Hydrolysis behavior of a precursor for bridged polysilsesquioxane 1,4-bis(triethoxysilyl)benzene: a 29Si NMR study

The hydrolysis behavior of 1,4-bis(triethoxysilyl)benzene (BTB), a precursor of bridged polysilsesquioxane, was investigated with high-resolution 29 Si nuclear magnetic resonance ( 29 Si NMR) spectroscopy at ambient temperature in a system with BTB:ethanol:water:HCl = 1:10: x :0.8 × 10 −4 ( x = 3,...

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Veröffentlicht in:	Journal of sol-gel science and technology 2011, Vol.57 (1), p.51-56
Hauptverfasser:	Saito, Hitomi, Nishio, Yuki, Kobayashi, Manabu, Sugahara, Yoshiyuki
Format:	Artikel
Sprache:	eng
Schlagworte:	Ambient temperature Atomic properties Benzene Ceramics Chemistry Chemistry and Materials Science Colloidal gels. Colloidal sols Colloidal state and disperse state Composites Ethanol Exact sciences and technology General and physical chemistry Glass Hydrocarbons Hydrolysis Hydroxyl groups Inorganic Chemistry Materials Science Molecular interactions Nanotechnology Natural Materials NMR Nuclear magnetic resonance Optical and Electronic Materials Original Paper Polysilsesquioxanes Precursors Silicon Sol gel process
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