Synthesis and characterization of novel four-arm star PDMAEMA-stabilized colloidal silver nanoparticles
Spontaneous formation and efficient stabilization of colloidal silver nanoparticles were achieved in aqueous four-arm star poly(N,N-dimethylaminoethyl methacrylate) (PDMAEMA) solution at ambient temperature in the absence of any other reducing agent. In this reaction, four-arm star PDMAEMA acted as...
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| Veröffentlicht in: | Colloid and polymer science 2010-12, Vol.288 (18), p.1713-1722 |
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| creator | Sun, Huaming Gao, Ziwei Yang, Lin Gao, Lingxiang Lv, Xushe |
| description | Spontaneous formation and efficient stabilization of colloidal silver nanoparticles were achieved in aqueous four-arm star poly(N,N-dimethylaminoethyl methacrylate) (PDMAEMA) solution at ambient temperature in the absence of any other reducing agent. In this reaction, four-arm star PDMAEMA acted as both reducing and stabilizing agents for silver nanoparticles. More importantly, four-arm star PDMAEMA is a tertiary-amine-containing star homopolymer, which shows that the scope of the reducing and stabilizing agents for metal nanoparticles can be extended from the general homopolymers and the block copolymers to the water-soluble simple tertiary-amine-containing star homopolymers. Fourier transform infrared, UV-vis absorption spectroscopy, and transmission electron microscopy were used to characterize the synthetic silver nanoparticles. A plausible mechanism for the formation of silver nanoparticles was proposed in the presence of linear and star PDMAEMA homopolymers. Moreover, the size of the resultant silver nanoparticles can be easily tuned by changing the concentrations of AgNO₃. |
| doi_str_mv | 10.1007/s00396-010-2290-y |
| format | Article |
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In this reaction, four-arm star PDMAEMA acted as both reducing and stabilizing agents for silver nanoparticles. More importantly, four-arm star PDMAEMA is a tertiary-amine-containing star homopolymer, which shows that the scope of the reducing and stabilizing agents for metal nanoparticles can be extended from the general homopolymers and the block copolymers to the water-soluble simple tertiary-amine-containing star homopolymers. Fourier transform infrared, UV-vis absorption spectroscopy, and transmission electron microscopy were used to characterize the synthetic silver nanoparticles. A plausible mechanism for the formation of silver nanoparticles was proposed in the presence of linear and star PDMAEMA homopolymers. 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Gao, Ziwei ; Yang, Lin ; Gao, Lingxiang ; Lv, Xushe</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c468t-18a5bfdcf82e20bb9d2dbcc8f2f6ba5fce057f07b99c2ef98ee384b8e1ee7173</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Absorption spectroscopy</topic><topic>Ambient temperature</topic><topic>Applied sciences</topic><topic>Atom transfer radical polymerization (ATRP)</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Colloidal silver nanoparticles</topic><topic>Colloids</topic><topic>Complex Fluids and Microfluidics</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Exact sciences and technology</topic><topic>Food Science</topic><topic>Fourier transforms</topic><topic>Infrared</topic><topic>Materials science</topic><topic>Nanoparticles</topic><topic>Nanopowders</topic><topic>Nanoscale materials and structures: fabrication and characterization</topic><topic>Nanotechnology and Microengineering</topic><topic>Organic polymers</topic><topic>Original Contribution</topic><topic>Physical Chemistry</topic><topic>Physicochemistry of polymers</topic><topic>Physics</topic><topic>Polymer Sciences</topic><topic>Polymers with particular properties</topic><topic>Preparation, kinetics, thermodynamics, mechanism and catalysts</topic><topic>Silver</topic><topic>Soft and Granular Matter</topic><topic>Stabilization</topic><topic>Star polymers</topic><topic>Stars</topic><topic>Water-soluble polymers</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sun, Huaming</creatorcontrib><creatorcontrib>Gao, Ziwei</creatorcontrib><creatorcontrib>Yang, Lin</creatorcontrib><creatorcontrib>Gao, Lingxiang</creatorcontrib><creatorcontrib>Lv, Xushe</creatorcontrib><collection>AGRIS</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection (ProQuest)</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><jtitle>Colloid and polymer science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sun, Huaming</au><au>Gao, Ziwei</au><au>Yang, Lin</au><au>Gao, Lingxiang</au><au>Lv, Xushe</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and characterization of novel four-arm star PDMAEMA-stabilized colloidal silver nanoparticles</atitle><jtitle>Colloid and polymer science</jtitle><stitle>Colloid Polym Sci</stitle><date>2010-12-01</date><risdate>2010</risdate><volume>288</volume><issue>18</issue><spage>1713</spage><epage>1722</epage><pages>1713-1722</pages><issn>0303-402X</issn><eissn>1435-1536</eissn><coden>CPMSB6</coden><abstract>Spontaneous formation and efficient stabilization of colloidal silver nanoparticles were achieved in aqueous four-arm star poly(N,N-dimethylaminoethyl methacrylate) (PDMAEMA) solution at ambient temperature in the absence of any other reducing agent. In this reaction, four-arm star PDMAEMA acted as both reducing and stabilizing agents for silver nanoparticles. More importantly, four-arm star PDMAEMA is a tertiary-amine-containing star homopolymer, which shows that the scope of the reducing and stabilizing agents for metal nanoparticles can be extended from the general homopolymers and the block copolymers to the water-soluble simple tertiary-amine-containing star homopolymers. Fourier transform infrared, UV-vis absorption spectroscopy, and transmission electron microscopy were used to characterize the synthetic silver nanoparticles. A plausible mechanism for the formation of silver nanoparticles was proposed in the presence of linear and star PDMAEMA homopolymers. Moreover, the size of the resultant silver nanoparticles can be easily tuned by changing the concentrations of AgNO₃.</abstract><cop>Berlin/Heidelberg</cop><pub>Berlin/Heidelberg : Springer-Verlag</pub><doi>10.1007/s00396-010-2290-y</doi><tpages>10</tpages></addata></record> |
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| subjects | Absorption spectroscopy Ambient temperature Applied sciences Atom transfer radical polymerization (ATRP) Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Colloidal silver nanoparticles Colloids Complex Fluids and Microfluidics Cross-disciplinary physics: materials science rheology Exact sciences and technology Food Science Fourier transforms Infrared Materials science Nanoparticles Nanopowders Nanoscale materials and structures: fabrication and characterization Nanotechnology and Microengineering Organic polymers Original Contribution Physical Chemistry Physicochemistry of polymers Physics Polymer Sciences Polymers with particular properties Preparation, kinetics, thermodynamics, mechanism and catalysts Silver Soft and Granular Matter Stabilization Star polymers Stars Water-soluble polymers |
| title | Synthesis and characterization of novel four-arm star PDMAEMA-stabilized colloidal silver nanoparticles |
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