan T, Zhu, Yinghuai, Ghosh, Subhash C, Chen, Anqi, Chai, Christina L L, Seayad, Abdul M
Format:	Artikel
Sprache:	eng
Schlagworte:	Amides Amines - chemistry Atmospheric Pressure Barometric pressure Catalysis Hydrocarbons, Aromatic - chemical synthesis Hydrocarbons, Aromatic - chemistry Iodides Iodides - chemical synthesis Iodides - chemistry Leaching Nanoparticles Nanoparticles - chemistry Nanoparticles - ultrastructure Organometallic Compounds - chemistry Palladium Palladium - chemistry Synthesis
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Beschreibung
Zusammenfassung:	An efficient amide synthesis by atmospheric pressure aminocarbonylation using palladium nanoparticles supported on MOF-5 is reported. Interestingly, only 0.5 wt% palladium loading was required to achieve high yields. The catalyst is recyclable and offers negligible palladium leaching.
ISSN:	1359-7345 1364-548X
DOI:	10.1039/c2cc16808a