Synthesis of Ag nanoparticle-decorated 2,4,6-tris(2-pyridyl)-1,3,5-triazine nanobelts and their application for H2O2 and glucose detection
The present paper reports on the first preparation of 2,4,6-tris(2-pyridyl)-1,3,5-triazine nanobelts (TPTNBs) by adjusting the pH value of the solution and the subsequent synthesis of Ag nanoparticle (AgNP)-decorated TPTNBs (AgNP-TPTNBs) by mixing an aqueous AgNO(3) solution with preformed TPTNBs wi...
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| Veröffentlicht in: | Analyst (London) 2012-02, Vol.137 (4), p.939-943 |
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| creator | XIAOYUN QIN WENBO LU YONGLAN LUO GUOHUI CHANG ASIRI, Abdullah M AL-YOUBI, Abdulrahman O XUPING SUN |
| description | The present paper reports on the first preparation of 2,4,6-tris(2-pyridyl)-1,3,5-triazine nanobelts (TPTNBs) by adjusting the pH value of the solution and the subsequent synthesis of Ag nanoparticle (AgNP)-decorated TPTNBs (AgNP-TPTNBs) by mixing an aqueous AgNO(3) solution with preformed TPTNBs without use of any external reducing agent. It is found that the resultant AgNP-TPTNBs exhibit notable catalytic performance for H(2)O(2) reduction. A glucose biosensor was fabricated by immobilizing glucose oxidase (GOD) onto a AgNP-TPTNBs-modified glassy carbon electrode (GCE) for glucose detection. The constructed glucose sensor has a wide linear response range from 3 mM to 20 mM (r: 0.999) with a detection limit of 190 μM. It is further shown that this glucose biosensor can be used for glucose detection in human blood serum. |
| doi_str_mv | 10.1039/c2an15996a |
| format | Article |
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It is found that the resultant AgNP-TPTNBs exhibit notable catalytic performance for H(2)O(2) reduction. A glucose biosensor was fabricated by immobilizing glucose oxidase (GOD) onto a AgNP-TPTNBs-modified glassy carbon electrode (GCE) for glucose detection. The constructed glucose sensor has a wide linear response range from 3 mM to 20 mM (r: 0.999) with a detection limit of 190 μM. It is further shown that this glucose biosensor can be used for glucose detection in human blood serum.</description><identifier>ISSN: 0003-2654</identifier><identifier>EISSN: 1364-5528</identifier><identifier>DOI: 10.1039/c2an15996a</identifier><identifier>PMID: 22179818</identifier><identifier>CODEN: ANALAO</identifier><language>eng</language><publisher>Cambridge: Royal Society of Chemistry</publisher><subject>Analytical chemistry ; Biological and medical sciences ; Biosensing Techniques - methods ; Biosensors ; Biotechnology ; Blood Glucose - analysis ; Chemistry ; Exact sciences and technology ; Fundamental and applied biological sciences. Psychology ; General, instrumentation ; Glucose - analysis ; Glucose Oxidase - chemistry ; Humans ; Hydrogen Peroxide - analysis ; Limit of Detection ; Metal Nanoparticles - chemistry ; Methods. Procedures. Technologies ; Nanocomposites ; Pyridines - chemistry ; Silver - chemistry ; Triazines - chemistry ; Various methods and equipments</subject><ispartof>Analyst (London), 2012-02, Vol.137 (4), p.939-943</ispartof><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27923,27924</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=25567168$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/22179818$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>XIAOYUN QIN</creatorcontrib><creatorcontrib>WENBO LU</creatorcontrib><creatorcontrib>YONGLAN LUO</creatorcontrib><creatorcontrib>GUOHUI CHANG</creatorcontrib><creatorcontrib>ASIRI, Abdullah M</creatorcontrib><creatorcontrib>AL-YOUBI, Abdulrahman O</creatorcontrib><creatorcontrib>XUPING SUN</creatorcontrib><title>Synthesis of Ag nanoparticle-decorated 2,4,6-tris(2-pyridyl)-1,3,5-triazine nanobelts and their application for H2O2 and glucose detection</title><title>Analyst (London)</title><addtitle>Analyst</addtitle><description>The present paper reports on the first preparation of 2,4,6-tris(2-pyridyl)-1,3,5-triazine nanobelts (TPTNBs) by adjusting the pH value of the solution and the subsequent synthesis of Ag nanoparticle (AgNP)-decorated TPTNBs (AgNP-TPTNBs) by mixing an aqueous AgNO(3) solution with preformed TPTNBs without use of any external reducing agent. It is found that the resultant AgNP-TPTNBs exhibit notable catalytic performance for H(2)O(2) reduction. A glucose biosensor was fabricated by immobilizing glucose oxidase (GOD) onto a AgNP-TPTNBs-modified glassy carbon electrode (GCE) for glucose detection. The constructed glucose sensor has a wide linear response range from 3 mM to 20 mM (r: 0.999) with a detection limit of 190 μM. It is further shown that this glucose biosensor can be used for glucose detection in human blood serum.</description><subject>Analytical chemistry</subject><subject>Biological and medical sciences</subject><subject>Biosensing Techniques - methods</subject><subject>Biosensors</subject><subject>Biotechnology</subject><subject>Blood Glucose - analysis</subject><subject>Chemistry</subject><subject>Exact sciences and technology</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>General, instrumentation</subject><subject>Glucose - analysis</subject><subject>Glucose Oxidase - chemistry</subject><subject>Humans</subject><subject>Hydrogen Peroxide - analysis</subject><subject>Limit of Detection</subject><subject>Metal Nanoparticles - chemistry</subject><subject>Methods. Procedures. Technologies</subject><subject>Nanocomposites</subject><subject>Pyridines - chemistry</subject><subject>Silver - chemistry</subject><subject>Triazines - chemistry</subject><subject>Various methods and equipments</subject><issn>0003-2654</issn><issn>1364-5528</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNpFkL1OKzEUhC0Eglyg4QGQGwRXisH_WZcR4l6QkCiAOjrrtcHI8S62U4RH4KlZIIjq6Mx8M8UgdMToOaPCXFgOiSljNGyhCRNaEqV4s40mlFJBuFZyD_0p5WV8GVV0F-1xzmamYc0Evd-vU312JRTcezx_wglSP0CuwUZHOmf7DNV1mE_lVJOaQznjZFjn0K3jX8KmYqo-VXgLyX1lWxdrwZA6PNaGjGEYYrBQQ5-w7zO-5nf8y36KK9sXhztXnf20D9COh1jc4ebuo8d_Vw-X1-T27v_N5fyWDFzSStiMttILI6z3LTgtm46NCqO67VQrqbWjQ03rBTecSy6o4TPwWiphmLJS7KPT794h968rV-piGYp1MUJy_aosDGvomNVmJI835Kpdum4x5LCEvF78zDcCJxsAioXoMyQbyi-nlJ4x3YgPMsd9Xg</recordid><startdate>20120221</startdate><enddate>20120221</enddate><creator>XIAOYUN QIN</creator><creator>WENBO LU</creator><creator>YONGLAN LUO</creator><creator>GUOHUI CHANG</creator><creator>ASIRI, Abdullah M</creator><creator>AL-YOUBI, Abdulrahman O</creator><creator>XUPING SUN</creator><general>Royal Society of Chemistry</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>7X8</scope></search><sort><creationdate>20120221</creationdate><title>Synthesis of Ag nanoparticle-decorated 2,4,6-tris(2-pyridyl)-1,3,5-triazine nanobelts and their application for H2O2 and glucose detection</title><author>XIAOYUN QIN ; WENBO LU ; YONGLAN LUO ; GUOHUI CHANG ; ASIRI, Abdullah M ; AL-YOUBI, Abdulrahman O ; XUPING SUN</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p240t-170b4f393cffbae648d10b4106bd5b40cc3cf09bf329224230927af6453915c43</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Analytical chemistry</topic><topic>Biological and medical sciences</topic><topic>Biosensing Techniques - methods</topic><topic>Biosensors</topic><topic>Biotechnology</topic><topic>Blood Glucose - analysis</topic><topic>Chemistry</topic><topic>Exact sciences and technology</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>General, instrumentation</topic><topic>Glucose - analysis</topic><topic>Glucose Oxidase - chemistry</topic><topic>Humans</topic><topic>Hydrogen Peroxide - analysis</topic><topic>Limit of Detection</topic><topic>Metal Nanoparticles - chemistry</topic><topic>Methods. Procedures. Technologies</topic><topic>Nanocomposites</topic><topic>Pyridines - chemistry</topic><topic>Silver - chemistry</topic><topic>Triazines - chemistry</topic><topic>Various methods and equipments</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>XIAOYUN QIN</creatorcontrib><creatorcontrib>WENBO LU</creatorcontrib><creatorcontrib>YONGLAN LUO</creatorcontrib><creatorcontrib>GUOHUI CHANG</creatorcontrib><creatorcontrib>ASIRI, Abdullah M</creatorcontrib><creatorcontrib>AL-YOUBI, Abdulrahman O</creatorcontrib><creatorcontrib>XUPING SUN</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>MEDLINE - Academic</collection><jtitle>Analyst (London)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>XIAOYUN QIN</au><au>WENBO LU</au><au>YONGLAN LUO</au><au>GUOHUI CHANG</au><au>ASIRI, Abdullah M</au><au>AL-YOUBI, Abdulrahman O</au><au>XUPING SUN</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of Ag nanoparticle-decorated 2,4,6-tris(2-pyridyl)-1,3,5-triazine nanobelts and their application for H2O2 and glucose detection</atitle><jtitle>Analyst (London)</jtitle><addtitle>Analyst</addtitle><date>2012-02-21</date><risdate>2012</risdate><volume>137</volume><issue>4</issue><spage>939</spage><epage>943</epage><pages>939-943</pages><issn>0003-2654</issn><eissn>1364-5528</eissn><coden>ANALAO</coden><abstract>The present paper reports on the first preparation of 2,4,6-tris(2-pyridyl)-1,3,5-triazine nanobelts (TPTNBs) by adjusting the pH value of the solution and the subsequent synthesis of Ag nanoparticle (AgNP)-decorated TPTNBs (AgNP-TPTNBs) by mixing an aqueous AgNO(3) solution with preformed TPTNBs without use of any external reducing agent. It is found that the resultant AgNP-TPTNBs exhibit notable catalytic performance for H(2)O(2) reduction. A glucose biosensor was fabricated by immobilizing glucose oxidase (GOD) onto a AgNP-TPTNBs-modified glassy carbon electrode (GCE) for glucose detection. The constructed glucose sensor has a wide linear response range from 3 mM to 20 mM (r: 0.999) with a detection limit of 190 μM. It is further shown that this glucose biosensor can be used for glucose detection in human blood serum.</abstract><cop>Cambridge</cop><pub>Royal Society of Chemistry</pub><pmid>22179818</pmid><doi>10.1039/c2an15996a</doi><tpages>5</tpages></addata></record> |
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| source | MEDLINE; Royal Society of Chemistry Journals Archive (1841-2007); Royal Society Of Chemistry Journals 2008-; Alma/SFX Local Collection |
| subjects | Analytical chemistry Biological and medical sciences Biosensing Techniques - methods Biosensors Biotechnology Blood Glucose - analysis Chemistry Exact sciences and technology Fundamental and applied biological sciences. Psychology General, instrumentation Glucose - analysis Glucose Oxidase - chemistry Humans Hydrogen Peroxide - analysis Limit of Detection Metal Nanoparticles - chemistry Methods. Procedures. Technologies Nanocomposites Pyridines - chemistry Silver - chemistry Triazines - chemistry Various methods and equipments |
| title | Synthesis of Ag nanoparticle-decorated 2,4,6-tris(2-pyridyl)-1,3,5-triazine nanobelts and their application for H2O2 and glucose detection |
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